Abstract: Disclosed is a tungsten film coating method using tungsten oxide powders including the steps of contacting the tungsten oxide powders with a metal substrate and carrying out thermal reduction treatment thereon at a temperature of at least 650° C. under a hydrogen atmosphere just to coat the tungsten film on the metal substrate. Accordingly, the present invention enables to provide a simple method of coating a tungsten thin film on a metal substrate using the phenomenon of tungsten migration through vapor phase when thermal reduction treatment is carried out on tungsten oxide powders without using previous chemical or physical vapor depositions requiring expensive precision equipments or causing environmental pollution.

Abstract: A hollow work having a hole communicating with the outside and a fine metal powder producing material are placed into a treating vessel, where the fine metal powder producing material is brought into flowing contact with the surface of the work, thereby adhering a fine metal powder produced from the fine metal powder producing material to the surface of the work. The hollow work may be a ring-shaped bonded magnet. Thus, a film having an excellent corrosion resistance can be formed without use of a third component such as a resin and a coupling agent by providing an electric conductivity to the entire surface of the magnet, i.e., not only to the outer surface (including end faces) but also to the inner surface of the magnet and subjecting the magnet to an electroplating treatment.

Abstract: A negative electrode material is provided for a rechargeable lithium-ion electrochemical cell comprising an intimate mixture of finely-divided elemental nickel and tin particles characterized in that the total oxygen content of said material is less than about 6 percent by weight of the mixture. Preferably, the negative electrode material comprises from about 5 to 90 percent by weight nickel particles and from about 10 to 95 percent by weight tin particles, the nickel and tin particles being composed of discrete, non-spherical, smooth particles of a size ranging from about 1 to 10 micrometers and having a density which is greater than about 5 grams per milliter and a specific surface area of less than about 1 square meter per gram.

Abstract: The invention relates to a process for producing a surface layer with embedded inter-metallic phases, which is distinguished by the fact that a layer comprising a metal and a ceramic is applied to a substrate element, that a reaction takes place between the metal and the ceramic of the layer as a result of energy being introduced during the application of the layer or as a result of a subsequent introduction of energy, and as a result the surface layer is produced, with inter-metallic phases being formed.

Abstract: A method of manufacturing a permanent magnet by the steps of preparing an admixture of magnetic material and binder material, the admixture material having a particle size of less than 325 mesh. Then heating a carrier gas to a temperature substantially below the melting point of either component of the admixture. The admixture is introduced into the carrier gas and the admixture is sprayed atop a ductile carrier. The admixture adheres to the carrier and forms a solid permanent magnet. An electric field is applied to the sprayed admixture to create a permanent magnetic moment.

Abstract: Disclosed is a process for making a flexible magnet with an induced anisotropy, and in particular to a process for making a flexible anisotropic magnet by thermal spraying in the presence of an applied magnetic field. The method may be used to fabricate a substrate having a flexible anisotropic magnetic coating or a free standing anisotropic flexible magnet.

Abstract: A cold spraying process for forming a coating of powder particles sprayed in a gas substantially at ambient temperature onto a workpiece is improved by placement in a low ambient pressure environment in which the pressure is substantially less than atmospheric pressure. The low pressure environment acts to substantially accelerate the sprayed powder particles, thereby forming an improved coating of the particles on the workpiece. The low ambient pressure environment is provided by a vacuum tank coupled to a vacuum pump and having both the workpiece and a cold spray gun located therein. The cold spray gun is coupled to a source of pressurized inert gas as well as to a feeder for providing a flow of the powder to be sprayed. A gas compressor downstream of the vacuum pump compresses gas from the vacuum tank for recycling to the source of pressurized gas.

Abstract: A method is provided for applying metallic or metal-ceramic coatings to a product surface, particularly during the manufacture and repair of pressurized articles and products which require increased corrosion resistance, heat resistance and other qualities. Compressed air is preliminary heated to a temperature of from 400 to 700° C., forming a high-velocity air flow in a supersonic nozzle. A powder material, which is a mechanical mixture of ceramic and metal powders, is accelerating by the flow and is applied to a product surface. The metal powder is a powder mixture of at least two metals, one of which is zinc powder in an amount of from 20 to 60% of the metal powder total weight. The presence of zinc in the powder material and the heating of the compressed air to 400 to 700° C. assures high-efficiency production of coatings having low gas-permeability and high coating-to-substrate bond strength.

