Magnetic Layer Having Oxygen (i.e., Uncombined Or Oxide) Patents (Class 428/836.2)
  • Patent number: 11270727
    Abstract: In the magnetic tape cartridge, a tape has a tape thickness of 5.3 ?m or less, and a difference Winner?Wouter between a tape width Winner at a position of 50 m±1 m from a tape inner end and a tape width Wouter at a position of 50 m±1 m from a tape outer end is 4.1 ?m to 19.9 ?m as a value measured on 100th day from a date of magnetic tape cartridge manufacture, and a difference Ginner?Gouter between a servo band interval Ginner in a range of 49 m to 51 m from the tape inner end and a servo band interval Gouter in a range of 49 m to 51 m from the tape outer end is ?3.9 ?m to 0.0 ?m as a value measured on 100th day from the date of magnetic tape cartridge manufacture.
    Type: Grant
    Filed: March 20, 2020
    Date of Patent: March 8, 2022
    Assignee: FUJIFILM Corporation
    Inventors: Yuto Murata, Norihito Kasada, Yusuke Kagawa
  • Patent number: 11257518
    Abstract: Provided is a magnetic tape cartridge of a single reel type in which a magnetic tape is wound around a reel, in which the magnetic tape includes a non-magnetic support and a magnetic layer containing a ferromagnetic powder, and has a tape thickness of 5.3 ?m or less, the magnetic layer includes a plurality of servo bands, and a difference (Ginner?Gouter) between a servo band interval Ginner in a range of 49 m to 51 m from a tape inner end and a servo band interval Gouter in a range of 49 m to 51 m from a tape outer end is ?3.9 ?m to ?1.1 ?m as a value measured on 100th day from a date of magnetic tape cartridge manufacture.
    Type: Grant
    Filed: March 20, 2020
    Date of Patent: February 22, 2022
    Assignee: FUJIFILM Corporation
    Inventors: Yuto Murata, Norihito Kasada, Yusuke Kagawa
  • Patent number: 11195644
    Abstract: The disclosure describes techniques for forming nanoparticles including Fe16N2 phase. In some examples, the nanoparticles may be formed by first forming nanoparticles including iron, nitrogen, and at least one of carbon or boron. The carbon or boron may be incorporated into the nanoparticles such that the iron, nitrogen, and at least one of carbon or boron are mixed. Alternatively, the at least one of carbon or boron may be coated on a surface of a nanoparticle including iron and nitrogen. The nano particle including iron, nitrogen, and at least one of carbon or boron then may be annealed to form at least one phase domain including at least one of Fe16N2, Fe16(NB)2, Fe16(NC)2, or Fe16(NCB)2.
    Type: Grant
    Filed: March 26, 2015
    Date of Patent: December 7, 2021
    Assignees: REGENTS OF THE UNIVERSITY OF MINNESOTA, UT-BATTELLE, LLC, UNIVERSITY OF TENNESSEE RESEARCH FOUNDATION
    Inventors: Jian-Ping Wang, Yanfeng Jiang, Craig A. Bridges, Michael Brady, Orlando Rios, Roberta A. Meisner, Lawrence F. Allard, Edgar Lara-Curzio, Shihai He
  • Patent number: 10706883
    Abstract: Perpendicular magnetic recording media including a carbon grain isolation initiation layer for reducing intergranular exchange coupling in the recording layer are provided. In one such case, the media includes a substrate, a plurality of underlayers on the substrate, a grain isolation initiation layer (GIIL) on the plurality of underlayers, the GIIL including C, a metal, and an oxide, and a magnetic recording layer directly on the GIIL and including a non-ordered structure. In another case, a method of fabricating such magnetic media is provided.
    Type: Grant
    Filed: October 20, 2017
    Date of Patent: July 7, 2020
    Assignee: WESTERN DIGITAL TECHNOLOGIES, INC.
    Inventors: Sylvia Helena Florez, Cristian Papusoi, Mrugesh Desai, Prakash Mani
  • Patent number: 10127932
    Abstract: A perpendicular magnetic recording medium includes a soft magnetic underlayer, an underlayer, an intermediate layer, and a perpendicular magnetic recording layer successively stacked on a nonmagnetic substrate. The soft magnetic underlayer includes a soft magnetic layer having an amorphous structure. The underlayer includes a first underlayer, and a second underlayer provided between the first underlayer and the intermediate layer. The first underlayer is made of a TiV alloy having an amorphous structure, and the second underlayer is made of an NiW alloy including at least one element selected from a group consisting of Co, Cu, Al, Cr, and Fe. The intermediate layer is made of Ru or an Ru alloy, and wherein the soft magnetic layer, the first underlayer, and the second underlayer are stacked in this order.
    Type: Grant
    Filed: April 1, 2016
    Date of Patent: November 13, 2018
    Assignee: SHOWA DENKO K.K.
    Inventors: Chen Xu, Gohei Kurokawa
  • Patent number: 9886978
    Abstract: The present invention provides a process for production of a magnetic thin film which has insulation properties, serves as a permanent magnet, and has improved residual magnetization in comparison with prior arts, the magnetic thin film, and a magnetic material. When a magnetic thin film 3 is formed, an external magnetic field with a predetermined intensity is applied to a coating liquid containing magnetic particles containing epsilon-type iron-oxide-based compounds which have insulation properties and which serve as a permanent magnet, and the coating liquid is let cured in order to form the magnetic thin film 3. Accordingly, the magnetic particles containing the epsilon-type iron-oxide-based compounds can be fixed while being oriented regularly in a magnetization direction. This realizes the process for production of the magnetic thin film 3 which has insulation properties and which serve as a permanent magnet, the magnetic thin film 3, and a magnetic material 1.
