Milling, Grinding, Crushing, Or Comminuting In Liquid Patents (Class 430/137.19)
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Patent number: 10335754Abstract: A nozzle for producing microparticles includes a nozzle body having an oscillating device and an amplifying portion connected to the oscillating device and located between first and second ends of the nozzle body. A through-hole extends from the first end through the amplifying portion and the second end. A tube assembly is mounted in the through-hole and includes first and second tubes between which a first fluid passageway is defined. A second fluid passageway is defined in the second tube. Two ends of the first tube respectively form a first filling port and a plurality of first outlet ports both of which intercommunicate with the first fluid passageway. Two ends of the second tube respectively form a second filling port and a second outlet port both of which intercommunicate with the second fluid passageway. A formation space is defined between the second outlet port and the first outlet ports.Type: GrantFiled: December 15, 2016Date of Patent: July 2, 2019Assignee: Metal Industries Research & Development CentreInventors: Zong-Hsin Liu, Cheng-Han Hung, Ying-Chieh Lin, Cheng-Tang Pan, Yao-Kun Huang, Ying-Cheng Lu
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Patent number: 9115291Abstract: Provided are high viscosity essentially non-aqueous dispersions containing acrylic core/shell polymer particles in a non-aqueous solvent; sheetfed, heatset and coldset lithographic ink compositions containing the dispersions; and methods of printing with ink containing the dispersions to improve the setting and drying properties and rub resistance of sheet fed offset, heatset and coldset lithographic inks. The lithographic inks containing the dispersions set quickly enough to allow processing of printed sheets soon after printing.Type: GrantFiled: November 15, 2011Date of Patent: August 25, 2015Assignee: Sun Chemical CorporationInventors: Jerome Bollard, Ramasamy Krishnan, Christian Johnke, Hiroyuki Sugiyama, Mark Schneider, David Klein
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Patent number: 9116462Abstract: An image forming apparatus includes an image holding member, a charging unit, an electrostatic charge image forming unit, a developing unit that accommodates an electrostatic charge image developer containing flake shape toner particles, a transfer unit, an arranging unit that causes transfer residual toner to rise from the surface of the image holding member, a cleaning unit, and a fixing unit.Type: GrantFiled: May 27, 2014Date of Patent: August 25, 2015Assignee: FUJI XEROX CO., LTD.Inventor: Naoki Ota
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Patent number: 9098004Abstract: A liquid developer containing toner particles containing a resin and a pigment, and an insulating liquid, the toner particles being dispersed in the insulating liquid, wherein the insulating liquid contains an olefin having 12 carbon atoms or more and 18 carbon atoms or less in an amount of 10% by mass or more. The liquid developer of the present invention can be suitably used in developing latent images formed in, for example, an electrophotographic method, an electrostatic recording method, an electrostatic printing method, or the like.Type: GrantFiled: December 20, 2013Date of Patent: August 4, 2015Assignee: Kao CorporationInventors: Tatsuya Yamada, Shingo Takada
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Publication number: 20150118448Abstract: The present disclosure discloses a liquid electrophotographic ink. The ink includes a liquid vehicle, an ethylene acid copolymer, and an ethylene/(meth)acrylic acid C1-10 alkyl ester copolymer. Also disclosed is a method for the manufacture that ink and a method for performing a liquid electrophotographic process by printing a substrate with the ink.Type: ApplicationFiled: April 27, 2012Publication date: April 30, 2015Inventors: Stella Stolin Roditi, Swissa Shay, Eyal Bachar, Getahun Biadglin, Marc Klein
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Patent number: 9017915Abstract: The present disclosure provides inks, systems, and methods directed towards dispersed pigments. In one embodiment, an electrophotographic ink can comprise an aliphatic solvent and a pigment having a surface comprising carbonyl groups stabilized by an amine dispersant having the structure: R1R2N[(CH2)nNR5]m(CH2)pNR3R4, where R1, R3, R4, and R5 are independently selected from the group of H; COR6; COOR6; CONHR6; linear or branched, substituted or unsubstituted, alkyl; linear or branched, substituted or unsubstituted, aryl; and combinations thereof; R2 is an aliphatic polymer chain; R6 is selected from the group of H; linear or branched, substituted or unsubstituted, alkyl; linear or branched, substituted or unsubstituted, aryl; and combinations thereof; m is from 0 to 200; n is from 1 to 20; and p is from 1 to 20; where the electrophotographic ink has a low field conductivity of less than 200 pS/cm and a viscosity from about 0.5 to about 40 cps.Type: GrantFiled: July 7, 2010Date of Patent: April 28, 2015Assignee: Hewlett-Packard Development Company, L.P.Inventors: Sivapackia Ganapathiappan, Hou T. Ng