Abstract: Described herein is a method to fabricate porous thin-film electrodes for fuel cells and fuel cell stacks. Furthermore, the method can be used for all fuel cell electrolyte materials which utilize a continuous electrolyte layer. An electrode layer is deposited on a porous host structure by flowing gas (for example, Argon) from the bottomside of the host structure while simultaneously depositing a conductive material onto the topside of the host structure. By controlling the gas flow rate through the pores, along with the process conditions and deposition rate of the thin-film electrode material, a film of a pre-determined thickness can be formed. Once the porous electrode is formed, a continuous electrolyte thin-film is deposited, followed by a second porous electrode to complete the fuel cell structure.

Abstract: Disclosed is a system and a method for applying both a kinetic spray applied coating layer and a thermal spray applied layer onto a substrate using a single application nozzle. The system includes a higher heat capacity gas heater to permit oscillation between a kinetic spray mode wherein the particles being applied are not thermally softened and a thermal spray mode wherein the particles being applied are thermally softened prior to application. The system increases the versatility of the spray nozzle and addresses several problems inherent in kinetic spray applied coatings.

Abstract: A metallic base material is covered with a coating layer of intermetallic compound, or a plurality of metallic base materials are welded to each other with an intermetallic compound, with reduced energy consumption within a short period of time. First metallic substance 31 in powdery form is piled up on metallic base material 2. Second metallic substance 3 in molten form is delivered onto piling layer 80 of the first substance. Thus, under the control of reaction initiation temperature, coating layer (or building up coating layer) 84 of intermetallic compound having a thickness of hundreds of microns (&mgr;m) to millimeters (mm) is formed on the base material 2 by the self-exothermic reaction between the first substance and the second substance. This method is also useful in the welding of a plurality of metallic base materials to each other with an intermetallic compound. The first substance can be constituted of, for example, Ni, Co or Fe. The second substance can be constituted of, for example, Al or Ti.

Abstract: A method for manufacturing a cover assembly including a transparent window portion and a metallic frame that can be joined to a micro-device package base to form a hermetically sealed micro-device package. A sheet of a transparent material is provided having a window portion defined thereupon, the window portion having finished top and bottom surfaces. A frame-attachment area is prepared on the sheet, the frame-attachment area circumscribing the window portion. A first quantity of powdered metal particles is sprayed onto the prepared frame-attachment area of the sheet using a jet of gas, the gas being at a temperature below the fusing temperature of the metal particles. The jet of gas has a velocity sufficient to cause the metal particles to merge with one another upon impact with the sheet and with one another so as to form an initial continuous metallic coating adhering to the frame-attachment area of the sheet.

Abstract: An abrasive coating and a process for forming the abrasive coating by co-depositing hard particles within a matrix material onto a substrate using a cold spray process. The cold sprayed combination of hard particles and matrix material provides a coating that is wear, erosion and oxidation resistant. The abrasive coating may have different compositions across its depth. The hard particles may be deposited at different densities across the thickness of the matrix material. A first layer of the abrasive coating proximate the surface of the substrate may be devoid of hard particles.

Abstract: A method for producing an orthopaedic implant having enhanced fatigue strength. A forged implant substrate having an elongated stem is incorporated with a melting point lowering substance. Then, metal particles are sintered to the substrate, forming a porous layer on the substrate which enhances bone in growth or the mechanical interlock with bone cement. Advantageously, the sintering occurs at a lower temperature than if the substance were not incorporated into the substrate, which in turn results in an enhanced fatigue strength of the inventive implant. The fatigue strength of a forged or cast implant can also be improved by nitrogen diffusion hardening and/or thermally processing the implant after the porous coating is adhered by sintering. Further, the fatigue strength can be further improved by combining incorporating the melting point lowering substance with nitrogen diffusion hardening and/or aging treatment subsequent to sintering.

