Carbide-, Nitride-, Or Sulfide-containing Layer Patents (Class 428/698)
  • Patent number: 11878945
    Abstract: In some examples, a method may include depositing, from a slurry comprising particles including silicon metal, a bond coat precursor layer including the particles comprising silicon metal directly on a ceramic matrix composite substrate. The method also may include locally heating the bond coat precursor layer to form a bond coat comprising silicon metal. Additionally, the method may include forming a protective coating on the bond coat. In some examples, an article may include a ceramic matrix composite substrate, a bond coat directly on the substrate, and a protective coating on the bond coat. The bond coat may include silicon metal and a metal comprising at least one of Zr, Y, Yb, Hf, Ti, Al, Cr, Mo, Nb, Ta, or a rare earth metal.
    Type: Grant
    Filed: February 3, 2021
    Date of Patent: January 23, 2024
    Assignees: Rolls-Royce Corporation, Rolls-Royce High Temperature Composites, Inc.
    Inventors: Sungbo Shim, Kang N. Lee, Stephen Isaiah Harris, Andrew Joseph Lazur
  • Patent number: 11832521
    Abstract: A method of forming a piezoelectric thin film can include depositing a material on a first surface of a Si substrate to provide a stress neutral template layer. A piezoelectric thin film including a Group III element and nitrogen can be sputtered onto the stress neutral template layer and a second surface of the Si substrate that is opposite the first surface can be processed to remove that Si substrate and the stress neutral template layer to provide a remaining portion of the piezoelectric thin film. A piezoelectric resonator can be formed on the remaining portion of the piezoelectric thin film.
    Type: Grant
    Filed: April 17, 2020
    Date of Patent: November 28, 2023
    Assignee: Akoustis, Inc.
    Inventors: Craig Moe, Jeffrey M. Leathersich
  • Patent number: 11767268
    Abstract: A cubic boron nitride sintered material comprises 30% by volume or more and 99.9% by volume or less of cubic boron nitride grains and 0.1% by volume or more and 70% by volume or less of a binder phase, the cubic boron nitride grain having a carbon content of 0.08% by mass or less, the cubic boron nitride sintered material being free of free carbon.
    Type: Grant
    Filed: December 16, 2019
    Date of Patent: September 26, 2023
    Assignee: SUMITOMO ELECTRIC INDUSTRIES, LTD.
    Inventors: Akito Ishii, Katsumi Okamura
  • Patent number: 11591695
    Abstract: A surface coated member having improved stability and a longer service life is provided. The surface coated member includes a base member and a hard coating formed on a surface thereof. The hard coating is constituted of one or more layers. At least one layer among the layers is a layer including hard particles. The hard particles include a multilayer structure having a first unit layer and a second unit layer being layered alternately. The first unit layer includes a first compound. The second unit layer includes a second compound. The first compound and the second compound are respectively made of one or more kind of element selected from the group consisting of a group 4 element, a group 5 element, a group 6 element of a periodic table, and Al, and one or more kind of element selected from the group consisting of B, C, N, and O.
    Type: Grant
    Filed: October 9, 2019
    Date of Patent: February 28, 2023
    Assignee: Sumitomo Electric Hardmetal Corp.
    Inventors: Anongsack Paseuth, Kazuo Yamagata, Susumu Okuno, Hideaki Kanaoka, Hiroyuki Morimoto, Minoru Itoh
  • Patent number: 11591267
    Abstract: An automated preparation method of a SiCf/SiC composite flame tube, comprising the following steps: preparing an interface layer for a SiC fiber by a chemical vapor infiltration process, and obtaining the SiC fiber with a continuous interface layer; laying a unidirectional tape on the SiC fiber with the continuous interface layer and winding the SiC fiber with the continuous interface layer to form and obtaining a preform of a net size molding according to a fiber volume and a fiber orientation obtained in a simulation calculation; and adopting a reactive melt infiltration process and the chemical vapor infiltration process successively for a densification and obtaining a high-density SiCf/SiC composite flame tube in a full intelligent way. The SiCf/SiC composite flame tube prepared by the present disclosure not only has a high temperature resistance, but also has a low thermal expansion coefficient, high thermal conductivity and high thermal shock resistance.
    Type: Grant
    Filed: September 14, 2021
    Date of Patent: February 28, 2023
    Assignee: CENTRAL SOUTH UNIVERSITY
    Inventor: Haitang Yang
  • Patent number: 11566203
    Abstract: A non-stoichiometric nanocomposite coating and method of making and using the coating. The non-stoichiometric nanocomposite coating is disposed on a base material, such as a metal or ceramic; and the nanocomposite consists essentially of a matrix of an alloy selected from the group of Cu, Ni, Pd, Pt and Re which are catalytically active for cracking of carbon bonds in oils and greases and a grain structure selected from the group of borides, carbides and nitrides.
    Type: Grant
    Filed: September 25, 2020
    Date of Patent: January 31, 2023
    Assignee: UChicago Argonne, LLC
    Inventors: Osman Levent Eryilmaz, Vanessa DaSilva, Ali Erdemir
  • Patent number: 11555255
    Abstract: A member for an apparatus for manufacturing a semiconductor single crystal having long product life and a tantalum carbide coated carbon material are provided. The tantalum carbide coated carbon material according to the present invention is a tantalum carbide coated carbon material in which at least a part of a surface of a carbon base material is coated with a tantalum carbide coated film containing tantalum carbide as a main component, in which in the tantalum carbide coated film, an intensity of an X-ray diffraction line corresponding to a plane with respect to an out-of-plane direction is larger than intensities of X-ray diffraction lines corresponding to other crystal planes, and the intensity ratio is 60% or more with respect to a sum of intensities of X-ray diffraction lines corresponding to all crystal planes.