    Type: Grant
    Filed: June 24, 2010
    Date of Patent: February 6, 2018
    Assignees: The University of Tokyo, Dowa Electronics Materials Co., Ltd.
    Inventors: Shin-Ichi Ohkoshi, Asuka Namai, Kazuyuki Takami, Koutaro Tomita
  • Patent number: 9818442
    Abstract: A method and system provide a magnetic recording media usable in a magnetic storage device. The magnetic recording media includes a substrate, at least one intermediate layer and a magnetic recording stack for storing magnetic data. The intermediate layer(s) include a majority phase having a first diffusion constant and a secondary phase having a second diffusion constant greater than the first diffusion constant. The magnetic recording stack residing on the intermediate layer such that the at least one intermediate layer is between the substrate and the magnetic recording stack.
    Type: Grant
    Filed: December 1, 2014
    Date of Patent: November 14, 2017
    Assignee: WD MEDIA, LLC
    Inventors: Kumar Srinivasan, Tuqiang Li, Mrugesh Desai
  • Patent number: 9767836
    Abstract: A method for making an ordered magnetic alloy includes (a) providing a thermally conductive base having opposite first and second surfaces; (b) forming a thermal barrier layer on the first surface of the thermally conductive base; (c) forming a disordered magnetic alloy layer on the thermal barrier layer, the disordered magnetic alloy layer being made from a disordered alloy which contains a first metal selected from Fe, Co, and Ni, and a second metal selected from Pt and Pd; and (d) after step (c), applying a transient heat to the thermally conductive base to cause rapid thermal expansion of the thermally conductive base, which, in turn, causes generation of an in-plane tensile stress in the disordered magnetic alloy layer.
    Type: Grant
    Filed: October 25, 2013
    Date of Patent: September 19, 2017
    Assignee: NATIONAL TSING HUA UNIVERSITY
    Inventors: Chih-Huang Lai, Liang-Wei Wang, Yun-Chung Wu, Wen-Chieh Shih
  • Patent number: 9728218
    Abstract: A magnetic recording medium for heat-assisted magnetic recording is provided. A magnetic recording layer includes upper and lower magnetic recording layers. The lower magnetic recording layer has a lower granular structure including lower magnetic crystal grains, and a lower non-magnetic portion, that surrounds the lower magnetic crystal grains, mainly composed of carbon. The upper magnetic recording layer has an upper granular structure including upper magnetic crystal grains, and an upper non-magnetic portion, that surrounds the upper magnetic crystal grains, formed from a material selected from the group consisting of silicon nitride, titanium oxide and titanium nitride.
    Type: Grant
    Filed: September 12, 2014
    Date of Patent: August 8, 2017
    Assignee: FUJI ELECTRIC CO., LTD.
    Inventor: Shinji Uchida
  • Patent number: 9272515
    Abstract: A liquid ejecting head includes a passage-forming substrate provided with a pressure-generating chamber communicating with a nozzle orifice for ejecting a liquid and includes a piezoelectric element including a diaphragm disposed on the passage-forming substrate, a first electrode disposed on the diaphragm, a piezoelectric layer disposed on the first electrode, and second electrode disposed on the piezoelectric layer. The diaphragm includes a metal oxide layer of a metal oxide formed by a gas-phase method and a zirconium oxide layer of zirconium oxide formed by a liquid-phase method.
    Type: Grant
    Filed: February 6, 2014
    Date of Patent: March 1, 2016
    Assignee: Seiko Epson Corporation
    Inventors: Koji Ohashi, Shiro Yazaki, Eiju Hirai
  • Publication number: 20150111066
    Abstract: A magnetic recording medium includes a nonmagnetic support body, and a magnetic layer containing magnetic powder, in which the magnetic powder contains ?-Fe2O3 crystal (including a case of substituting a portion of Fe site with a metal element M), a product of residual magnetization and a thickness of the magnetic layer is from 0.5 mA to 6.0 mA, and a squareness ratio which is measured in a longitudinal direction of the magnetic layer is 0.3 or less.
    Type: Application
    Filed: October 15, 2014
    Publication date: April 23, 2015
    Applicant: Sony Corporation
    Inventors: Masaru Terakawa, Yoichi Kanemaki, Minoru Yamaga
  • Publication number: 20140342188
    Abstract: An apparatus includes a substrate and a magnetic layer coupled to the substrate. The magnetic layer includes an alloy that has magnetic hardness that is a function of the degree of chemical ordering of the alloy. The degree of chemical ordering of the alloy in a first portion of the magnetic layer is greater than the degree of chemical ordering of the alloy in a second portion of the magnetic layer, and the first portion of the magnetic layer is closer to the substrate than the second portion of the magnetic layer.
    Type: Application
    Filed: August 5, 2014
    Publication date: November 20, 2014
    Inventors: Yingguo Peng, Xiaowei Wu, Ganping Ju, Bin Lu
  • Patent number: 8877359
    Abstract: Provided are a magnetic disk comprising a granular magnetic recording layer which causes less noise even with a recording capacity thereof of 250 G or more bits per square inch; and a method for manufacturing the same. The magnetic disk according to the present invention comprises: a granular magnetic recording layer (20) which is formed on a disk substrate 10 directly or via an intermediate layer and which has non-magnetic regions between granular columnar particles; and an auxiliary recording layer (22) which is formed on the granular magnetic recording layer 20 and which causes exchange interaction among the granular columnar particles, wherein the auxiliary recording layer (22) contains 0.1 to 3 moles of oxygen.