Abstract: A method for protecting low-carbon steel and stainless steel from coking and corrosion at elevated temperatures in corrosive environments, such as during ethylene production by pyrolysis of hydrocarbons or the reduction of oxide ores, by coating the stainless steel with a coating of MCrAlXSiT in which M is nickel, cobalt, iron or a mixture thereof, X is yttrium, hafnium, zirconium, lanthanum, scandium or combination thereof, and T is tantalum, titanium, platinum, palladium, rhenium, molybdenum, tungsten, niobium, boron or combination thereof. A blended powder composition to produce a desired MCrAlXSiT surface alloy may be applied to the substrate. The overlay coating and stainless steel substrate preferably are heat-treated at about 1000 to 1200° C. for about 10 minutes or longer effective to metallurgically bond the overlay coating to the substrate and to form a multiphased microstructure.

Abstract: A method for forming a pattern on a surface of a panel substrate, includes electrically charging pattern-forming material particles, jetting out the electrically charged pattern-forming material particles through a nozzle by applying electrostatic force to the pattern-forming material particles to form a pattern, and fixing the pattern onto the panel substrate.

Abstract: A process for coating an object formed of magnesium or a magnesium alloy comprising the steps of: immersion coating the object in a sonicated bath to form an undercoat and topcoating the object to form a topcoat. When desirable to protect against topcoat failure, the undercoat may be equally noble or more noble than the topcoat. If topcoat failure is not a concern, the nobility of the topcoat relative to the undercoat need not be considered. The process promotes uniform coating of a magnesium and its alloys.

Abstract: A process for fabricating a ceramic electroactive transducer of a predetermined shape is disclosed. The process comprises the steps of providing a suitably shaped core having an outer surface, attaching a first conductor to the outer surface of the core, coating an inner conductive electrode on the the outer surface of the core such that the inner conductive electrode is in electrical communication with the first conductor, coating a ceramic layer onto the inner electrode, thereafter sintering the ceramic layer, coating an outer electrode onto the sintered ceramic layer to produce an outer electrode that is not in electrical communication with the first conductor, and then poling the sintered ceramic layer across the inner electrode and the outer electrode to produce the ceramic electrode.

Abstract: A substrate is coated with a conductive layer, which comprises a conductive layer of bonded ultrafine metal particles formed on the top surface thereof. The ultrafine metal particles have a diameter of 1-20 nm, and the substrate is of a flexible high polymer material. Since the conductive layer is formed by bonded layer of the ultrafine metal particles, an extremely thin layer having high conductivity can be formed. This structure enables the formation of a flexible printed circuit board with high-density interconnects or a transparent conductive film provided with both transparency and conductivity. Conventional vacuum equipments and complicated processes are not necessary for forming the conductive layer on the substrate.

Abstract: Methods of manufacturing printed circuit boards are disclosed. The methods utilize various printing techniques to apply conductive compositions to substrates in the creation of printed circuit boards. The method of manufacturing printed circuit board comprises the step of applying conductive composition to a substrate through a cold welding process.

Abstract: The present invention is drawn toward a method of forming conductive paths on a substrate using ink-jet technology. An ink-jettable suspension or solution can be formed containing a conductive particulate having certain desired conductive properties. The suspension can then be ink-jetted onto a substrate such as ceramic, epoxy glass, or other materials in a given pattern using various ink-jet printing technologies and methods. Depending on the chosen conductive particulates, suspension components, and substrate, the printed pattern of conductive particulates may then be heated to further enhance the conductive properties of the particulates through bonding and/or sintering.

Abstract: A method of depositing large particles having an average nominal diameter of greater than 106 microns up to 250 microns onto substrates using a kinetic spray system is disclosed. The method utilizes a powder injector tube having a reduced inner diameter and a de Laval type nozzle having an elongated throat to exit end length. The method permits deposition of much larger particles than previously possible.

Abstract: Nanostructured non-stoichiometric materials are disclosed. Novel photonic materials and their applications are discussed. More specifically, the specifications teach the use of nanotechnology and nanostructured materials for developing novel photonic and optical applications.

Abstract: Colored roofing granules and methods for their preparations, having decorative metallic appearance and enhanced stability against discoloration of color containing a silica-encapsulated metallic flake or colored lamellar effect pigment distributed in an insolubilized alkali silicate coating.