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Patent number: 8940469Abstract: A liquid developer for electrography, comprising toner particles dispersed in a liquid carrier, wherein the toner particles include a pigment, a thermoplastic resin, and an organic filler, which organic filler is reactive with groups of the thermoplastic resin and incompatible with the liquid carrier.Type: GrantFiled: October 13, 2006Date of Patent: January 27, 2015Assignee: Hewlett-Packard Development Company, L.P.Inventors: Albert Teishev, Stalla Stolin Rodith, Michael Shishkin
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Publication number: 20140363208Abstract: The present invention relates to a liquid electrophotographic ink comprising a carrier liquid, a pigmented resin composite dispersed in the carrier liquid, and about 0.15 to about 10% (w/w) of an organic wax. The liquid electrophotographic ink is typically formulated for printing in a liquid electrophotographic printer.Type: ApplicationFiled: December 19, 2011Publication date: December 11, 2014Applicant: Hewlett-Packard Indigo B.V.Inventors: Stella Stolin Roditi, Haim Cohen, Getahun Biadglin, Femanda Orilik, Nava Klein, Albert Teishev
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Patent number: 8871420Abstract: A method and system for magnetic actuated mixing which use magnetic particles and magnetic field to facilitate the mixing for preparing latex emulsion. In embodiments, a suitable process includes dissolving a resin in an organic solvent, optionally adding a surfactant, adding a neutralization agent and water, adding magnetic particles, and subjecting the mixture to a magnetic actuated mixing to form a latex emulsion. In embodiments, the latex emulsion thus produced may be utilized to form a toner.Type: GrantFiled: April 10, 2013Date of Patent: October 28, 2014Assignee: Xerox CorporationInventors: Yu Liu, Ke Zhou, Yulin Wang, Frank Ping-Hay Lee
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Patent number: 8852842Abstract: A production process of a toner, wherein wet colored resin particles are poured into a rotary vane type agitating device having a structure that an agitating vane fixed to a rotating drive shaft extending through a bottom wall of an agitation vessel is arranged at a bottom of the agitation vessel, and at least one gas inlet port and at least one gas outlet port are arranged at a lower portion of the agitation vessel and an upper portion of the agitation vessel, respectively, the wet colored resin particles are dried by a method, in which the wet colored resin particles are agitated by the rotary vane within the agitation vessel while supplying a heated gas, thereby forming a fluidized bed, and a mixed gas containing water is discharged from the gas outlet port to the outside, and at that time, drying conditions are controlled in such a manner that the temperature of the gas discharged falls within a range from 20 to 60° C.Type: GrantFiled: February 18, 2009Date of Patent: October 7, 2014Assignee: Zeon CorporationInventors: Takashi Iga, Hisashi Kurokawa
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Patent number: 8846289Abstract: A method of manufacturing toner including melting, mixing, and kneading a releasing agent and a coloring agent with at least part of a polyester binder resin, and suspending and granulating an oil phase comprising the binder resin, the coloring agent, and the releasing agent in an aqueous medium.Type: GrantFiled: September 24, 2010Date of Patent: September 30, 2014Assignee: Ricoh Company, Ltd.Inventors: Satoshi Ogawa, Tsuyoshi Sugimoto, Naohito Shimota, Hiroshi Yamashita, Masana Shiba, Junichi Awamura
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Publication number: 20140234771Abstract: The present invention provides an electrostatic ink composition comprising a carrier liquid, a resin, a pigment and a conductive polymer. Method for producing the electrostatic ink composition and methods for printing the composition are also disclosed.Type: ApplicationFiled: September 30, 2011Publication date: August 21, 2014Applicant: Hewlett-Packard Indigo B.V.Inventors: Gil Bar-Haim, Anatoly Sobolevsky, Yaron Grinwald
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Publication number: 20140186764Abstract: A method for producing a liquid developer containing toner particles containing a resin containing a polyester and a pigment, and an insulating liquid, wherein the toner particles are dispersed in the insulating liquid, including: step 1: melt-kneading the resin and the pigment, and pulverizing a melt-kneaded mixture to provide toner particles; step 2: dispersing the toner particles obtained in the step 1 in the insulating liquid in the presence of a basic dispersant to provide a dispersion of toner particles; and step 3: wet-milling the dispersion of toner particles obtained in the step 2 to provide a liquid developer, wherein the basic dispersant is an amide compound obtained by a reaction between a polyethyleneimine and a polyester (D) obtained by self-condensation of 12-hydroxystearic acid.Type: ApplicationFiled: December 26, 2013Publication date: July 3, 2014Applicant: Kao CorporationInventors: Tatsuya YAMADA, Hiromi Ito, Yoko Hanada
