Carnauba Wax, Beeswax, Montan Wax, Or Oxidized Microcrystalline Wax Or Modified Forms Thereof Patents (Class 524/277)
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Patent number: 6652979Abstract: Biaxially-drawn polyester film for fabrication which is characterized in that it is a film comprising polyester in which ethylene terephthalate units and/or ethylene naphthalate units are the chief structural component and containing 0.1-2 wt % of a carnauba wax and 1 to 200 ppm of germanium, and the melting point of said film is 180-270° C., the angle of contact to water is 70°-120°, and the planar orientation coefficient is 0.08-0.15. This film shows outstanding release properties following repeated use, use after fabrication and use in an aqueous environment and, furthermore, it exhibits stable properties with little variation and, in particular, following lamination to metal sheet such as steel or aluminium, when used as the inner face of a fabricated metal can, it is outstanding in its non-stick properties to the contents, and provides a combination of heat resistance and processability.Type: GrantFiled: August 2, 2001Date of Patent: November 25, 2003Assignee: Toray Industries, Inc.Inventors: Kohzo Takahashi, Ryosuke Matsui, Masahiro Kimura
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Publication number: 20030204001Abstract: A plastic film comprised of a polymer material, fragrance, and a waxy chemical composition for imparting to the film substantial impermeability to odors. A method for producing such films including the steps of: adding a liquid fragrance to highly porous polymer pellets; adding a waxy chemical composition to the fragrance and polymer; blending the polymer, fragrance, and waxy composition mixture; adding additional polymer to the blended mixture; extruding the resultant composition, thereby forming pellets; mixing the pellets with additional polymer; and forming a film therefrom. A plastic film, produced according to this method, for packaging or for masking unpleasant odors, comprising polyethylene or polypropylene, a fragrance, and a bis fatty-acid amide is also disclosed.Type: ApplicationFiled: May 27, 2003Publication date: October 30, 2003Inventors: David Van Gelder, Sharon Voss
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Publication number: 20030204003Abstract: Continuous coatings including floor finishes can be prepared using novel two part compositions and methods. The two part compositions comprise a solid particulate polymer part and a liquid coalescing agent part. A novel method of the invention involves contacting the coalescing agent with the polymer in a variety of coating methods including applying the polymer to the coalescing agent, applying the coalescing agent to the polymer or applying the coalescing agent and polymer simultaneously. The polymer and coalescing agent interact to form a continuous coating layer or finish layer.Type: ApplicationFiled: May 13, 2003Publication date: October 30, 2003Inventors: Keith E. Olson, Bryan M. Anderson, Robert D.P. Hei
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Patent number: 6632863Abstract: A cellulose/polyolefin pellet comprising polyolefin material and cellulosic material. The pellet may be concentrated such that it contains less than about 20% by weight of the polyolefin material and at least about 55% by weight of the cellulosic material. The pellet may be shipped to a remote manufacturing location where it may be blended with additional polyolefin material to make a synthetic wood component.Type: GrantFiled: October 25, 2001Date of Patent: October 14, 2003Assignee: Crane Plastics Company LLCInventors: Herbert L. Hutchison, Jeffrey R. Brandt
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Patent number: 6624221Abstract: A resin composition comprising, in admixture, (A) a specific thermoplastic resin component, (B) at least one wax component selected from among (b-1) a fatty acid having 20-80 carbon atoms and/or a derivative thereof and (b-2) an oxidized natural wax and/or derivative having a neutralization value of 60-190 mg KOH/g, and optionally, (C) a basic inorganic metal compound capable of neutralizing acid groups in the thermoplastic resin component (A) and/or the wax component (B) is improved in flow, moldability and heat resistance and thus suitable to form a layer of a golf ball which exhibits improved rebound and distance properties.Type: GrantFiled: May 30, 2001Date of Patent: September 23, 2003Assignee: Bridgestone Sports Co., Ltd.Inventors: Rinya Takesue, Yasushi Ichikawa
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Patent number: 6551688Abstract: A calendered film or sheet of a polyester resin composition has a haze value of less than 5 percent. The polyester resin composition comprises a polyester having a crystallization half-time from a molten state of at least 5 minutes and an additive comprising (i) a fatty acid or a salt of a fatty acid containing more than 18 carbon atoms and (ii) an ester wax comprising a fatty acid containing more than 18 carbon atoms with an alcohol containing from 2 to 28 carbon atoms, wherein the ratio of the fatty acid or salt of the fatty acid to the ester wax is 1:1 or greater. Also, the present invention is a process for producing such calendered film or sheet having a haze value of less than 5 percent.Type: GrantFiled: February 28, 2001Date of Patent: April 22, 2003Assignee: Eastman Chemical CompanyInventors: Eric Jon Moskala, Kevin Douglas Horton