Abstract: A method and apparatus for directly making rapid prototype tooling from a computer model having a free-form shape. The method steps comprise essentially: (a) machining a soft metal tooling base so as to contour at least one free-form surface in conformity with the computer model; (b) cold-gas dynamic spraying the contoured surface to form superimposed impact welded metal particle layers, the layers consisting of at least one thermal management under-layer comprising primarily copper, and at least an outer wear resistant layer comprising primarily tool steel.

Abstract: A method of manufacturing electric machines comprised of geometrically patterned arrays of permanent magnets, soft magnetic materials, and electrical conductors deposited by kinetic spraying methods directly atop a carrier. The magnets and planar coils of the present invention may be integrally formed atop carriers to form electrical machines such as motors, generators, alternators, solenoids, and actuators. The manufacturing techniques used in this invention may produce highly defined articles that do not require additional shaping or attaching steps. Very high-purity permanent and soft magnetic materials, and conductors with low oxidation are produced.

Abstract: The present invention relates to methods for selectively enhancing corrosion protection of fabricated metal parts. One method of the present invention includes providing a non-galvanized metal sheet to be processed to form the fabricated metal part; selecting a localized region on the non-galvanized metal sheet; roughening the localized region for acceptance of a protective coating; applying a protective coating to localized region; and fabricating the non-galvanized metal sheet into a fabricated metal part. Another method includes providing a galvanized metal sheet; selecting a localized region on the galvanized metal sheet; applying a protective coating to the localized region; and fabricating the galvanized metal sheet into a fabricated metal part. Yet another method includes selecting a localized region on a fabricated metal part; roughening the localized region for acceptance of a protective coating; and applying the protective coating to the localized region.

Abstract: Nanostructured non-stoichiometric materials are disclosed. Novel sensing materials and their applications are discussed. More specifically, the specifications teach the use of nanotechnology and nanostructured materials for developing novel sensing devices and products.

Abstract: A method for making an electrically conductive pattern, including:

Abstract: A negative electrode material is provided for a rechargeable lithium-ion electrochemical cell comprising an intimate mixture of finely-divided elemental nickel and tin particles characterized in that the total oxygen content of said material is less than about 6 percent by weight of the mixture. Preferably, the negative electrode material comprises from about 5 to 90 percent by weight nickel particles and from about 10 to 95 percent by weight tin particles, the nickel and tin particles being composed of discrete, non-spherical, smooth particles of a size ranging from about 1 to 10 micrometers and having a density which is greater than about 5 grams per milliter and a specific surface area of less than about 1 square meter per gram.

Abstract: A drill resistant plate, which presents a rough surface of hardened particles to drilling attack, and which tends to snap or destroy drill bits before they can began drilling. The plate is made by brazing hard particles into a matrix of brazing material attached to a steel plate. Nickel-Silver brazing material is used to form the matrix on the steel plate, and tungsten carbide particles of 8-10 mesh are secured within the matrix, with the hard particles of tungsten carbide partially exposed, presenting a roughened surface with angular pieces of tungsten carbide to the drilling attack.

Abstract: A method for modifying a porous mechanical component by using an ER or MR substance including the steps of providing at least one porous component having a porosity sufficient to receive the MR substance within a plurality of pores and impregnating the component with the MR substance.

Abstract: Magnetic composites exhibit distinct flux properties due to gradient interfaces. The composites can be used to improve fuel cells and effect transport and separation of different species of materials. A variety of devices can be made utilizing the composites including a separator, a cell, an electrode for channeling flux of magnetic species, an electrode for effecting electrolysis of magnetic species, a system for channeling electrolyte species, a system for separating particles with different magnetic susceptibilities. Some composites can be used to make a dual sensor for distinguishing between two species of materials and a flux switch to regulate the flow of a redox species and a flux switch to regulate the flow of a chemical species. Some composites can control chemical species transport and distribution.

Abstract: A method for coating a surface of a substrate, includes providing a substrate having a surface, and coating the surface with a foam suspension containing a powder suspended in a foam to form a coating on the surface. The substrate is then heat treated to densify the coating along the surface.