    Type: Grant
    Filed: December 7, 2009
    Date of Patent: November 4, 2014
    Assignee: WD Media (Singapore) Pte. Ltd.
    Inventors: Chiyo Saito, Tokichiro Sato, Takenori Kajiwara
  • Publication number: 20140147700
    Abstract: A method and apparatus for forming magnetic media substrates is provided. A patterned resist layer is formed on a substrate having a magnetically susceptible layer. A conformal protective layer is formed over the patterned resist layer to prevent degradation of the pattern during subsequent processing. The substrate is subjected to an energy treatment wherein energetic species penetrate portions of the patterned resist and conformal protective layer according to the pattern formed in the patterned resist, impacting the magnetically susceptible layer and modifying a magnetic property thereof. The patterned resist and conformal protective layers are then removed, leaving a magnetic substrate having a pattern of magnetic properties with a topography that is substantially unchanged.
    Type: Application
    Filed: January 31, 2014
    Publication date: May 29, 2014
    Applicant: Applied Materials, Inc.
    Inventors: Christopher Dennis BENCHER, Roman GOUK, Steven VERHAVERBEKE, Li-Qun XIA, Yong-Won LEE, Matthew D. SCOTNEY-CASTLE, Martin A. HILKENE, Peter I. PORSHNEV
  • Patent number: 8722212
    Abstract: A magnetic recording medium includes a non-magnetic granular layer, and a recording layer provided on the non-magnetic granular layer, wherein the recording layer includes a first granular magnetic layer provided on the non-magnetic granular layer, and a second granular magnetic layer provided on the first granular magnetic layer, and a non-magnetic material magnetically separating metal grains of the non-magnetic granular layer is different from a non-magnetic material magnetically separating magnetic grains of the first granular magnetic layer.
    Type: Grant
    Filed: March 2, 2010
    Date of Patent: May 13, 2014
    Assignee: Showa Denko K.K.
    Inventors: Ryo Kurita, Satoshi Igarashi, Isatake Kaitsu, Akira Kikuchi
  • Patent number: 8722214
    Abstract: Magnetic layers are described that include the use of magnetic grains and non-magnetic grain boundaries with hybrid additives. Hybrid additives include the use of at least two different additives in the composition of the grain boundaries of a magnetic layer in magnetic recording media. The use of hybrid additives in the grain boundaries results in improved recording media. Methods for forming magnetic layers and magnetic recording media with the hybrid additive grain boundaries are also described.
    Type: Grant
    Filed: September 14, 2012
    Date of Patent: May 13, 2014
    Assignee: Seagate Technology LLC
    Inventors: Yingguo Peng, Ganping Ju
  • Patent number: 8685547
    Abstract: Aspects are directed to recording media with enhanced magnetic properties for improved writability. Examples can be included or related to methods, systems and components that allow for improved writability while reducing defects so as to obtain uniform magnetic properties such as uniformly high anisotropy and narrow switching field distribution. Some examples include a recording medium with an exchange tuning layer inserted between the hard layer and the soft, semi-soft or thin semi-hard layer so as to maximize the writability improvement of the media. Preferably, the exchange tuning layer is granular and reduces or optimizes the vertical coupling between the hard layer and the soft, semi-soft or semi-hard layer of a magnetic recording or storing device.
    Type: Grant
    Filed: February 19, 2009
    Date of Patent: April 1, 2014
    Assignee: Seagate Technology LLC
    Inventors: Bo Bian, Shoutao Wang, Weilu Xu, Abebe Hailu, Miaogen Lu, Charles C. Chen, Thomas Patrick Nolan, Alexander Yulievich Dobin
  • Patent number: 8679654
    Abstract: Surface flatness of magnetic recording medium to which a magnetic recording layer made of L10 FePt magnetic alloy thin film, with distance between a magnetic head and a magnetic recording medium sufficiently reduced. The magnetic recording layer includes: magnetic layers containing a magnetic alloy including Fe and Pt as principal materials; and one non-magnetic material selected from carbon, oxide and nitride. The first magnetic layer disposed closer to a substrate has a granular structure in which magnetic alloy grains including FePt alloy as the principal material are separated from grain boundaries including the non-magnetic material as the principal material. The second magnetic layer disposed closer to the surface than the first magnetic layer is fabricated so as to have a homogeneous structure in which an FePt alloy and the non-magnetic material are mixed in a state finer than diameters of the FePt magnetic alloy grains in the first magnetic layer.
    Type: Grant
    Filed: February 13, 2012
    Date of Patent: March 25, 2014
    Assignee: Hitachi, Ltd.
    Inventors: Hiroaki Nemoto, Ikuko Takekuma, Kimio Nakamura, Junichi Sayama
  • Patent number: 8603650
    Abstract: A magnetic disk 10 for use in perpendicular magnetic recording has at least a magnetic recording layer on a substrate 1. The magnetic recording layer is composed of a ferromagnetic layer 5 of a granular structure containing silicon (Si) or an oxide of silicon (Si) between crystal grains containing cobalt (Co), a stacked layer 7 having a first layer containing cobalt (Co) or a Co alloy and a second layer containing palladium (Pd) or platinum (Pt), and a spacer layer 6 interposed between the ferromagnetic layer 5 and the stacked layer 7. After forming the ferromagnetic layer 5 on the substrate 1 by sputtering in an argon gas atmosphere, the stacked layer 7 is formed by sputtering in the argon gas atmosphere at a gas pressure lower than that used when forming the ferromagnetic layer 5.