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Patent number: 8765349Abstract: A method of manufacturing toner is provided. In the method, toner constituents are dissolved or dispersed in an organic solvent to prepare a toner constituents liquid. The toner constituents liquid is degassed so that the toner constituents liquid includes dissolved oxygen in an amount of 3 mg/L or less. The toner constituents liquid is vibrated in a chamber having at least one nozzle to form a liquid column resonance standing wave in the toner constituents liquid. The toner constituents liquid is discharged from the nozzle disposed within an area including an antinode of the liquid column resonance standing wave to form the toner constituents liquid into liquid droplets. The liquid droplets are dried to solidify the liquid droplets into solid particles.Type: GrantFiled: July 25, 2012Date of Patent: July 1, 2014Assignee: Ricoh Company, Ltd.Inventors: Yoshihiro Norikane, Andrew Mwaniki Mulwa, Kiyotada Katoh, Yasutada Shitara
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Patent number: 8741531Abstract: A method of manufacturing toner includes forming liquid droplets. The forming liquid droplets includes vibrating a toner constituents liquid in a liquid column resonance liquid chamber having a plurality of nozzles to form a liquid column resonance pressure standing wave therein, and discharging the toner constituents liquid from the nozzles. The method further includes solidifying the liquid droplets. The toner constituents liquid includes an organic solvent and toner constituents dissolved or dispersed in the organic solvent. The toner constituents include a resin, a colorant, and a release agent. The nozzles are disposed within an area including an antinode of the liquid column resonance pressure standing wave. One of the nozzles disposed closer to a node of the liquid column resonance pressure standing wave has a smaller outlet diameter than that disposed farther from the node. The toner constituents liquid is applied with a uniform pressure at a vicinity of each nozzle.Type: GrantFiled: April 12, 2012Date of Patent: June 3, 2014Assignee: Ricoh Company, Ltd.Inventors: Yoshihiro Norikane, Masaru Ohgaki
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Publication number: 20140147172Abstract: A deinkable liquid toner is disclosed herein. The deinkable liquid toner includes a non-polar carrier fluid, a styrene-alkyl acrylate, and a colorant. The styrene-alkyl acrylate has a glass transition temperature ranging from about 65 C to about 100 C. A method for making the deinkable liquid toner and a printing system are also disclosed herein.Type: ApplicationFiled: July 26, 2011Publication date: May 29, 2014Applicant: HEWLETT-PACKARD DEVELOPMENT COMPANY, L.P.Inventors: Hou T. Ng, Sivapackia Ganapathiappan, Albert Teishev
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Patent number: 8703375Abstract: To provide a toner A containing: base particles, each containing polyester, microcrystalline wax, and a colorant; and spherical silica particles having an average primary particle diameter of 100 nm to 150 nm, wherein the microcrystalline wax has an onset temperature of 45° C. to 60° C. as determined by DSC, and a carbon number distribution of 25 to 55.Type: GrantFiled: July 22, 2011Date of Patent: April 22, 2014Assignee: Ricoh Company, Ltd.Inventors: Naohito Shimota, Takahiro Honda, Tsuneyasu Nagatomo, Ryuta Chiba
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Publication number: 20140099576Abstract: A toner for developing an electrostatic charge image includes toner particles obtained by dissolving or dispersing a binder resin and an additive in an organic solvent to prepare an oil phase component, and dispersing and granulating the oil phase component in an aqueous medium containing an inorganic dispersant dispersed therein. The binder resin is a polyester resin obtained from a material containing from 6.5 to 7.5 mol % of a long-chain alkyl group represented by a formula (1), the polyester resin having an acid value of from 4.9 to 7.Type: ApplicationFiled: September 27, 2013Publication date: April 10, 2014Applicant: Oki Data CorporationInventor: Manami HIRAIDE
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Publication number: 20140093821Abstract: A method of producing a liquid developer containing an insulation liquid and toner particles is provided. The method includes: grinding a toner material under the presence of a substance A in the insulation liquid; subjecting a dispersion liquid to a heat treatment at a higher temperature than a glass transition temperature of a resin material while giving shear force to the dispersion liquid: and mixing the dispersion liquid having been subjected to the heat treatment with a substance B. A liquid developer including an insulation liquid, toner particles, and a substance B is also provided. The toner particles are constituted of a substance A, a resin material and a coloring agent. The resin material is a polyester resin and/or a styrene-acrylic resin. The substance A is an acrylic modified silicone sufficiently soluble to the insulation liquid and the substance B is a silanol group-containing polysiloxane and/or a fluorine modified silicone.Type: ApplicationFiled: September 25, 2013Publication date: April 3, 2014Applicants: Shin-Etsu Chemical Co., Ltd., SEIKO EPSON CORPORATIONInventors: Tsutomu TERAOKA, Fuminori YANO, Masanao KAMEI