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Patent number: 6545077Abstract: Various monofilament dental tapes with substantive coatings including: solutions of block copolymers and non-ionic surfactants, melt emulsions of waxes emulsified in surfactants and inverse melt emulsions of surfactants emulsified in a continuous wax phase, and their methods of manufacture are described.Type: GrantFiled: August 23, 2001Date of Patent: April 8, 2003Assignee: International Tape Partners, LLCInventors: Ira D. Hill, Dale G. Brown
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Publication number: 20030060542Abstract: A process for reducing the water-vapor permeability of films or coatings made from polymer compositions (Q) comprising beeswax or comprising montan ester wax or comprising mixtures of these, by preparing a composition (Z) comprising Z1) from 40 to 98.5% by weight of at least one polymer compatible with the polymer (Q1) which is the basis of Q, Z2) from 0.5 to 20% by weight of starch or cellulose or a mixture of these as compatibilizer, Z3) from 1 to 20% by weight of beeswax or montan ester wax or a mixture of these, and Z4) from 0 to 20% by weight of at least one additive, where the percentages by weight are based on the total weight of Z, and in a second step combining the composition Z with the polymer (Q1) which is the basis of Q.Type: ApplicationFiled: August 27, 2002Publication date: March 27, 2003Inventors: Uwe Witt, Gabriel Skupin
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Patent number: 6538049Abstract: The invention relates to an aqueous ink composition for use in ink jet printers comprising an aqueous carrier, a colorant, a polymeric dispersant, and a specific cosolvent mixture comprising C2-C8 terminal alkanediols with a second component selected from polyethylene glycol-type materials and polyol/alkylene oxide condensates. The ink compositions demonstrate excellent stability, good maintenance characteristics for the printers in which they are used, and excellent optical density and print characteristics.Type: GrantFiled: May 21, 1997Date of Patent: March 25, 2003Assignee: Lexmark International, Inc.Inventors: William David Kappele, Anna Marie Pearson
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Patent number: 6534572Abstract: The present invention relates to a composition comprising a thermoplastic component and at least one superabsorbent polymer, methods of use for such composition, and articles comprising such composition. The composition may be formed into a film layer or applied to an article with various hot melt adhesive application techniques. The composition is useful for a variety of end-uses, particularly for use in disposable absorbent articles such as disposable diapers, feminine napkins and medical dressings.Type: GrantFiled: May 6, 1999Date of Patent: March 18, 2003Assignee: H. B. Fuller Licensing & Financing, Inc.Inventors: Sharf U. Ahmed, Andualem W. Emiru, Leslie J. Clapp, Mark S. Kroll
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Patent number: 6534573Abstract: The present invention provides a method for reducing bleeding number in wax compositions comprising wax and oil, wherein said waxes are selected from petroleum and synthetic waxes and said oil is present in the range of 1 to 45% w/w, by incorporating in the composition an effective amount of an oil retention agent in the form of an elastomeric polymer. The invention has particularly useful application to wax compositions used for wax candles. The invention further provides the use of elastomeric polymers for reducing bleeding number in wax compositions.Type: GrantFiled: March 29, 2000Date of Patent: March 18, 2003Assignee: Shell Oil CompanyInventors: Jean-Michel Mace, Olivier Roumache
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Patent number: 6518343Abstract: A wet-stick pressure-sensitive adhesive is provided wherein the pressure-sensitive adhesive comprises: at least one copolymerized monoethylenically unsaturated (meth)acrylic acid ester monomer, wherein the (meth)acrylic acid ester monomer, when homopolymerized, has a Tg of less than about 10° C.; at least one copolymerized hydrophilic acidic comonomer; and at least one nonreactive copolymer comprising at least two copolymerized alkylene oxides, at least one of which is hydrophobic and at least one of which is hydrophilic.Type: GrantFiled: August 13, 1999Date of Patent: February 11, 2003Assignee: 3M Innovative Properties CompanyInventors: Donald H. Lucast, Dong-Wei Zhu