    Type: Grant
    Filed: June 29, 2005
    Date of Patent: December 10, 2013
    Assignee: WD Media (Singapore) Pte. Ltd.
    Inventors: Yoshiaki Sonobe, Teiichiro Umezawa, Chikara Takasu
  • Patent number: 8603649
    Abstract: A perpendicular magnetic recording medium includes a magnetic recording layer 22 having a granular structure composed of crystal grains containing cobalt (Co) and grown in a columnar shape and a grain boundary portion comprising a nonmagnetic substance and formed between the crystal grains, and a continuous layer 24 of a thin film magnetically continuous in a film plane direction. The continuous layer 24 includes a plurality of layers 24a and 24b containing cobalt, chromium (Cr), and platinum (Pt). Among the layers, the layer 24a nearer to the magnetic recording layer has a greater chromium content.
    Type: Grant
    Filed: October 6, 2008
    Date of Patent: December 10, 2013
    Assignee: WD Media (Singapore) Pte. Ltd.
    Inventor: Takahiro Onoue
  • Patent number: 8592061
    Abstract: In order to provide a magnetic recording medium having excellent electromagnetic conversion characteristics, a magnetic recording medium (10) is provided with a substrate (12), and a magnetic recording layer (20) formed on the substrate (12). The magnetic recording layer (20) is provided with a granular layer (32), i.e., a magnetic layer, including magnetic grains and a nonmagnetic material surrounding the magnetic grains in a section parallel to the main surface of the substrate. The ratio of the long diameter to the short diameter of each magnetic grain contained in the granular layer (32) is calculated in the section. In the histogram of such ratio, a half width at half maximum of the histogram is 0.6 or less and the variance of grain diameters of the magnetic grains in the section is 20% or less of the average grain diameter of the magnetic grains.
    Type: Grant
    Filed: September 26, 2007
    Date of Patent: November 26, 2013
    Assignee: WD Media (Singapore) Pte. Ltd.
    Inventors: Takahiro Onoue, Akira Shimada
  • Patent number: 8507116
    Abstract: According to one embodiment, a magnetic recording medium includes a substrate, a soft magnetic layer, an underlayer, a magnetic recording layer, and a protective layer, wherein the magnetic recording layer is provided with a pattern including recording portions and non-recording portions, the non-recording portions have a composition that is equal to a composition obtained by demagnetizing the recording portions, the non-recording portions contain at least one metal element selected from the group consisting of vanadium and zirconium and at least one element selected from the group consisting of nitrogen, carbon, boron and oxygen, and the at least one element selected from the group consisting of nitrogen, carbon, boron and oxygen is contained in the non-recording portions at a higher content than the content of the at least one element selected from the group consisting of nitrogen, carbon, boron and oxygen in the recording portions.
    Type: Grant
    Filed: July 1, 2011
    Date of Patent: August 13, 2013
    Assignee: Kabushiki Kaisha Toshiba
    Inventors: Takeshi Iwasaki, Kaori Kimura, Yoshiyuki Kamata, Masatoshi Sakurai
  • Patent number: 8507114
    Abstract: A magnetic stack includes multiple granular layers, at least one of the multiple granular layers is a magnetic layer that includes exchange coupled magnetic grains separated by a segregant having Ms greater than 100 emu/cc. Each of the multiple granular layers have anisotropic thermal conductivity.
    Type: Grant
    Filed: June 30, 2011
    Date of Patent: August 13, 2013
    Assignee: Seagate Technology LLC
    Inventors: Yingguo Peng, Jan-Ulrich Thiele, Ganping Ju, Thomas Patrick Nolan, Yinfeng Ding, Alexander Qihong Wu
  • Publication number: 20130170075
    Abstract: A magnetic media has a substrate with an underlayer and a seed layer on the underlayer. The seed layer has a non-continuous metallic layer with a cubed crystalline lattice that is 001 textured, and has a lattice mismatch within 15% of a crystalline lattice structure of FePt with a metallic additive. This structure defines nucleation sites with an established epitaxial interface.
    Type: Application
    Filed: December 28, 2011
    Publication date: July 4, 2013
    Applicant: Hitachi Global Storage Technologies Netherlands B.V.
    Inventors: Qing Dai, Oleksandr Mosendz, Simone Pisana, Dieter K. Weller
  • Patent number: 8475949
    Abstract: A magnetic recording medium is presented that includes protruded magnetic patterns formed on a substrate, and a nonmagnetic material filled in recesses between the magnetic patterns in which an oxygen concentration thereof is higher at a surface side than at a substrate side. The nonmagnetic material is at least one selected from the group consisting of Si, SiC, SiC—C, SiOC, SiON, Si3N4, Al, AlxOy, Ti and TiOx.
    Type: Grant
    Filed: September 20, 2011
    Date of Patent: July 2, 2013
    Assignee: Kabusihki Kaisha Toshiba
    Inventors: Kaori Kimura, Yoshiyuki Kamata, Satoshi Shirotori, Masatoshi Sakurai
  • Patent number: 8440332
    Abstract: Embodiments of the present invention provide a perpendicular magnetic recording medium that reduces the noise of granular recording layers, obtains sufficient overwrite characteristic that suppresses an increase in the magnetic cluster size, and allows high-density recording. According to one embodiment, a perpendicular magnetic recording medium comprising substrate having thereon at least soft magnetic layer, nonmagnetic intermediate layer, a perpendicular recording layer and protective layer formed in that order. The perpendicular recording layer consists of three or more layers of first recording layer, a second recording layer, and a third recording layer from the side nearer to the substrate. The first recording layer and the second recording layer have a granular structure comprising a grain boundary of an oxide surrounding ferromagnetic crystal grains containing Co and Pt, and the third recording layer has a non-granular structure mainly comprising Co and not containing an oxide.