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Patent number: 8685607Abstract: The continuous process for manufacturing toners disclosed herein includes continuously feeding components of a toner composition into a feed section of a screw extruder at a controlled rate. The continuous process for manufacturing toners may include feeding the components of a toner composition into the feed section of a screw extruder without performing an external or secondary dispersion step. That is to say, the components of the toner composition may be fed directly into the extruder without using dispersions of individual components as used in batch processes. Rather, the toner components are added to the extruder in dry form, melt-mixed, and may be dispersed in aqueous form in the extruder. The process may produce micron-sized toner particles, thus no further size reduction may be necessary.Type: GrantFiled: August 29, 2012Date of Patent: April 1, 2014Assignee: Xerox CorporationInventors: Joo T. Chung, Chieh-Min Cheng, Zhen Lai, Mark E. Mang, Eugene F. Young, Brian Andaya, Joseph Leonardo
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Patent number: 8673534Abstract: The particulate material production method includes vibrating a particulate material composition liquid in a liquid column resonance chamber having at least one nozzle to form a standing wave in the particulate material composition liquid caused by liquid column resonance, so that droplets of the particulate material composition liquid are ejected in a droplet ejection direction from the nozzle so as to fly in a space in a flight direction; feeding a gas in a direction substantially perpendicular to the droplet ejection direction to change the flight direction of the ejected droplets; and solidifying the droplets in the space to produce a particulate material. The particulate material composition liquid includes at least a solvent and a component of the particulate material dissolved or dispersed in the solvent, and the nozzle is located at a location corresponding to an anitnode of the standing wave.Type: GrantFiled: April 3, 2012Date of Patent: March 18, 2014Assignee: Ricoh Company, Ltd.Inventors: Kiyotada Katoh, Yasutada Shitara, Minoru Masuda, Yoshihiro Norikane, Kenta Kenjoh, Satoshi Takahashi
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Publication number: 20130302733Abstract: A liquid electrophotographic ink is disclosed herein. One example of the liquid electrophotographic ink includes a non-polar carrier liquid; pigmented toner particles; a charge director; and polymer resin encapsulated metal oxide nanoparticles. A method for making the liquid electrophotographic ink is also disclosed herein.Type: ApplicationFiled: January 31, 2011Publication date: November 14, 2013Inventors: Doris Pik-Yiu Chun, Hou T. Ng, Albert Teishev
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Patent number: 8580476Abstract: A toner for developing an electrostatic image is provided. The toner includes at least a binder resin; a colorant; and a particulate release agent. The particulate release agent is prepared by heating the release agent to a temperature not lower than a melting point of the release agent to melt the release agent, dissolving the melted release agent in a supercritical fluid or a sub-critical fluid, and feeding the solution into a liquid so that the solution is depressurized and the particulate release agent is formed in the liquid.Type: GrantFiled: March 14, 2011Date of Patent: November 12, 2013Assignee: Ricoh Company, Ltd.Inventors: Masahide Yamada, Chiaki Tanaka, Masahiro Kawamoto, Tatsunori Kamiyama, Satoshi Izumi
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Patent number: 8568628Abstract: A method of preparing a toner, including periodically dripping and discharging droplets of a toner constituent liquid comprising a resin and a colorant with a dripper comprising a thin film comprising plural nozzles configured to discharge the droplets, and an electromechanical converter configured to oscillate the thin film; and solidifying the droplets to form toner particles, wherein the nozzle has an aperture discharging the droplet, having a circular or an ellipsoidal cross-sectional shape and cross-sectional area smaller than a cross-sectional area of another aperture contacting the toner constituent liquid.Type: GrantFiled: May 14, 2008Date of Patent: October 29, 2013Assignee: Ricoh Company, Ltd.Inventors: Yoshihiro Norikane, Shinji Ohtani, Yohichiroh Watanabe, Kazumi Suzuki, Takahiro Honda
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Patent number: 8455172Abstract: A method for producing a toner, containing: dispersing, in an aqueous medium, an oil phase which contains an organic solvent, and a binder resin component contained in the organic solvent, where the binder resin component contains a crystalline polyester resin and an amorphous polyester resin; and removing the organic solvent from the dispersion to obtain the toner, in which the dispersing further contains heating and dissolving the crystalline polyester and the amorphous polyester in the organic solvent to obtain a solution, cooling the solution so as to recrystallize the crystalline polyester resin, and mechanically pulverizing the recrystallized crystalline polyester resin so as to obtain a crystalline polyester dispersion.Type: GrantFiled: September 27, 2010Date of Patent: June 4, 2013Assignee: Ricoh Company, Ltd.Inventors: Junichi Awamura, Hiroshi Yamashita, Teruki Kusahara, Tsuyoshi Sugimoto, Tomomi Suzuki