Abstract: To provide a film forming method, a film forming apparatus and a manufacturing method of ultrafine particle films, implementing an efficient and proper film thickness control. The manufacturing method of ultrafine particle films includes the steps of: guiding metal ultrafine particles generated in an ultrafine particle generation chamber together with a carrier gas through a conveying pipe to the film forming chamber; and forming a film on a substrate installed over a stage in the film forming chamber through a nozzle, and the evaporated amount of said evaporation material or the thickness of a formed film is controlled by using either the intensity of the emission spectrum intrinsic to an evaporation material or that of the emission spectrum intrinsic to the carrier gas, or else by using both of these.

Abstract: A method for forming a metal-containing layer on a substrate is disclosed. A slurry of the metal is first deposited on the substrate; followed by heating to remove volatile material from the slurry, and to form a layer of the metal. In another embodiment, a slurry of aluminum is deposited over the slurry of the metal, before or after the metal has been heat-treated to some degree. A diffusion heat treatment results in a coating which includes the noble-metal aluminide compound. Related articles are also disclosed.

Abstract: Provided is a ceramic coated product and a coating for it, making it possible to improve corrosion resistance, wear resistance and the like of a material to be treated, and heighten aesthetically commercial value by a thin film forming or producing method using low-priced equipment. An ejection powder and a reactive ejecting gas are ejected onto a surface of a material to be treated comprising a metal product, a ceramic, or a mixture thereof. The ejection powder is heated on the surface of the material to be treated and then is reacted with the reactive ejecting gas. The resultant product is activation-adsorbed onto the surface of the material to be treated and caused to diffuse and penetrate thereinto. Thus, a layer made of a nitride or other compounds is formed.

Abstract: Corrosion resistant metal, either platinum or MCrAlY is bonded to a corrosion sensitive metal such as nickel based superalloys by coating the surface with the corrosion resistant metal particles held in a binder and covering this with a metalide generating tape. This is then heated to cause the formation of the metalide coating on the metal surface, which in turn, bonds the corrosion resistant metal to the surface.

Abstract: A process (20) for applying a thermal barrier coating (51) to a turbine component (50) including the step (34) of depositing a bond coating layer (56) by, directing solid particles using a cold spray process. The layer of bond coating material may have different depths (80,82) in different areas of the component (50), and it may have different compositions (60,62) across its depth. The precise control afforded by the cold spray material deposition step allows the surface of the bond coating material layer to be formed with a predetermined surface roughness or with a plurality of micro-ridges (86) in order to optimize its bond to the overlying ceramic insulating layer (52).

Abstract: A method for providing the surface of base bodies of displacement or angle measuring systems with magnetizable material. Hard ferrite powder or materials comprising rare earths are preferred components of the magnetizable coating material. The composition of the material is changed during application of the coating such that the percentage of the ferrite or rare earth compound is increased.

Abstract: A method of applying blend drop granules to an asphalt coated sheet includes moving an asphalt coated sheet in a machine direction, and depositing blend drops of granules on a blend drop conveyor that is positioned above the asphalt coated sheet. The blend drop conveyor has an upper flight moving in a direction opposite the machine direction and a lower flight moving in the machine direction. The blend drops are moved from the upper flight to the lower flight of the blend drop conveyor while retaining the blend drops in contact with the blend drop conveyor by magnetic force. Finally. The blend drops are released from the blend drop conveyor for contact with the asphalt coated sheet.

Abstract: A “one-step” method of forming diffused noble metal-aluminide coatings with or without minor incorporations of Si, Cr, Mn, Hf, La, and Y, is disclosed. With the inventive method, two or more powdered metals or metal alloys are applied and diffused into the metal substrate together, using a sequential multi-stage heating process. This method contrasts with the prior art technology where metals were applied and diffused into the substrate separately.

Abstract: A method for producing an orthopaedic implant having enhanced fatigue strength. A forged implant substrate having an elongated stem is incorporated with a melting point lowering substance. Then, metal particles are sintered to the substrate, forming a porous layer on the substrate which enhances bone ingrowth or the mechanical interlock with bone cement. Advantageously, the sintering occurs at a lower temperature than if the substance were not incorporated into the substrate, which in turn results in an enhanced fatigue strength of the inventive implant. The fatigue strength of a forged or cast implant can also be improved by nitrogen diffusion hardening and/or thermally processing the implant after the porous coating is adhered by sintering. Further, the fatigue strength can be further improved by combining incorporating the melting point lowering substance with nitrogen diffusion hardening and/or aging treatment subsequent to sintering.