    Type: Grant
    Filed: April 8, 2009
    Date of Patent: May 14, 2013
    Assignee: HGST Netherlands B.V.
    Inventors: Ichiro Tamai, Kiwamu Tanahashi
  • Patent number: 8431257
    Abstract: A perpendicular magnetic recording medium is used for information recording of a perpendicular magnetic recording type. The perpendicular magnetic recording medium includes a substrate, a soft magnetic layer, an underlayer, and a magnetic layer having a multilayered structure including a plurality of magnetic layers. The soft magnetic layer, the underlayer, and the magnetic layer are formed on the substrate. At least one of the magnetic layers includes CoPt magnetic grains containing oxide. The oxide includes at least one material selected from the group consisting of SiO2, TiO2, Cr2O3, Ta2O5, WO3, CoO, and Co3O4.
    Type: Grant
    Filed: March 29, 2010
    Date of Patent: April 30, 2013
    Assignee: WD Media (Singapore) PTE. Ltd.
    Inventors: Kong Kim, Hi Shin, Tomoko Seki, Satoshi Ishii
  • Patent number: 8404370
    Abstract: A perpendicular magnetic recording medium 100 has, over a substrate, at least a magnetic recording layer 122 with a granular structure in which nonmagnetic grain boundaries are formed between magnetic grains continuously grown into a columnar shape. The magnetic grains of the magnetic recording layer 122 contain Co, Cr, and Pt. The magnetic recording layer 122 contains at least one oxide selected from a group A including SiO2, TiO2, and Cr2O3, at least one oxide selected from a group B consisting of oxides each having a larger Gibbs free energy ?G than the group A, and a reducing agent adapted to reduce the oxides of the group B.
    Type: Grant
    Filed: March 31, 2010
    Date of Patent: March 26, 2013
    Assignee: WD Media (Singapore) Pte. Ltd.
    Inventors: Tokichiro Sato, Takahiro Onoue, Takenori Kajiwara
  • Publication number: 20130071695
    Abstract: Magnetic layers are described that include the use of magnetic grains and non-magnetic grain boundaries with hybrid additives. Hybrid additives include the use of at least two different additives in the composition of the grain boundaries of a magnetic layer in magnetic recording media. The use of hybrid additives in the grain boundaries results in improved recording media. Methods for forming magnetic layers and magnetic recording media with the hybrid additive grain boundaries are also described.
    Type: Application
    Filed: September 14, 2012
    Publication date: March 21, 2013
    Applicant: SEAGATE TECHNOLOGY LLC
    Inventors: Yingguo Peng, Ganping Ju
  • Publication number: 20130034748
    Abstract: The present invention provides: a method of producing, at low temperature, a magnetic recording medium comprising an L10FePt thin film which is highly (001)-oriented and highly L10-ordered; and a magnetic recording medium comprising an L10FePt thin film that can be obtained by this method. In the production method of a magnetic recording medium (10), a thin film formation step S1 of forming a thin film 2 containing an FePt alloy and an oxide of metal having a melting point of 100° C. or more and 500° C. or less is carried out; an annealing step S2 of annealing the thin film 2 to a predetermined temperature is carried out; thereby a magnetic recording layer 2? containing the FePt alloy having a L10-ordered structure and the oxide of metal is formed. The magnetic recording medium can be obtained by this production method.
    Type: Application
    Filed: April 21, 2011
    Publication date: February 7, 2013
    Applicant: AKITA UNIVERSITY
    Inventors: Shunji Ishio, Shun Shibata
  • Patent number: 8367229
    Abstract: The present invention relates to a perpendicular magnetic recording medium including a nonmagnetic substrate, and at least a soft magnetic layer (SUL), an alignment control layer, a magnetic recording layer and a protective layer formed on the nonmagnetic substrate, wherein the magnetic recording layer is constituted of two or more layers and includes a first magnetic recording layer and a second magnetic recording layer from the nonmagnetic substrate side and, regarding magnetocrystalline anisotropic energy Ku of each magnetic recording layer, the first magnetic recording layer has 4×106 erg/cc or higher and the second magnetic recording layer has 2×106 erg/cc or lower, wherein the first magnetic recording layer is constituted of CoCrPtRu magnetic alloy crystal grains and grain boundaries made of an oxide and the area of grain boundaries is 30% or more based on the entire area in a planar TEM observation of the first magnetic recording layer.
    Type: Grant
    Filed: September 30, 2008
    Date of Patent: February 5, 2013
    Assignee: Showa Denko K.K.
    Inventor: Yuzo Sasaki
  • Patent number: 8268462
    Abstract: Magnetic layers are described that include the use of magnetic grains and non-magnetic grain boundaries with hybrid additives. Hybrid additives include the use of at least two different additives in the composition of the grain boundaries of a magnetic layer in magnetic recording media. The use of hybrid additives in the grain boundaries results in improved recording media. Methods for forming magnetic layers and magnetic recording media with the hybrid additive grain boundaries are also described.