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Publication number: 20130095422Abstract: A toner, including a crystalline resin as a binder resin, wherein the toner comprises a THF-soluble component in a weight-average molecular weight not less than 20,000, and has a 50% wettability not less than 20% by volume when subjected to a methanol wettability test.Type: ApplicationFiled: October 1, 2012Publication date: April 18, 2013Inventors: Atsushi YAMAMOTO, Shinya Nakayama, Masahide Yamada, Hideyuki Santo, Daiki Yamashita, Ryota Inoue
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Patent number: 8389196Abstract: Provided is a method of preparing a toner, the method including: preparing a solvent emulsion by stirring a medium including a polar medium, an organic solvent, and a surfactant; adding toner components including a resin and a pigment to the solvent emulsion; removing the organic solvent from the solvent emulsion including the toner components; and collecting a toner particle from the solvent emulsion from which the organic solvent is removed.Type: GrantFiled: September 19, 2008Date of Patent: March 5, 2013Assignee: Samsung Fine Chemicals Co., Ltd.Inventors: Woo Young Yang, Keon Il Kim, Dae Il Hwang, Il Hyuk Kim, Jae Bum Park, Il Sun Hwang, Jae Kwang Hwang, Dae Woong Choi, Dong Won Kim, Duck Kyun Ahn
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Patent number: 8362198Abstract: There is provided a method for producing a resin particle capable of unprecedentedly realizing both excellent heat resistant keeping property and melting property. The present invention is a method for producing a resin particle (X) comprising the step of treating a resin particle (B) containing a resin (A) composed of a crystalline part (a) containing, as an essential constitutional component, a polyester (p1) not containing an aromatic ring or a polyester (p2) containing an aromatic ring, and produced by polycondensation of a polyol component and a polycarboxylic acid component, and a noncrystalline part (b), with liquid or supercritical carbon dioxide (C), and removing (C), wherein a heat of fusion measured by differential scanning calorimetry (DSC) of the obtained (X) satisfies the following relational formula (1): 0?H2/H1?0.Type: GrantFiled: February 18, 2011Date of Patent: January 29, 2013Assignee: Sanyo Chemical Industries, Ltd.Inventors: Yasuhiro Shindo, Sho Kim
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Patent number: 8362197Abstract: There is provided a method for producing a resin particle capable of unprecedentedly realizing both excellent heat resistant keeping property and melting property. The present invention is a method for producing a resin particle (X) comprising the step of treating a resin particle (B) containing a resin (A) composed of a crystalline part (a) containing, as an essential constitutional component, a polyester (p1) not containing an aromatic ring or a polyester (p2) containing an aromatic ring, and produced by polycondensation of a polyol component and a polycarboxylic acid component, and a noncrystalline part (b), with liquid or supercritical carbon dioxide (C), and removing (C), wherein a heat of fusion measured by differential scanning calorimetry (DSC) of the obtained (X) satisfies the following relational formula (1): 0?H2/H1?0.Type: GrantFiled: May 20, 2009Date of Patent: January 29, 2013Assignee: Sanyo Chemical Industries, Ltd.Inventors: Yasuhiro Shindo, Sho Kim
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Publication number: 20120301820Abstract: A liquid developer is provided. The liquid developer includes a liquid insulator and toner particles. The liquid insulator toner particles include a resin material, a colorant, a substance A, a substance B, and a substance C. The substance A is an acrylic-modified silicone. The substance B is at least one selected from the group consisting a quaternary cationic silicone, an aminophenyl-modified silicone, and a phenyl-modified silicone. The substance C is at least one of a silanol-containing polysiloxane and a fluorine-modified silicone. The average degree of roundness R1 of the toner particles is 0.890 or greater, if the degree of roundness is expressed as L0/L1, where L1 (?m) is a circumference of a profile view of a measured particle and L0 (?m) is the circumference of a perfect circle of a circumference of a profile view corresponding to the profile view of the measured particle.Type: ApplicationFiled: November 22, 2011Publication date: November 29, 2012Applicant: SEIKO EPSON CORPORATIONInventors: Kenichi NUMAKURA, Yoshihiro UENO, Masahiro OKI, Tsutomu TERAOKA