    Type: Grant
    Filed: January 15, 2021
    Date of Patent: January 17, 2023
    Assignee: SHIN-ETSU CHEMICAL CO., LTD.
    Inventors: Chikara Mori, Waichi Yamamura, Shoji Kano, Akihiro Hirate
  • Patent number: 11541468
    Abstract: A coated tool of the present disclosure is provided with a base member and a coating layer located on a surface of the base member. The coating layer includes a TiCNO layer and an Al2O3 layer. The Al2O3 layer is located in contact with the TiCNO layer at a position farther from the base member than the TiCNO layer is. The TiCNO layer includes a plurality of first protrusions that project toward the Al2O3 layer, and a beam that extends in a direction intersecting a direction in which the first protrusions project, to connect the first protrusions. A cutting tool of the present disclosure is provided with: a holder extending from a first end toward a second end and including a pocket on a side of the first end; and the above-described coated tool located in the pocket.
    Type: Grant
    Filed: January 28, 2019
    Date of Patent: January 3, 2023
    Assignee: KYOCERA Corporation
    Inventors: Yuusaku Sugawa, Yoshikazu Kodama, Kenji Kumai, Takanori Sugiyama, Hirotoshi Itoh
  • Patent number: 11534835
    Abstract: A coated tool of the present disclosure is provided with a base member and a coating layer located on a surface of the base member. The coating layer includes a TiCNO layer and an Al2O3 layer. The Al2O3 layer is located in contact with the TiCNO layer at a position farther from the base member than the TiCNO layer is. The TiCNO layer includes a first composite protrusion including a first protrusion that projects toward the Al2O3 layer and a second protrusion that projects from the first protrusion in a direction intersecting a direction in which the first protrusion projects. A cutting tool of the present disclosure is provided with: a holder extending from a first end toward a second end and including a pocket on a side of the first end; and the above-described coated tool located in the pocket.
    Type: Grant
    Filed: January 28, 2019
    Date of Patent: December 27, 2022
    Assignee: KYOCERA Corporation
    Inventors: Yuusaku Sugawa, Yoshikazu Kodama, Kenji Kumai, Takanori Sugiyama, Hirotoshi Itoh
  • Patent number: 11517966
    Abstract: A coated tool of the present disclosure is provided with a base member and a coating layer located on a surface of the base member. The coating layer includes a TiCNO layer and an Al2O3 layer. The Al2O3 layer is located in contact with the TiCNO layer at a position farther from the base member than the TiCNO layer is. The TiCNO layer includes a composite protrusion including a first protrusion that projects toward the Al2O3 layer, a second protrusion that projects from the first protrusion in a direction intersecting a direction in which the first protrusion projects, and a third protrusion that projects from the second protrusion in a direction intersecting the direction in which the second protrusion projects.
    Type: Grant
    Filed: January 28, 2019
    Date of Patent: December 6, 2022
    Assignee: KYOCERA CORPORATION
    Inventors: Yuusaku Sugawa, Yoshikazu Kodama, Kenji Kumai, Takanori Sugiyama, Hirotoshi Itoh
  • Patent number: 11511352
    Abstract: Provided is a coated cutting tool having a base material side single layer portion and a laminated portion provided as a hard coating in order from a base material side. The base material side single layer portion is formed of a nitride-based hard coating in which a proportion of Al is highest among metal (including metalloid) elements, a sum of Al and Cr in a content ratio (atomic ratio) is 0.9 or more, and at least B is contained. In the laminated portion, a nitride-based a layer in which a proportion of Ti is highest among metal (including metalloid) elements and at least B is contained, and a nitride-based b layer in which a proportion of Al is highest among metal (including metalloid) elements and at least Cr and B are contained are alternately laminated.
    Type: Grant
    Filed: March 27, 2019
    Date of Patent: November 29, 2022
    Assignee: MOLDINO Tool Engineering, Ltd.
    Inventor: Ryoutarou Fuwa
  • Patent number: 11471949
    Abstract: Provided is a coated cutting tool having a base material side single layer portion and a laminated portion provided as a hard coating in order from a base material side. The base material side single layer portion is formed of a nitride-based hard coating in which a proportion of Al is highest among metal (including metalloid) elements, a sum of Al and Cr in a content ratio (atomic ratio) is 0.9 or more, and at least B is contained. In the laminated portion, a nitride-based a layer in which a proportion of Ti is highest among metal (including metalloid) elements and at least B is contained, and a nitride-based b layer in which a proportion of Al is highest among metal (including metalloid) elements and at least Cr and B are contained are alternately laminated.
    Type: Grant
    Filed: March 27, 2019
    Date of Patent: October 18, 2022
    Assignee: MOLDINO Tool Engineering, Ltd.