Abstract: A method for preparing an aluminum alloy-containing coating composition is described. A slurry containing a selected amount of aluminum is combined with at least one additional slurry containing a selected amount of a second metal which forms an alloy with aluminum. The resulting slurry mixture is applied to a metal substrate, and then heated to form a substantially devolatilized coating. The coating then receives a secondary heat treatment. Related compositions and articles are also described, as are processes for repairing a damaged or worn coating, utilizing the slurry.

Abstract: A resin molded product and a fine metal powder producing material are placed into a treating vessel. The fine metal powder producing material is brought into flowing contact with the surface of the resin molded product, thereby producing a fine metal powder, and forming a metal layer of the fine metal powder on the surface of the resin molded product. In this process, the metal layer of the fine metal powder can be formed firmly and at high density on the surface of the resin molded product. The metal layer exhibits a function as an electrically conductive layer. Therefore, a metal film having an excellent thickness accuracy, an excellent surface smoothness and a high peel strength can be formed in a simple manner on the metal layer by carrying out an electroplating treatment. In addition, it is possible for the metal layer itself to exhibit functions or properties such as an ornamentality.

Abstract: To provide a film forming method, a film forming apparatus and a manufacturing method of ultrafine particle films, implementing an efficient and proper film thickness control. The manufacturing method of ultrafine particle films includes the steps of: guiding metal ultrafine particles generated in an ultrafine particle generation chamber together with a carrier gas through a conveying pipe to the film forming chamber; and forming a film on a substrate installed over a stage in the film forming chamber through a nozzle, and the evaporated amount of said evaporation material or the thickness of a formed film is controlled by using either the intensity of the emission spectrum intrinsic to an evaporation material or that of the emission spectrum intrinsic to the carrier gas, or else by using both of these.

Abstract: A cold spray process (20) for applying an abradable coating (16) to a substrate material (12). A bond coat layer (14) and/or an abradable coating material layer (16) are applied to a substrate (12) by directing particles of the material toward the substrate surface at a velocity sufficiently high to cause the particles to deform and to adhere to the surface. Particles of the bond coat material may first be directed toward the substrate surface at a velocity sufficiently high to clean the surface (24) but not sufficiently high to cause the particles to deform and to adhere to the surface.

Abstract: A method of applying blend drop granules to an asphalt coated sheet includes moving an asphalt coated sheet in a machine direction, and depositing blend drops of granules on a blend drop conveyor that is positioned above the asphalt coated sheet. The blend drop conveyor has an upper flight moving in a direction opposite the machine direction and a lower flight moving in the machine direction. The blend drops are moved from the upper flight to the lower flight of the blend drop conveyor while retaining the blend drops in contact with the blend drop conveyor by magnetic force. Finally. The blend drops are released from the blend drop conveyor for contact with the asphalt coated sheet.

Abstract: A metallic base material is covered with a coating layer of intermetallic compound, or a plurality of metallic base materials are welded to each other with an intermetallic compound, with reduced energy consumption within a short period of time. First metallic substance 31 in powdery form is piled up on metallic base material 2. Second metallic substance 3 in molten form is delivered onto piling layer 80 of the first substance. Thus, under the control of reaction initiation temperature, coating layer (or building up coating layer) 84 of intermetallic compound having a thickness of hundreds of microns (&mgr;m) to millimeters (mm) is formed on the base material 2 by the self-exothermic reaction between the first substance and the second substance. This method is also useful in the welding of a plurality of metallic base materials to each other with an intermetallic compound. The first substance can be constituted of, for example, Ni, Co or Fe. The second substance can be constituted of, for example, Al or Ti.

Abstract: A hollow work having a hole communicating with the outside and a fine metal powder producing material are placed into a treating vessel, where the fine metal powder producing material is brought into flowing contact with the surface of the work, thereby adhering a fine metal powder produced from the fine metal powder producing material to the surface of the work. The hollow work may be a ring-shaped bonded magnet. Thus, a film having an excellent corrosion resistance can be formed without use of a third component such as a resin and a coupling agent by providing an electric conductivity to the entire surface of the magnet, i.e., not only to the outer surface (including end faces) but also to the inner surface of the magnet and subjecting the magnet to an electroplating treatment.