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Patent number: 8309681Abstract: There is provided a method for producing a resin particle capable of unprecedentedly realizing both excellent heat resistant keeping property and melting property. The present invention is a method for producing a resin particle (X) comprising the step of treating a resin particle (B) containing a resin (A) composed of a crystalline part (a) containing, as an essential constitutional component, a lactone ring-opening polymer (p), and a noncrystalline part (b), with liquid or supercritical carbon dioxide (C), and removing (C), wherein a heat of fusion measured by differential scanning calorimetry (DSC) of the obtained (X) satisfies the following relational formula (1): 0?H2/H1?0.9??(1) [in the relational formula (1), H1 represents a measurement value of a heat of fusion (J/g) at the time of the initial temperature elevation measured by DSC; and H2 represents a measurement value of a heat of fusion (J/g) at the time of the second temperature elevation measured by DSC].Type: GrantFiled: July 22, 2009Date of Patent: November 13, 2012Assignee: Sanyo Chemical Industries, Ltd.Inventors: Takao Mukai, Koji Ota
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Patent number: 8288068Abstract: A toner for use in liquid electrostatic printing, comprising: a carrier liquid; and, a plurality of toner particles, the toner particles being comprised of a pigment; and a mixture of resins, a major portion of the mixture comprising at least a first resin and a minor portion comprising at least one second resin, the second resin having an affinity for the pigment, that is greater than the affinity of the first resin for the pigment, such that the amount of free pigment in the carrier liquid separate from the toner particles is reduced over the amount that would be present in the absence of the at least one second resin of the minor portion.Type: GrantFiled: March 9, 2007Date of Patent: October 16, 2012Assignee: Hewlett-Packard Development Company, L.P.Inventors: Victor Gal, Galia Golodetz, Jose Kuperwasser
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Patent number: 8247153Abstract: An object of the present invention is to provide a resin microparticle for a toner raw material that has a small particle diameter and a narrow particle diameter distribution and has a low odor. There are provided a resin microparticle for a toner raw material characterized in that all of the following requirements (i) to (iii) are satisfied: Requirement (i): A particle diameter of 50% volume (D50) satisfies the relationship 0.05 ?m?D50?1 ?m; Requirement (ii): A particle diameter of 10% volume (D10) and a particle diameter of 90% volume (D90) satisfy the relationship D90/D10?7; and Requirement (iii): The content of an organic solvent is not more than 70 ppm.Type: GrantFiled: September 23, 2008Date of Patent: August 21, 2012Assignee: Mitsui Chemicals, Inc.Inventors: Hiroshi Matsuoka, Ichirou Sasaki, Toshimitsu Narutaki, Masaru Wakizaka, Hiroyuki Takei
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Patent number: 8227167Abstract: The method for producing a developing agent according to the invention contains subjecting the toner material dispersion liquid to mechanical shearing to make the granular mixture into fine particles, thereby providing a dispersion liquid containing fine particles having a smaller particle diameter than a particle diameter of the granular mixture. The toner material dispersion liquid is subjected to mechanical shearing under a temperature of a glass transition point Tg of the binder resin or more and a pressure of 10 MPa or more, and the resulting dispersion liquid containing the fine particles is depressurized with two or more stages while maintaining the temperature of a glass transition point Tg of the binder resin or more and then cooled to a temperature of a glass transition point Tg of the binder resin or less.Type: GrantFiled: July 9, 2009Date of Patent: July 24, 2012Assignees: Kabushiki Kaisha Toshiba, Toshiba Tec Kabushiki KaishaInventors: Tsuyoshi Itou, Takayasu Aoki, Takashi Urabe, Yasuhito Noda, Motonari Udo, Satoshi Araki, Masahiro Ikuta, Takafumi Hara, Asumi Matsumoto
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Patent number: 8221955Abstract: Methods of making ink toners for use in electrostatic imaging are disclosed.Type: GrantFiled: July 25, 2006Date of Patent: July 17, 2012Assignee: Hewlett-Packard Development Company, L.P.Inventors: Gal Victor, Dan Scheffer, Galia Golodetz, Jose Kuperwasser, Natalia Katz
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Patent number: 8211611Abstract: A process for making particles is provided. In embodiments, a suitable process includes adding a rheology modifier to an emulsion utilized to form toner particles. The rheology modifier permits the use of a higher solid content in the emulsion, with a resulting higher yield of toner particles, without requiring the use of powerful mixing equipment.Type: GrantFiled: June 5, 2009Date of Patent: July 3, 2012Assignee: Xerox CorporationInventors: Zhaoyang Ou, Zhen Lai, Christopher D. Blair, Chieh-Min Cheng
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Patent number: 8198001Abstract: A process for producing a liquid developer includes: providing a dispersion liquid containing an aqueous dispersion medium and toner mother particles including a rosin resin; chemically modifying surfaces of the toner mother particles with an amine-based material by mixing the amine-based material with the dispersion liquid to obtain toner particles; and dispersing the toner particles in an insulating liquid.Type: GrantFiled: July 6, 2009Date of Patent: June 12, 2012Assignee: Seiko Epson CorporationInventors: Yoshihiro Ueno, Masahiro Oki