    Inventor: Ryoutarou Fuwa
  • Patent number: 11430686
    Abstract: Substrate supports comprising a top plate positioned on a shaft are described. The top plate including a primary heating element a first depth from the surface of the top plate, a inner zone heating element a second depth from the surface of the top plate and an outer zone heating element a third depth from the surface of the top plate. Substrate support assemblies comprising a plurality of substrate supports and methods of processing a substrate are also disclosed.
    Type: Grant
    Filed: October 9, 2020
    Date of Patent: August 30, 2022
    Assignee: APPLIED MATERIALS, INC.
    Inventors: Tejas Ulavi, Sanjeev Baluja, Dhritiman Subha Kashyap
  • Patent number: 11421307
    Abstract: Provided is a cemented carbide having superior wear resistance and fracture resistance. A cemented carbide containing 50.0 mass % or more and 94.5 mass % or less of tungsten carbide, 5.0 mass % or more and 12.0 mass % or less of Co, and 0.5 mass % or more and 4.0 mass % or less of Ru, the cemented carbide comprising a WC phase that includes tungsten carbide as a main component, and a binder phase that binds the WC phase, wherein the binder phase contains Co, the lattice constant of Co in the binder phase is 3.580 ? or more and 3.610 ? or less, and the saturation magnetization of the cemented carbide is 40% or more and 58% or less.
    Type: Grant
    Filed: November 16, 2020
    Date of Patent: August 23, 2022
    Assignee: TUNGALOY CORPORATION
    Inventor: Harufumi Suzuki
  • Patent number: 11377390
    Abstract: A cubic boron nitride sintered material includes: more than 80 volume % and less than 100 volume % of cubic boron nitride grains; and more than 0 volume % and less than 20 volume % of a binder phase. The binder phase includes: at least one selected from a group consisting of a simple substance, an alloy, and an intermetallic compound selected from a group consisting of a group 4 element, a group 5 element, a group 6 element in a periodic table, aluminum, silicon, cobalt, and nickel. A dislocation density of the cubic boron nitride grains is more than or equal to 3×1017/m2 and less than or equal to 1×1020/m2.
    Type: Grant
    Filed: December 16, 2019
    Date of Patent: July 5, 2022
    Assignees: Sumitomo Electric Industries, Ltd., SUMITOMO ELECTRIC HARDMETAL CORP.
    Inventors: Akito Ishii, Katsumi Okamura, Hironari Moroguchi, Satoru Kukino
  • Patent number: 11370717
    Abstract: A protective coating system includes a substrate that has an exterior surface exhibiting a degree of valley/hill surface irregularity including a plurality of hills and a plurality of valleys and a first coating layer formed directly on to the exterior surface of the substrate and that conforms to the exterior surface of the substrate such that the first coating layer has a non-uniform coating thickness over the substrate. The protective coating system further includes a second coating layer formed directly on to the exterior surface of the first coating layer. The second coating layer includes a plurality of pores within the second coating layer. Still further, the protective coating system includes a third coating layer formed within at least some of the plurality of pores within the second coating layer.
    Type: Grant
    Filed: March 6, 2020
    Date of Patent: June 28, 2022
    Assignee: HONEYWELL INTERNATIONAL INC.
    Inventors: Reza Oboodi, Eric Passman, Bahram Jadidian
  • Patent number: 11362293
    Abstract: Embodiments related to interlayers (e.g., interlayers comprising a transition metal oxide, a transition metal oxynitride, and/or a transition metal nitride) and associated systems, devices (e.g., photovoltaic devices), and methods are disclosed. In some embodiments, a system for exciton transfer includes a substrate including an inorganic semiconductor. An interlayer may be disposed on the substrate, and a layer including a material that undergoes singlet exciton fission when exposed to electromagnetic radiation may be disposed on the interlayer. The interlayer may be disposed between the substrate and the layer. In some embodiments, a method for manufacturing a system for exciton transfer involves depositing an interlayer onto a substrate that includes an inorganic semiconductor. The method may also include depositing a layer including a material that undergoes singlet exciton fission when exposed to electromagnetic radiation onto the interlayer.
    Type: Grant
    Filed: May 30, 2019
    Date of Patent: June 14, 2022
    Assignee: Massachusetts Institute of Technology
    Inventors: Marc A. Baldo, Tony Wu, Markus Einzinger
  • Patent number: 11309213
    Abstract: A method for manufacturing a semiconductor structure includes following operations. A sacrificial layer is formed over the conductive layer, wherein the sacrificial layer includes a first sacrificial portion over the first conductive portion, and a second sacrificial portion over the second conductive portion, and a first thickness of the first sacrificial portion is larger than a second thickness of the second sacrificial portion. The first sacrificial portion and the second sacrificial portion of the sacrificial layer, and the second conductive portion of the conductive layer are removed.
    Type: Grant
    Filed: July 27, 2020
    Date of Patent: April 19, 2022
    Assignee: TAIWAN SEMICONDUCTOR MANUFACTURING COMPANY LTD.