    Type: Grant
    Filed: December 22, 2008
    Date of Patent: September 18, 2012
    Assignee: Seagate Technology LLC
    Inventors: Yingguo Peng, Ganping Ju
  • Patent number: 8168309
    Abstract: Perpendicular recording media with sublayers of dual oxide dopant magnetic materials are disclosed. The magnetic layer may comprise multiple sublayers of magnetic materials. In each sublayer, dual oxide dopants are incorporated. The compositions of the sublayers can be the same or different depending on the application. The magnetic layer may be deposited using a target comprising a mixture of CoPtCrB and dual oxides as dopants. The layer deposited with such targets can be the entire magnetic layer or a sublayer.
    Type: Grant
    Filed: August 13, 2009
    Date of Patent: May 1, 2012
    Assignee: Hitachi Global Storage Technologies Netherlands B.V.
    Inventors: Gunn Choe, Mohammad T. Mirzamaani, Kai Tang, Jinliu Wang
  • Patent number: 8124255
    Abstract: A highly reliable magnetic recording medium is provided which has a recording layer formed in a concavo-convex pattern and wherein the recording layer is unlikely to cause a change in magnetic properties. The magnetic recording medium includes a substrate, a recording layer formed in a predetermined concavo-convex pattern over the substrate, convex portions of the concavo-convex pattern serving as recording elements; and a filler portion filling a concave portion between the recording elements. The filler portion comprises a metal-based main filler material and oxygen. Oxygen is unevenly distributed in the filler portion so that the ratio of the number of oxygen atoms to the total of the number of atoms of the main filler material and the number of oxygen atoms is greater in an upper surface portion of the filler portion than in a lower portion of the filler portion.
    Type: Grant
    Filed: June 3, 2009
    Date of Patent: February 28, 2012
    Assignee: TDK Corporation
    Inventors: Shuichi Okawa, Kazuhiro Hattori, Narutoshi Fukuzawa, Takahiro Suwa
  • Patent number: 8119263
    Abstract: A magnetic recording medium having a substrate, a first magnetic layer and a second magnetic layer, in this order, wherein an exchange coupling in the first magnetic layer is lower than an exchange coupling in the second magnetic layer, and the first and second magnetic layers are in a film stack so that magnetic grains in the first magnetic layer are exchange coupled by a pathway through the second magnetic layer is disclosed. A method of manufacturing a magnetic recording medium by obtaining a substrate, depositing a first magnetic layer at a first sputter gas pressure and depositing a second magnetic layer at a second sputter gas pressure, in this order, wherein the first sputter gas pressure is higher than the second sputter gas pressure, and an exchange coupling in the first magnetic layer is lower than an exchange coupling in the second magnetic layer is also disclosed.
    Type: Grant
    Filed: September 22, 2005
    Date of Patent: February 21, 2012
    Assignee: Seagate Technology LLC
    Inventors: Thomas Patrick Nolan, Samuel D. Harkness, IV
  • Patent number: 8119264
    Abstract: A perpendicular magnetic recording disk has a granular cobalt alloy recording layer (RL) containing an additive oxide or oxides, an intermediate layer (IL) as an exchange-break layer on the “soft” magnetic underlayer (SUL), and an ultrathin nucleation film (NF) between the IL and the RL. In the method of making the disk, the IL is deposited at a relatively low sputtering pressure, to thereby reduce the roughness of the RL and overcoat (OC), while the NF and RL are deposited at substantially higher sputtering pressures. The resulting disk has good recording properties and improved corrosion resistance over a comparable disk made with an IL deposited at high sputtering pressure and without the NF. The NF may be a discontinuous film with an average thickness of less than about 1 nm.
    Type: Grant
    Filed: March 24, 2010
    Date of Patent: February 21, 2012
    Assignee: Hitachi Global Storage Technologies Netherlands B.V.
    Inventor: Ernesto E. Marinero
  • Patent number: 8039133
    Abstract: A magnetic recording medium, and method of manufacturing the same, is provided with excellent recording performance by employing a granular magnetic layer having a specified composition. A magnetic recording medium according to the present invention comprises a nonmagnetic underlayer, a granular magnetic layer, a protective film, and a liquid lubrication layer sequentially laminated on a nonmagnetic substrate. The granular magnetic layer consists of ferromagnetic crystal grains containing cobalt and nonmagnetic grain boundary region surrounding the ferromagnetic crystal grains. The ferromagnetic crystal grains contain platinum in the range of 15 at % to 17 at %.
    Type: Grant
    Filed: April 26, 2005
    Date of Patent: October 18, 2011
    Assignee: Fuji Electric Device Technology Co., Ltd.
    Inventors: Miyabi Nakamura, Takahiro Shimizu, Hiroyuki Uwazumi, Naoki Takizawa, Tadaaki Oikawa
  • Patent number: 8034470
    Abstract: A perpendicular magnetic recording medium is disclosed in which a soft magnetic layer used as a low Ku layer can be stably produced with high performance. Thermal stabilization of magnetization, ease of writing by a magnetic head, and SNR also are improved. A method of manufacturing the medium is disclosed. The perpendicular magnetic recording medium includes at least a nonmagnetic underlayer, a magnetic recording layer, and a protective layer formed in this order on a nonmagnetic substrate. The magnetic recording layer includes a low Ku layer having a relatively small perpendicular magnetic anisotropy constant (Ku value), and a high Ku layer in which the Ku value is relatively large, and the low Ku layer includes a soft magnetic thin film including an iron group element-based microcrystal structure, in which a nitrogen element is added to a ferromagnetic material mainly containing one of metals of Co, Ni and Fe or an alloy of the metal.
    Type: Grant
    Filed: March 14, 2008
    Date of Patent: October 11, 2011
    Assignee: Fuji Electric Co., Ltd.