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Patent number: 8192911Abstract: A method of manufacturing a toner including dispersing a binder resin, a coloring agent and a releasing agent in an organic solvent to obtain an oil phase; dispersing the oil phase in an aqueous medium with a shearing force to obtain a dispersion emulsion; wherein the shearing force is made by a screen or vessel that is situated around a rotor, the screen spinning in a direction opposite to the direction that the rotor spins. Toner produced. Method of using the toner.Type: GrantFiled: May 8, 2009Date of Patent: June 5, 2012Assignee: Ricoh Company, Ltd.Inventors: Junichi Awamura, Akinori Saitoh, Osamu Uchinokura, Masahide Yamada, Tomomi Suzuki
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Patent number: 8187784Abstract: A toner composition including toner particles, wherein the toner particles are prepared by a method in which toner constituents including at least a binder resin and a colorant are kneaded upon application of heat to prepare a toner constituent mixture; the toner constituent mixture is dissolved or swelled in an organic solvent capable of dissolving or swelling at least the binder resin to prepare an oil phase liquid; the oil phase liquid is emulsified in an aqueous liquid to prepare an emulsion; the emulsion is coagulated; and then the coagulated emulsion is dried to prepare the toner particles.Type: GrantFiled: October 29, 2010Date of Patent: May 29, 2012Assignee: Ricoh Company LimitedInventors: Hiroshi Yamashita, Masami Tomita, Shigeru Emoto, Tsunemi Sugiyama
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Patent number: 8163458Abstract: A toner capable of forming high quality images of excellent image reproducibility at high definition and high resolution, being decreased for the bleed-out of a wax ingredient to the surface, causing less filming to a photoreceptor and offset phenomenon in a high temperature region, is provided. The toner is manufactured by a method including a preliminary pulverizing step of pulverizing a melt-kneaded product of toner raw materials in a liquid to obtain a coarse powder slurry containing a coarse toner powder, a finely pulverizing step of passing the coarse powder slurry through a pressure resistant nozzle under heating and pressurization thereby further pulverizing the coarse toner powder to obtain a fine powder slurry containing a fine toner powder and in a heated and pressurized state, a cooling step of cooling the fine powder slurry, and a depressurizing step of depressurizing the fine powder slurry.Type: GrantFiled: July 3, 2008Date of Patent: April 24, 2012Assignee: Sharp Kabushiki KaishaInventors: Keiichi Kikawa, Katsuru Matsumoto
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Publication number: 20120009516Abstract: The present disclosure provides inks, systems, and methods directed towards dispersed pigments. In one embodiment, an electrophotographic ink can comprise an aliphatic solvent and a pigment having a surface comprising carbonyl groups stabilized by an amine dispersant having the structure: R1R2N[(CH2)nNR5]m(CH2)pNR3R4, where R1, R3, R4, and R5 are independently selected from the group of H; COR6; COOR6; CONHR6; linear or branched, substituted or unsubstituted, alkyl; linear or branched, substituted or unsubstituted, aryl; and combinations thereof; R2 is an aliphatic polymer chain; R6 is selected from the group of H; linear or branched, substituted or unsubstituted, alkyl; linear or branched, substituted or unsubstituted, aryl; and combinations thereof; m is from 0 to 200; n is from 1 to 20; and p is from 1 to 20; where the electrophotographic ink has a low field conductivity of less than 200 pS/cm and a viscosity from about 0.5 to about 40 cps.Type: ApplicationFiled: July 7, 2010Publication date: January 12, 2012Inventors: Sivapackia Ganapathiappan, Hou T. Ng
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Patent number: 8039191Abstract: A toner having a BET specific surface area of from 1.5 to 3.5 m2/g, obtainable by a process including the steps of; step (1): pulverizing a toner composition containing at least a resin binder and a colorant in the presence of fine inorganic particles having an average primary particle size of from 6 to 20 nm to obtain mother toner particles having a volume-median particle size of from 3 to 8 ?m; and step (2): externally adding silica having an average primary particle size of from 25 to 60 nm to the mother toner particles obtained in the above step (1). The toner of the present invention is suitably used for, for example, developing a latent image formed in electrophotography, electrostatic recording method, electrostatic printing method, or the like.Type: GrantFiled: June 6, 2007Date of Patent: October 18, 2011Assignee: Kao CorporationInventor: Akihiro Eida
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Patent number: 8012661Abstract: A method for producing a developing agent contains mechanically shearing a mixture containing a polyester resin, a colorant and a releasing agent to form first fine particles, aggregating the first fine particles to form aggregated particles as a core, aggregating second fine particles containing a polyester resin onto the core to form a shell.Type: GrantFiled: October 29, 2008Date of Patent: September 6, 2011Assignees: Kabushiki Kaisha Toshiba, Toshiba Tec Kabushiki KaishaInventors: Motonari Udo, Takayasu Aoki, Takashi Urabe, Tsuyoshi Itou, Yasuhito Noda, Satoshi Araki, Masahiro Ikuta, Takafumi Hara