    Inventors: Yu-Hsiang Liao, Ya-Huei Li, Li-Wei Chu, Chun-Wen Nieh, Hung-Yi Huang, Chih-Wei Chang, Ching-Hwanq Su
  • Patent number: 11298748
    Abstract: A surface coated cutting tool comprises a base material and a coating layer that coats the base material, the coating layer including an alternate layer composed of a first unit layer and a second unit layer alternately stacked, the first unit layer being composed of a nitride containing aluminum and zirconium, in the first unit layer, when the total number of metal atoms constituting the first unit layer is represented as 1, a ratio thereto of the number of atoms of the zirconium being not less than 0.65 and not more than 0.95, the second unit layer being composed of a nitride containing titanium and aluminum, in the second unit layer, when the total number of metal atoms constituting the second unit layer is represented as 1, a ratio thereto of the number of atoms of the aluminum being larger than 0.40 and not more than 0.70.
    Type: Grant
    Filed: October 16, 2018
    Date of Patent: April 12, 2022
    Assignee: SUMITOMO ELECTRIC HARDMETAL CORP.
    Inventors: Haruyo Fukui, Makoto Setoyama, Keizo Tanaka, Kouhei Yoshimura
  • Patent number: 11292066
    Abstract: To provide a tool that ensures improved durability even when a diamond coating containing boron is formed. A diamond coating (40) includes a first layer (41) that is formed as a layer on a surface layer side of the diamond coating (40) and is regarded as containing no boron, and a second layer (42) positioned on a side of a base material (30) with respect to the first layer (41) and contains at least 1000 ppm or more of the boron. Since the first layer (41) with a larger compressive stress is formed on the surface layer of the diamond coating (40), a crack generation from the surface layer side of the diamond coating (40) during the process can be reduced. Consequently, the durability of a tool (1) can be improved even when the diamond coating (40) containing 1,000 ppm or more of boron is formed.
    Type: Grant
    Filed: January 16, 2017
    Date of Patent: April 5, 2022
    Assignee: OSG CORPORATION
    Inventors: Hiroyuki Hanyu, Yasuo Fukui
  • Patent number: 11285545
    Abstract: A coated cutting tool includes a substrate of cemented carbide and a coating. The cemented carbide is made of WC and a binder phase of one or more of Co, Fe and Ni. The carbon content in the cemented carbide is a substoichiometric carbon content SCC, wherein ?0.13 wt %?SCC<0 wt %, or ?0.30 wt %?SCC??0.16 wt %. The coating includes one or more layers being a metal carbide, metal nitride or metal carbonitride, the metal being at least one of Zr and Hf, and wherein Ti is present in an amount of at most 10 at-% of the amount metal. The one or more layers is situated between the substrate and the aluminum oxide layer.
    Type: Grant
    Filed: March 7, 2018
    Date of Patent: March 29, 2022
    Assignee: SANDVIK INTELLECTUAL PROPERTY AB
    Inventors: Jose Luis Garcia, Jeanette Persson
  • Patent number: 11273497
    Abstract: A coated cutting tool comprising: a substrate; and a coating layer formed on a surface of the substrate, wherein: the coating layer comprises a lower layer, an intermediate layer and an upper layer in this order from the substrate side; the lower layer comprises one or more Ti compound layers containing a Ti compound of Ti and an element of at least one kind selected from the group consisting of C, N, O and B; and the intermediate layer comprises an ?-Al2O3 layer containing ?-Al2O3; and the upper layer comprises a TiCN layer containing TiCN; an average thickness of the coating layer is within a specific range, and an average thickness of the upper layer is within a specific range; in a cross section perpendicular to the surface of the substrate, the grains in the TiCN layer constituting the upper layer satisfies a specific condition.
    Type: Grant
    Filed: December 6, 2019
    Date of Patent: March 15, 2022
    Assignee: TUNGALOY CORPORATION
    Inventor: Naoyuki Fukushima
  • Patent number: 11253926
    Abstract: A coated tool may include a base member including a first surface, and a coating layer located at least on the first surface of the base member. The coating layer may include a first layer and a second layer. The first layer may be located on the first surface and may include a titanium compound. The second layer may be contactedly located on the first layer and may include aluminum oxide. The coating layer may include a plurality of voids located side by side in the first layer in a direction along a boundary between the first layer and the second layer in a cross section orthogonal to the first surface.
    Type: Grant
    Filed: March 23, 2018
    Date of Patent: February 22, 2022
    Assignee: KYOCERA Corporation
    Inventor: Tadashi Katsuma
  • Patent number: 11253927
    Abstract: A coated cutting tool comprising a substrate and a coating layer formed on a surface of the substrate, wherein: the coating layer comprises a lower layer, an intermediate layer, and an upper layer in this order from the substrate side; the lower layer comprises one or two or more Ti compound layers containing a Ti compound of Ti and an element of at least one kind selected from the group consisting of C, N, O and B, the intermediate layer comprises an ?-Al2O3 layer containing ?-Al2O3, and the upper layer comprises a TiCNO layer containing TiCNO; an average thickness of the coating layer is 5.0 ?m or more and 30.0 ?m or less; in a specific first cross section, a misorientation A satisfies a specific condition; and in a specific second cross section, a misorientation B satisfies a specific condition.