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Patent number: 6518334Abstract: This invention relates to polymer blends comprising a polycarboxypolyamide resin with an alkali dispersible resin. This invention also relates to the use of the polymer blends to prepare aqueous dispersions. The aqueous dispersions were obtained by heating polycarboxypolyamide resins with alkali dispersible resins in an aqueous medium. The invention further relates to coating compositions containing the aqueous dispersions. Such coating compositions include inks, floor finishes, overprint varnishes, sizing, paints and adhesives.Type: GrantFiled: March 22, 2000Date of Patent: February 11, 2003Assignee: JohnsonDiversey, Inc.Inventors: Glenn C. Calhoun, Michael T. Sarkis
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Publication number: 20030027910Abstract: A thermally conductive mechanically compliant pad including a quantity of gallium and/or indium alloy liquid at temperatures below about 120° C. and a boron nitride particulate solid blended into the liquid metal alloy to form a paste. The paste is then combined with a quantity of a matrix forming flowable plastic resin such as microwax, silicone wax, or other silicone polymer to form the thermally conductive mechanically compliant pad, the compliant pad comprising from between about 10% and 90% of metal alloy coated particulate, balance flowable plastic resin.Type: ApplicationFiled: September 5, 2001Publication date: February 6, 2003Applicant: The Bergquist CompanyInventors: Sanjay Misra, Gm Fazley Elahee
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Patent number: 6515057Abstract: A method and product which provides a solid, non-powdered homogeneous form to liquid and low melting point solid compounds which facilitates stability, storage, dispersability and handling and which may be added directly to formulations requiring the liquid compound or low melting point solid compound. The liquid or low melting point solid ingredient is combined with a binder which is comprised of at least a wax and thermoplastic polymer. During the method of forming the product, both the binder and the liquid compound (or low melting point solid compound) pass through a liquid phase during which they are mixed. The product is then formed and cooled.Type: GrantFiled: November 21, 2000Date of Patent: February 4, 2003Assignee: Rhein Chemie CorporationInventors: Richard D. Cortelezzi, Clifford C. Martin
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Publication number: 20030022978Abstract: The invention relates to the use of polyolefin waxes, which are produced by means of metallocene catalysis, for dispersing pigments in plastics.Type: ApplicationFiled: August 27, 2002Publication date: January 30, 2003Inventors: Gerd Hohner, Rainer Bott, Reiner Hess
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Publication number: 20020188092Abstract: A calendered film or sheet of a polyester resin composition has a haze value of less than 5 percent. The polyester resin composition comprises a polyester having a crystallization half-time from a molten state of at least 5 minutes and an additive comprising (i) a fatty acid or a salt of a fatty acid containing more than 18 carbon atoms and (ii) an ester wax comprising a fatty acid containing more than 18 carbon atoms with an alcohol containing from 2 to 28 carbon atoms, wherein the ratio of the fatty acid or salt of the fatty acid to the ester wax is 1:1 or greater. Also, the present invention is a process for producing such calendered film or sheet having a haze value of less than 5 percent.Type: ApplicationFiled: February 28, 2001Publication date: December 12, 2002Inventors: Eric Jon Moskala, Kevin Douglas Horton
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Patent number: 6492463Abstract: A composition comprising a thermotropic liquid crystalline polymer (LCP) and small quantities of low molecular weight polyethylene (PE) is disclosed. The PP acts as an internal lubricant or mold release, but suprisingly does not significantly increase the flammability of the LCP.Type: GrantFiled: July 7, 1998Date of Patent: December 10, 2002Assignee: E. I. du Pont de Nemours and CompanyInventor: Marion Glen Waggoner
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Patent number: 6465066Abstract: A packaged potable liquid, such as bottled water, wherein the liquid has little or no plastic off-taste. The packaged liquid includes a closure wherein the closure shell or the liner within the closure comprises a plastic matrix and an organic slip agent dispersed in the plastic matrix, the slip agent being substantially fully ethylenically saturated and the closure or the liner being substantially free of an ethylenically unsaturated compound. The packaged liquid also includes a container which is desirably substantially free of an ethylenically unsaturated compound.Type: GrantFiled: May 11, 1999Date of Patent: October 15, 2002Assignee: The Coca-Cola CompanyInventors: Mark Rule, James Ellison Shepherd, Colin Beveridge, Homaira Naseem