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Patent number: 8012663Abstract: A method of manufacturing a toner includes preparing a droplet forming device, comprising a storage portion to store a toner composition solution, a thin film formed from a rigid material, bonded to the storage portion by a bonding material, and provided with a nozzle and an oscillation device including an oscillation generation device configured to generate an oscillation upon the thin film and an oscillation amplification device which has an oscillation surface including a position that is parallel and opposite to the thin film and is configured to amplify the oscillation, periodically forming a droplet of the toner composition solution including at least a resin and a coloring agent to be supplied between the thin film and the oscillation surface and discharging the droplet via the nozzle, and solidifying the droplet of the toner composition solution discharged via the nozzle, and forming a toner particle.Type: GrantFiled: March 10, 2009Date of Patent: September 6, 2011Assignee: Ricoh Company, Ltd.Inventors: Yoshihiro Norikane, Shinji Aoki, Tetsuya Sonoda, Keisuke Uchida
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Patent number: 8003291Abstract: A method of charging toner particles in a liquid toner comprising: mixing the toner with an acid; and mixing the toner with a base that reacts with the acid to charge the toner particles.Type: GrantFiled: March 20, 2007Date of Patent: August 23, 2011Assignee: Hewlett-Packard Development Company, L.P.Inventors: Yaacov Almog, Avi Koller, Ilya Taraniuk
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Patent number: 8003290Abstract: A method for manufacturing a developing agent by mixing a resin having a dissociable functional group and an aqueous medium, subjecting the mixture to mechanical shearing, finely pulverizing the pulverized mixture to form resin microparticles, adding a dispersion of colorant particles, causing the resin microparticles and colorant particles to agglomerate, and forming toner particles.Type: GrantFiled: January 16, 2007Date of Patent: August 23, 2011Assignees: Kabushiki Kaisha Toshiba, Toshiba Tec Kabushiki KaishaInventors: Takashi Urabe, Tsuyoshi Ito, Motonari Udo, Masahiro Ikuta
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Patent number: 7939238Abstract: A dry toner for developing an electrostatic image, including a toner binder containing a urea-modified polyester. The toner has an average sphericity of 0.96 or more and contains no more than 30% by weight of particles having a sphericity of less than 0.95.Type: GrantFiled: February 12, 2009Date of Patent: May 10, 2011Assignee: Ricoh Company, Ltd.Inventors: Hiroshi Yamashita, Tsunemi Sugiyama, Shigeru Emoto, Masami Tomita
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Patent number: 7901862Abstract: It is intended to provide a method includes the step of forming agglomerated particles by agglomerating fine particulate mixture containing a binder resin and a colorant. In the step of forming agglomerated particles, a cationic organic coagulating agent having an average molecular weight of from 1000 to 100000 is added to a liquid dispersion containing fine particles.Type: GrantFiled: October 2, 2008Date of Patent: March 8, 2011Assignees: Kabushiki Kaisha Toshiba, Toshiba Tec Kabushiki KaishaInventors: Tsuyoshi Itou, Takayasu Aoki, Takashi Urabe, Motonari Udo, Yasuhito Noda, Satoshi Araki, Masahiro Ikuta, Takafumi Hara
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Patent number: 7879523Abstract: A toner composition including toner particles, wherein the toner particles are prepared by a method in which toner constituents including at least a binder resin and a colorant are kneaded upon application of heat to prepare a toner constituent mixture; the toner constituent mixture is dissolved or swelled in an organic solvent capable of dissolving or swelling at least the binder resin to prepare an oil phase liquid; the oil phase liquid is emulsified in an aqueous liquid to prepare an emulsion; the emulsion is coagulated; and then the coagulated emulsion is dried to prepare the toner particles.Type: GrantFiled: January 12, 2009Date of Patent: February 1, 2011Assignee: Ricoh Company LimitedInventors: Hiroshi Yamashita, Masami Tomita, Shigeru Emoto, Tsunemi Sugiyama
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Publication number: 20110014561Abstract: Provided are a toner and a toner manufacturing method with which high image density and a broad range of color reproduction are obtained, and with which high-quality images are also obtained. The toner is composed of toner particles that comprise a binding resin containing a polyester resin and a colorant, and contains 10-1,500 ppm of a metal element selected from titanium, germanium, and aluminum, and a cyclic phenol sulfide represented by general formula (1) selected from thiacalixarene, sulfinyl thiacalixarene and sulfonyl thiacalixarene.Type: ApplicationFiled: June 26, 2009Publication date: January 20, 2011Applicant: KONICA MINOLTA BUSINESS TECHNOLOGIES, INC.Inventors: Masahiro Anno, Masahiko Nakamura, Tsuyoshi Uchida, Kouichi Sugama, Kenichi Onaka, Junya Onishi