    Type: Grant
    Filed: January 13, 2020
    Date of Patent: February 22, 2022
    Assignee: TUNGALOY CORPORATION
    Inventors: Kinya Takahashi, Naoyuki Fukushima
  • Patent number: 11247276
    Abstract: A coated cutting tool includes a substrate of cemented carbide, cermet, ceramics, steel or cubic boron nitride and a multi-layered wear resistant coating. The multi-layered wear resistant coating has a total thickness from 5 to 25 ?m and includes refractory coating layers deposited by chemical vapour deposition (CVD) or moderate temperature chemical vapour deposition (MT-CVD). The multi-layered wear resistant coating has at least one pair of layers (a) and (b), with layer (b) being deposited immediately on top of layer (a). Layer (a) is a layer of aluminium nitride having hexagonal crystal structure (h-AlN) and a thickness from 10 nm to 750 nm. Layer (b) is a layer of titanium aluminium nitride or titanium aluminium carbonitride represented by the general formula Ti1-xAlxCyNz with 0.4?x?0.95, 0?y?0.10 and 0.85?z?1.15, having a thickness from 0.5 ?m to 15 ?m, and at least 90% of the Ti1-xAlxCyNz of layer (b) has a face-centered cubic (fcc) crystal structure.
    Type: Grant
    Filed: March 31, 2017
    Date of Patent: February 15, 2022
    Assignee: Walter AG
    Inventors: Dirk Stiens, Thorsten Manns
  • Patent number: 11235388
    Abstract: A substrate holder for a lithographic apparatus has a main body having a thin-film stack provided on a surface thereof. The thin-film stack forms an electronic or electric component such as an electrode, a sensor, a heater, a transistor or a logic device, and has a top isolation layer. A plurality of burls to support a substrate are formed on the thin-film stack or in apertures of the thin-film stack.
    Type: Grant
    Filed: December 30, 2020
    Date of Patent: February 1, 2022
    Assignee: ASML NETHERLANDS B.V.
    Inventors: Raymond Wilhelmus Louis Lafarre, Sjoerd Nicolaas Lambertus Donders, Nicolaas Ten Kate, Nina Vladimirovna Dziomkina, Yogesh Pramod Karade, Elisabeth Corinne Rodenburg
  • Patent number: 11236408
    Abstract: A method of forming a functionally designed cemented tungsten carbide can include forming a particulate matrix mixture including a primary particulate tungsten carbide and a primary particulate metal binder. A particulate enhancement mixture can be formed having a secondary particulate tungsten carbide, a secondary particulate metal binder, and a particulate grain growth inhibitor, where the enhancement mixture has a finer particle size than the matrix mixture. The particulate matrix mixture can be assembled with the particulate enhancement mixture to form a structured composite where the matrix mixture forms a continuous phase and the enhancement mixture forms at least one of a dispersed granular phase and a surface layer adjacent the continuous phase to form the structured composite. This structured composite can be sintered to form the functionally designed cemented tungsten carbide having a differential grain size with the enhancement phase having a smaller grain size than the matrix phase.
    Type: Grant
    Filed: February 10, 2021
    Date of Patent: February 1, 2022
    Assignee: University of Utah Research Foundation
    Inventors: Zhigang Zak Fang, Kyu Sup Hwang
  • Patent number: 11225731
    Abstract: Reducing the microvoid (MV) density in AlN ameliorates numerous problems related to cracking during crystal growth, etch pit generation during the polishing, reduction of the optical transparency in an AlN wafer, and, possibly, growth pit formation during epitaxial growth of AlN and/or AlGaN. This facilitates practical crystal production strategies and the formation of large, bulk AlN crystals with low defect densities—e.g., a dislocation density below 104 cm?2 and an inclusion density below 104 cm?3 and/or a MV density below 104 cm?3.
    Type: Grant
    Filed: February 8, 2017
    Date of Patent: January 18, 2022
    Assignee: CRYSTAL IS, INC.
    Inventors: Robert Bondokov, Kenneth E. Morgan, Glen A. Slack, Leo J. Schowalter
  • Patent number: 11220745
    Abstract: A coated cutting tool comprising a substrate comprising a cubic boron nitride sintered body and a coating layer formed on the substrate, wherein the coating layer comprises a Ti carbonitride layer comprising Ti(CxN1-x); an average thickness of the Ti carbonitride layer is 0.5 ?m or more and 5.0 ?m or less; in the Ti carbonitride layer, R75 is higher than R25; in the Ti carbonitride layer, a texture coefficient TC (111) of a (111) plane is 1.0 or more and 2.0 or less; and in X-ray diffraction measurement of the Ti carbonitride layer, an absolute value of a difference between a maximum value and a minimum value of 2? is 0.1° or less on the (111) plane when the measurement is performed at each of ? angles of 0°, 30°, 50° and 70°.
    Type: Grant
    Filed: August 24, 2020
    Date of Patent: January 11, 2022
    Assignee: TUNGALOY CORPORATION
    Inventor: Hirosato Nishizawa
  • Patent number: 11207736
    Abstract: Provided is a cutting tool including a base material and a coating layer provided on the base material, the coating layer including a titanium carbonitride layer provided on the base material, an intermediate layer provided on the titanium carbonitride layer in contact therewith, and an alumina layer provided on the intermediate layer in contact therewith, the intermediate layer being composed of a compound made of titanium, carbon, oxygen, and nitrogen, the intermediate layer having a thickness of more than 1 ?m, when PN1 atomic % represents an atomic ratio of the nitrogen in an interface between the intermediate layer and the alumina layer, and PN2 atomic % represents an atomic ratio of the nitrogen at a point A away from the interface by 1 ?m on a side of the intermediate layer, a ratio PN1/PN2 of the PN1 to the PN2 being more than or equal to 1.03.