    Inventors: Tadaaki Oikawa, Hiroyuki Uwazumi
  • Patent number: 8029924
    Abstract: An apparatus includes a first seedlayer including a hexagonal close-packed alloy with a sigma phase addition, and an active layer including a plurality of quantum dots on the first seedlayer. The apparatus can further include a substrate, an adhesion layer on the substrate, and a wetting layer on the adhesion layer, wherein the first seedlayer is on the wetting layer.
    Type: Grant
    Filed: August 21, 2008
    Date of Patent: October 4, 2011
    Assignee: Seagate Technology LLC
    Inventors: Samuel Dacke Harkness, IV, Hans Jürgen Richter
  • Patent number: 8021771
    Abstract: A thin film structure including a plurality of grains of a first magnetic material having a first Curie temperature embedded in a matrix of a second material having a second Curie temperature, wherein the second Curie temperature is lower than the first Curie temperature and the second material comprises one or more of an oxide, a sulfide, a nitride, and a boride.
    Type: Grant
    Filed: January 8, 2010
    Date of Patent: September 20, 2011
    Assignee: Seagate Technology LLC
    Inventors: Dieter Klaus Weller, Edward Charles Gage, Ganping Ju, Bin Lu
  • Patent number: 7998607
    Abstract: A perpendicular recording magnetic media with a partially-oxidized cap layer combines a second oxide layer with a first cap layer to form the singular, partially-oxidized cap. The oxidized portion and the non-oxidized portion of the partially-oxidized layer are sputtered from a same target and have a same composition of metallic elements. The Ms of the oxidized portion is about twice as high as the non-oxidized portion. The oxidized portion has a thickness in the range of about 5 to 25 angstroms. The layer composition may comprise CoPtCrBTa, with a Cr at % of about 18-24%, Pt at about 13-20%, B at about 4-10%, and Ta at about 0-2%.
    Type: Grant
    Filed: July 31, 2009
    Date of Patent: August 16, 2011
    Assignee: Hitachi Global Storage Technologies Netherlands, B.V.
    Inventor: Yoshihiro Ikeda
  • Patent number: 7993765
    Abstract: In a perpendicular magnetic recording medium which includes a substrate (1) of a nonmagnetic material, first and second nonmagnetic underlayers (4 and 5) formed on the substrate, and a perpendicular magnetic recording layer (6) formed on the first and the second nonmagnetic underlayers, the first nonmagnetic underlayer is made of an amorphous nonmagnetic metal material containing a metal element which forms a face-centered cubic (fcc) crystal structure by a simple substance. The second nonmagnetic underlayer is formed on the first nonmagnetic underlayer in contact with the first nonmagnetic underlayer and made of a nonmagnetic material containing a hexagonal close packed structure. The perpendicular magnetic recording layer is formed on the second nonmagnetic underlayer in contact with the second nonmagnetic layer.
    Type: Grant
    Filed: July 26, 2004
    Date of Patent: August 9, 2011
    Assignee: WD Media (Singapore) Pte. Ltd.
    Inventors: Kong Kim, Kinobu Osakabe, Junichi Horikawa
  • Patent number: 7976965
    Abstract: A magnetic recording medium comprises a nonmagnetic substrate on which is disposed at least a vertical magnetic layer. The vertical magnetic layer comprises at least three layers including a lower layer, an intermediate layer and an upper layer from the substrate side. The lower, intermediate and upper magnetic layers are bound by ferro-coupling and are constituted of magnetic particles which are columnar crystals extending continuously from the lower layer to the upper layer. A nonmagnetic layer is between the lower and intermediate magnetic layers or between the intermediate and upper magnetic layers. The upper layer has a magnetic anisotropic constant (Ku) from 0.8×106 to 4×106 (erg/cc), the intermediate layer has a magnetic anisotropic constant (Ku) from 2×106 to 7×106 (erg/cc) and the lower layer has a magnetic anisotropic constant (Ku) from 1×106 to 4×106 (erg/cc).
    Type: Grant
    Filed: August 20, 2009
    Date of Patent: July 12, 2011
    Assignee: Showa Denko K.K.
    Inventors: Kenji Shimizu, Junichi Kishimoto
  • Patent number: 7923134
    Abstract: Embodiments of the present invention help to provide a discrete track medium for realizing a high track density in a low price by adopting a configuration, in which filling of a non-magnetic material into a guard band portion and smoothing processing of a medium surface are not required. According to one embodiment, a perpendicular magnetic recording medium, on the non-magnetic substrate, includes at least: a soft magnetic underlayer; a first recording layer including a crystal grain having a magnetic property and a non-magnetic grain boundary having an oxide, as a main component, surrounding the crystal grain; a second recording layer containing a ferromagnetic metal as a main component and not containing an oxide; and at least one non-magnetic layer provided between the first recording layer and the second recording layer.
    Type: Grant
    Filed: September 26, 2008
    Date of Patent: April 12, 2011
    Assignee: Hitachi Global Storage Technologies Netherlands BV
    Inventors: Takayuki Ichihara, Masayoshi Shimizu
  • Patent number: 7901803
    Abstract: A perpendicular magnetic recording medium includes: a substrate; at least one underlayer formed above the substrate; and a perpendicular magnetic recording layer formed above the at least one underlayer, an easy magnetization axis of the perpendicular magnetic recording layer being oriented perpendicular to the substrate, the perpendicular magnetic recording layer including magnetic crystal particles and grain boundaries surrounding the magnetic crystal particles, wherein the grain boundaries contain an oxide of silicon and at least one element selected from the group consisting of Li, Na, K, Rb, Cs, Ca, Sr, and Ba, and the ratio of a total amount of substance of Si, Li, Na, K, Rb, Cs, Ca, Sr, and Ba in the perpendicular magnetic recording layer is no less than 1 mol % and no more than 20 mol %.