    Type: Grant
    Filed: April 10, 2020
    Date of Patent: December 28, 2021
    Assignee: SUMITOMO ELECTRIC HARDMETAL CORP.
    Inventors: Susumu Okuno, Yasuki Kido, Fumiyoshi Kobayashi, Anongsack Paseuth
  • Patent number: 11208719
    Abstract: Provided is an SiC composite substrate 10 having a monocrystalline SiC layer 12 on a polycrystalline SiC substrate 11, wherein: some or all of the interface at which the polycrystalline SiC substrate 11 and the monocrystalline SiC layer 12 are in contact is an unmatched interface I12/11 that is not lattice-matched; the monocrystalline SiC layer 12 has a smooth obverse surface and has, on the side of the interface with the polycrystalline SiC substrate 11, a surface that has more pronounced depressions and projections than the obverse surface; and the close-packed plane (lattice plane 11p) of the crystals of the polycrystalline SiC in the polycrystalline SiC substrate 11 is randomly oriented with reference to the direction of a normal to the obverse surface of the monocrystalline SiC layer 12. The present invention improves the adhesion between the polycrystalline SiC substrate and the monocrystalline SiC layer.
    Type: Grant
    Filed: January 15, 2020
    Date of Patent: December 28, 2021
    Assignees: SHIN-ETSU CHEMICAL CO., LTD., CUSIC INC.
    Inventors: Yoshihiro Kubota, Shoji Akiyama, Hiroyuki Nagasawa
  • Patent number: 11203069
    Abstract: A coated cutting tool for chip forming machining of metals includes a substrate having a surface coated with a chemical vapour deposition (CVD) coating. The substrate is coated with a coating having a layer of ?-Al2O3, wherein the ?-Al2O3 layer exhibits a texture coefficient TC(0 0 12)?7.2 and wherein the ratio of I(0 0 12)/I(0 1 14)?0.8. The coating further includes a MTCVD TiCN layer located between the substrate and the ?-Al2O3 layer. The MTCVD TiCN layer exhibits a pole figure, as measured by EBSD, in a portion of the MTCVD TiCN layer parallel to the outer surface of the coating and less than 1 ?m from the outer surface of the MTCVD TiCN, wherein a pole plot based on the data of the pole figure, with a bin size of 0.25° over a tilt angle range of 0°???45° from the normal of the outer surface of the coating shows a ratio of intensity within ??15° tilt angle to the intensity within 0°???45° of ?45%.
    Type: Grant
    Filed: June 20, 2017
    Date of Patent: December 21, 2021
    Assignee: Sandvik Intellectual Property AB
    Inventors: Raluca Morjan Brenning, Jan Engqvist, Erik Lindahl, Ernesto Coronel
  • Patent number: 11193384
    Abstract: A method for preparing a seal assembly for a gas turbine engine, comprising a seal comprising a carbon material; and a seal seat positioned for rotation relative to the seal, wherein the method comprises the steps of: pre-filming a sealing surface of the seal seat with a carbon-based tribofilm; and assembling the seal seat relative to the seal in a gas turbine engine.
    Type: Grant
    Filed: September 18, 2019
    Date of Patent: December 7, 2021
    Assignee: Raytheon Technologies Corporation
    Inventors: Pantcho P. Stoyanov, Mark B. Gossner
  • Patent number: 11193217
    Abstract: A silicon-based molten composition according to an exemplary embodiment of the present invention is used in a solution growing method for forming silicon carbide single crystal, and is expressed in Formula 1 including silicon (Si), chromium (Cr), vanadium (V), and aluminum (Al). SiaCrbVcAld??[Formula 1] In Formula 1, a is equal to or greater than 0.4 and equal to or less than 0.9, b+c is equal to or greater than 0.1 and equal to or less than 0.6, c/(b+c) is equal to or greater than 0.05 and equal to or less than 0.95, and d is equal to or greater than 0.01 and equal to or less than 0.1.
    Type: Grant
    Filed: November 1, 2018
    Date of Patent: December 7, 2021
    Inventors: Junghwan Kim, Ho Rim Lee, Chan Yeup Chung, Jung Min Ko, Manshik Park
  • Patent number: 11185929
    Abstract: A coated cutting tool of a cemented carbide substrate made of WC, a metallic binder phase and a gamma phase has a well distributed gamma phase and a reduced amount of abnormal WC grains. Further, the coated cutting tool is provided with a CVD coating of TiCN and an ?-Al2O3 layer, wherein the ?-Al2O3 layer exhibits a texture coefficient TC(0 0 12)?7.2 and wherein in the ratio I(0 0 12)/I(0 1 14)?1. The coated cutting tool has an increased resistance against plastic deformation. whilst maintaining toughness.
    Type: Grant
    Filed: February 27, 2018
    Date of Patent: November 30, 2021
    Assignee: SANDVIK INTELLECTUAL PROPERTY AB
    Inventors: Leif Akesson, Anders Stenberg, Carl-Johan Maderud, Susanne Norgren, Elias Forssbeck Nyrot, Ake Ostlund, Jan Engqvist
  • Patent number: 11186525
    Abstract: A method to produce a protective surface layer having a predetermined topography on a ceramic matrix composite is described. The method includes applying a slurry layer to a surface of a fiber preform, and drying the slurry layer to form a particulate layer. A surface of the particulate layer is machined to improve surface smoothness and to form a machined surface. A ceramic tape is attached to the machined surface, and a tool comprising one or more features to be imprinted is placed on the ceramic tape, thereby forming a compression assembly. Heat and pressure are applied to the compression assembly to consolidate and bond the ceramic tape to the machined surface, while the one or more features of the tool are imprinted. Thus, a protective surface layer having a predetermined topography is formed.
    Type: Grant
    Filed: July 29, 2019
    Date of Patent: November 30, 2021
    Assignee: ROLLS-ROYCE HIGH TEMPERATURE COMPOSITES INC.
    Inventors: Sungbo Shim, Pathikumar Sellappan
  • Patent number: 11179782
    Abstract: A cutting tool including a rake face, a flank face, and a cutting edge portion, comprising a substrate and an AlTiN layer, the AlTiN layer including cubic AlxTi1-xN crystal grains, Al having an atomic ratio x of 0.7 or more and less than 0.95, the AlTiN layer including a central portion, the central portion at the rake face being occupied in area by (200) oriented crystal grains at a ratio of 80% or more, the central portion at the cutting edge portion being occupied in area by (200) oriented crystal grains at a ratio of 50% or more and less than 80%.
    Type: Grant
    Filed: February 27, 2020
    Date of Patent: November 23, 2021
    Assignee: SUMITOMO ELECTRIC HARDMETAL CORP.
    Inventors: Yasuki Kido, Anongsack Paseuth, Susumu Okuno, Shinya Imamura
  • Patent number: 11177186
    Abstract: A bonded body is formed by bonding a ceramic member formed of an Al-based ceramic and a copper member formed of copper or a copper alloy, in which, in a bonding layer formed between the ceramic member and the copper member, a crystalline active metal compound layer formed of a compound including an active metal is formed on a ceramic member side, and, the Al concentration is 0.15 at % or less in a thickness range of 0.5 ?m to 3 ?m from an interface of the active metal compound layer on a copper member side toward the copper member.
    Type: Grant
    Filed: October 25, 2018
    Date of Patent: November 16, 2021
    Assignee: MITSUBISHI MATERIALS CORPORATION
    Inventor: Nobuyuki Terasaki
  • Patent number: 11145616
    Abstract: The semiconductor device includes a semiconductor element substrate having an insulation property, and a wire for positioning the semiconductor element with respect to the semiconductor element substrate. The semiconductor element substrate includes a disposition region for disposing the semiconductor element. The wire is provided at least at a part of the periphery of the disposition region.
    Type: Grant
    Filed: June 22, 2017
    Date of Patent: October 12, 2021
    Assignee: Mitsubishi Electric Corporation
    Inventors: Takumi Shigemoto, Satoru Ishikawa, Yuji Imoto
  • Patent number: 11134868
    Abstract: The invention disclosed herein includes electrode compositions formed from processes that sputter metal in a manner that produces pillar architectures. Embodiments of the invention can be used in analyte sensors having such electrode architectures as well as methods for making and using these sensor electrodes. A number of working embodiments of the invention are shown to be useful in amperometric glucose sensors worn by diabetic individuals. However, the metal pillar structures have wide ranging applicability and should increase surface area and decrease charge density for catalyst layers or electrodes used with sensing, power generation, recording, and stimulation, in vitro and/or in the body, or outside the body.
    Type: Grant
    Filed: March 15, 2018
    Date of Patent: October 5, 2021
    Assignee: Medtronic MiniMed, Inc.
    Inventors: Akhil Srinivasan, Melissa Tsang, Robert C. Mucic, Tyler R. Wong, Rui Kong, Barry P. Pham
  • Patent number: 11139218
    Abstract: A bonded body is formed by bonding a ceramic member formed of an Al-based ceramic and a copper member formed of copper or a copper alloy, in which, in a bonding layer formed between the ceramic member and the copper member, a crystalline active metal compound layer formed of a compound including an active metal is formed on a ceramic member side, and, the Al concentration is 0.15 at % or less in a thickness range of 0.5 ?m to 3 ?m from an interface of the active metal compound layer on a copper member side toward the copper member.
    Type: Grant
    Filed: October 25, 2018
    Date of Patent: October 5, 2021
    Assignee: MITSUBISHI MATERIALS CORPORATION
    Inventor: Nobuyuki Terasaki
  • Patent number: 11131016
    Abstract: A coated substrate comprising a metal or metal alloy such as a high speed steel, TiAl based alloy or Ni based alloy or an electrically conductive ceramic material, wherein the coating comprises a hard material protective coating comprising alternating layers of different compositions, wherein a first composition of the alternating layers comprises silicon, Si, and/or a second composition of the alternating layers comprises boron, B.
    Type: Grant
    Filed: January 17, 2019
    Date of Patent: September 28, 2021
    Assignee: ROLLS-ROYCE plc
    Inventors: Arutiun Ehiasarian, Papken Hovsepian, David S Rickerby, Mark Dixon
  • Patent number: 11130191
    Abstract: A method for making an article is disclosed. According to the method, a digital model of the article is generated. The digital model is inputted into an additive manufacturing apparatus comprising an energy source. The additive manufacturing apparatus applies energy from the energy source to successively applied incremental quantities of a powder to fuse the powder to form the article corresponding to the digital model. The powder particles individually include a composite core including a first phase of a first metal and a second phase of a ceramic. A first shell including a second metal is disposed over the core.