    Type: Grant
    Filed: October 5, 2004
    Date of Patent: March 8, 2011
    Assignees: Showa Denko K.K., Kabushiki Kaisha Toshiba
    Inventors: Tomoyuki Maeda, Soichi Oikawa, Takeshi Iwasaki, Futoshi Nakamura, Hiroshi Sakai, Kenji Shimizu, Akira Sakawaki
  • Patent number: 7892663
    Abstract: Embodiments of the present invention provide a perpendicular magnetic recording media having excellent resolution, signal to noise ratio (S/N), and a small adjacent track erasure. According to one embodiment, underlayers for controlling the orientation and segregation of a magnetic layer, a magnetic layer including an oxide and an alloy of magnetic materials mainly composed of Co, Cr, and Pt, and a ferromagnetic-metal layer which does not contain oxygen, are formed over a substrate. The magnetic layer has at least two layers including ferromagnetic grains and oxides, a first magnetic layer, which is the part of the magnetic layer closer to the substrate, has grain boundaries mainly composed of Cr oxide and at least one oxide selected from Si, Ti, Nb, and Ta, and grain boundaries of a second magnetic layer at the ferromagnetic-metal layer side includes at least one oxide selected from Si, Ti, Nb, and Ta in which Cr oxide is less than the first magnetic layer.
    Type: Grant
    Filed: May 30, 2008
    Date of Patent: February 22, 2011
    Assignee: Hitachi Global Storage Technologies Netherlands B.V.
    Inventors: Hiroyuki Nakagawa, Ryoko Araki, Naoto Ito, Takayuki Ichihara
  • Patent number: 7879469
    Abstract: A ferrite magnet powder is represented by the composition formula AFe2+a(1-x)MaxFe3+bO27, wherein A represents at least one element selected from the group consisting of Sr, Ba, and Pb; and M represents at least one element selected from the group consisting of Zn, Co, Mn, and Ni, and wherein 0.05?x?0.80, 1.5?a?2.2, and 12?b?17. A high saturation magnetization 4?Is can be achieved by the partial substitution of the Fe2+ site of a W-type ferrite with an element M such as Zn within a certain range.
    Type: Grant
    Filed: February 5, 2004
    Date of Patent: February 1, 2011
    Assignee: TDK Corporation
    Inventors: Yoshihiko Minachi, Noboru Ito
  • Patent number: 7879470
    Abstract: A method for improving magnetic grain segregation in perpendicular recording media includes providing a substrate comprising a rigid support structure, depositing a soft underlayer on top of the substrate depositing an intermediate layer on top of the soft underlayer, providing a plurality of prospective segregants, determining the surface energies and the heat of formation of the prospective segregants and selecting the prospective segregant with a low surface energy and a high heat of formation. The method also includes providing at least one layer with surface energies progressively increasing to minimize the difference between the surface energy of a carbon overcoat and the segregant.
    Type: Grant
    Filed: November 15, 2007
    Date of Patent: February 1, 2011
    Assignee: Hitachi Global Storage Technologies Netherlands B.V.
    Inventors: Qing Dai, Hoa V. Do, Bruno Marchon, Kentaro Takano
  • Publication number: 20110020669
    Abstract: A magnetic recording medium having excellent stability of recorded magnetic signals and capable of recording magnetic signals by a thermally assisted magnetic recording system in which a magnetic recording layer of the magnetic recording medium contains ferromagnetic crystal grains of a Co—Ni—Pt alloy with a Pt content of 44 at % or more and 55 at % or less and with an atom content ratio: Ni/(Co+Ni) of 0.64 or more and 0.8 or less. The magnetic recording medium has extremely excellent stability of recorded magnetic signals since the Co—Ni—Pt alloy constituting the magnetic recording layer has an extremely high anisotropy field at a normal temperature. Further, the magnetic recording medium can perform signal recording based on the thermally assisted magnetic recording system since the Co—Ni—Pt alloy constituting the magnetic recording layer has a Curie point within an appropriate temperature range.
    Type: Application
    Filed: July 21, 2010
    Publication date: January 27, 2011
    Inventors: Junichi SAYAMA, Hiroaki Nemoto, Hiroshi Ide, Hiroyasu Kataoka, Nobuyukl Takahashi, Takehito Shimatsu, Osamu Kitakami, Satoshi Okamoto, Hajime Aoi
  • Patent number: 7875373
    Abstract: Embodiments in accordance with the present invention help to obtain a perpendicular magnetic recording medium having a granular structure, excellent recording/reproducing properties, and excellent durability. According to one embodiment, a recording layer includes a layer which has crystal grains mainly composed of cobalt and crystal grain boundaries mainly composed of the oxide; the oxygen content of the recoding layer is changed in the film thickness direction; the oxygen content in the area in the vicinity of the interface between the recording layer and the intermediate layer is made lower than the oxygen content in the area in the vicinity of the center of the recording layer; and the oxygen content in the area in the vicinity of the interface between the recording layer and the protective layer is made lower than the oxygen content in the area in the vicinity of the center of the recording layer.
    Type: Grant
    Filed: November 13, 2007
    Date of Patent: January 25, 2011
    Assignee: Hitachi Global Storage Technologies Netherlands B.V.
    Inventors: Yoshiyuki Hirayama, Ichiro Tamai, Reiko Arai