    Type: Grant
    Filed: July 22, 2016
    Date of Patent: September 28, 2021
    Assignee: HAMILTON SUNDSTRAND CORPORATION
    Inventors: Eric Karlen, William Louis Wentland
  • Patent number: 11123802
    Abstract: A surface-coated cutting tool includes a substrate and a coating formed on a surface of the substrate, the coating including one or two or more layers, at least one of the layers being an Al-rich layer including hard particles, the hard particle having a sodium chloride type crystal structure, and including a first unit phase in a form of a plurality of lumps and a second unit phase interposed between the lumps of the first unit phase, the first unit phase being composed of a nitride or carbonitride of AlxTi1-x, the first unit phase having an atomic ratio x of Al of 0.7 or more and 0.96 or less, the second unit phase being composed of a nitride or carbonitride of AlyTi1-y, the second unit phase having an atomic ratio y of Al exceeding 0.5 and less than 0.7.
    Type: Grant
    Filed: July 7, 2017
    Date of Patent: September 21, 2021
    Assignees: Sumitomo Electric Hardmetal Corp., Sumitomo Electric Industries, Ltd.
    Inventors: Anongsack Paseuth, Yasuki Kido, Shinya Imamura, Koji Kuramochi
  • Patent number: 11117196
    Abstract: A surface-coated cutting tool includes a substrate and a coating film that coats the substrate, wherein the coating film includes a WC1-x layer composed of a compound represented by WC1-x, where x is more than or equal to 0.54 and less than or equal to 0.58, and the compound represented by WC1-x includes a hexagonal crystal structure.
    Type: Grant
    Filed: March 14, 2019
    Date of Patent: September 14, 2021
    Assignee: Sumitomo Electric Industries, Ltd.
    Inventors: Sachiko Koike, Yuki Ueda, Keiichi Tsuda
  • Patent number: 11094534
    Abstract: A surface oxidation method for a wafer, the method comprises: raising a temperature on the wafer in an oxidation atmosphere, the temperature is raised from a start temperature to a target temperature at a temperature raising rate greater than 5° C./min, the temperature is raised in a vertical furnace tube of an annealing furnace, the vertical furnace tube includes a gas intake conduit arranged on a side wall, the gas intake conduit includes a gas inlet arranged to be proximate to a bottom of the vertical furnace tube and a gas outlet arranged to be proximate to a top of the furnace tube, the wafer overlying the vertical furnace tube; and isothermally oxidizing the wafer at the target temperature in the oxidation atmosphere.
    Type: Grant
    Filed: October 31, 2019
    Date of Patent: August 17, 2021
    Assignee: Shanghai Simgui Technology Co., Ltd.
    Inventors: Huijun Xu, Yujia Zhuang, Hao Wang, Xiangyu Li
  • Patent number: 11085106
    Abstract: The present invention relates to a powder for three-dimensional printing of a cermet or a cemented carbide body. The powder has 30-70 vol % of the particles that are <10 ?m in diameter. The present invention also relates to a method of making a cermet or cemented carbide body. The method includes the steps of forming the powder, 3D printing a body using the powder together with a printing binder to form a 3D printed cermet or cemented carbide green body and subsequently sintering the green body to form a cermet or cemented carbide body.
    Type: Grant
    Filed: November 30, 2016
    Date of Patent: August 10, 2021
    Assignee: SANDVIK INTELLECTUAL PROPERTY AB
    Inventor: John De Flon
  • Patent number: 11072857
    Abstract: A vanadium silicon nitride film formed as a hard film to a base material satisfies 0.30?a/b?1.7 and 0.24?b?0.36 when a=vanadium element concentration [at %]/(vanadium element concentration [at %]+silicon element concentration [at %]+nitrogen element concentration [at %]) and b=silicon element concentration [at %]/(vanadium element concentration [at %]+silicon element concentration [at %]+nitrogen element concentration [at %]), and has a hardness of 2300 HV or more.
    Type: Grant
    Filed: December 28, 2017
    Date of Patent: July 27, 2021
    Assignee: DOWA THERMOTECH CO., LTD.
    Inventors: Satoru Habuka, Hiroyuki Matsuoka, Wataru Sakakibara
  • Patent number: 11053855
    Abstract: A process for coating a component includes applying a bond coat on a substrate of a component; applying a thermal barrier material to the bond coat; and applying a conforming reflective layer to the thermal barrier material, the conforming reflective layer conforming to porous microstructure of the ceramic coating.
    Type: Grant
    Filed: June 6, 2019
    Date of Patent: July 6, 2021
    Assignee: Raytheon Technologies Corporation
    Inventors: Brian T. Hazel, Alan C. Barron, Mary Catherine Gurak
  • Patent number: 11047026
    Abstract: A cemented carbide body is provided with improved resistance to mechanical fatigue. The cemented carbide body comprises tantalum in the binder matrix material. The tantalum content is between 1.5 weight per cent and 3.5 weight per cent of the binder content.
    Type: Grant
    Filed: August 16, 2018
    Date of Patent: June 29, 2021
    Assignee: Element Six GmbH
    Inventors: Igor Yurievich Konyashin, Bernd Heinrich Ries