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Patent number: 6461549Abstract: A method of producing a biodegradable product. which is intended, for instance, for only temporarily containing foodstuffs, or of producing objects such as a container for snacks, a beaker for hot or cold,drinks, etc., which product is. manufactured under pressure and heat in a mold from a basic material. The method is characterized in that the composition of the basic material consists of a moist granulate consisting of 50-250 parts by weight amylose-comprising flour derived from an edible crop plant, 10-85 parts by weight wood flour, 2-30 parts by weight natural wax and 50-250 parts by weight water and optionally a natural colorant as an additive.Type: GrantFiled: March 10, 2000Date of Patent: October 8, 2002Assignee: Potatopak LimitedInventor: Marinus Comelis Meeuwsen
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Patent number: 6455618Abstract: Described is a thermoplastic molding composition comprising: a) 0.05 to 1.5 wt. %, with respect to the entire molding composition, of a fatty acid amide ester wax; b) 0.5 to 10 wt. %, with respect to the entire molding composition, of a silica selected from natural silica, synthetic silica and mixtures thereof; c) 0 to 1 wt. %, with respect to the entire molding composition, of a montan wax; and d) at least one thermoplastic elastomer. Also described are a method of preparing the thermoplastic molding composition, and methods of preparing articles from the thermoplastic molding composition.Type: GrantFiled: June 7, 2001Date of Patent: September 24, 2002Assignee: Wolff Walsrode AGInventors: Ralf Schledjewski, Hans-Werner Funk, Dirk Schultze, Rainer Brandt
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Patent number: 6433053Abstract: The present invention relates to compositions which modify the surface adhesion properties of a surface such as, tableware, cutting boards and food preparation areas generally.Type: GrantFiled: May 14, 2001Date of Patent: August 13, 2002Assignee: The Procter & Gamble CompanyInventors: Chandrika Kasturi, Keith Homer Baker, William Michael Scheper, Peter Yau-Tak Lin, Magda El-Nokaly
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Patent number: 6410627Abstract: A hot melt adhesive composition comprising (a) greater than 40% by weight of a polymeric component; and (b) 5 to 40% by weight of a high hydroxyl number compound, with hydroxyl number greater than 100 mg KOH/g.Type: GrantFiled: April 9, 1999Date of Patent: June 25, 2002Assignee: National Starch and Chemical Investment Holding CorporationInventors: Charles W. Paul, Mitchell J. Blumenthal
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Patent number: 6407160Abstract: The present invention relates to a polymer particle having a wax phase and a second phase. The wax phase includes a wax having a melting point of greater than 30° C. and comprising greater than 80% by weight of the wax phase. The second phase, free of ionic charge groups, includes a mono-alpha, beta-ethylenically unsaturated monomer free of ionic charge groups capable of addition polymerization to form a water soluble homopolymer including from 1 to 40% by weight of the second phase and a mono-alpha, beta-ethylenically unsaturated monomer capable of addition polymerization to form a water insoluble homopolymer.Type: GrantFiled: December 28, 1998Date of Patent: June 18, 2002Assignee: Eastman Kodak CompanyInventors: Yongcai Wang, James L. Bello, Janglin Chen, Dwight W. Schwark
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Patent number: 6384120Abstract: A synthetic resin film for agriculture suited as a covering material for greenhouses or the like, which shows good anti-clouding and anti-fogging properties immediately after being spread and for longer period than 2 years. The synthetic resin film for agriculture is obtained by using (a) an ester of sorbitan with a higher fatty acid mainly containing 24 to 34 carbon atoms (montanic acid wax), an ester of glycerin with montanic acid wax and/or alkylene oxide adducts thereto and/or an ester of polyoxyalkylene with montanic acid wax as an anti-clouding agent, and (b) a fluorine-containing surfactant as an anti-fogging agent, kneading them with a film-forming resin such as vinyl chloride resin, polyethylene, ethylene/vinyl acetate copolymer, and forming it into a film.Type: GrantFiled: September 14, 1999Date of Patent: May 7, 2002Assignee: Clariant Finance (BVI) LimitedInventors: Takuya Hoga, Hiroshi Ohsawa, Masaki Nakamura
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Patent number: 6369126Abstract: The present invention relates to topical adhesives used for the attachment of articles to the skin. The topical adhesive provides secure attachment and is pleasing to the skin upon application, yet causes no discomfort and a low level of adhesive residue on the skin upon removal. The topical adhesive is selected to have rheological characteristics determined by the relationship between the elastic modulus G′ and the viscous modulus G″.Type: GrantFiled: June 23, 1999Date of Patent: April 9, 2002Assignee: The Procter & Gamble Co.Inventors: Fabio Cinelli, Peter Coles, Italo Corzani
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Publication number: 20020016402Abstract: A moistureproof hot melt composition comprising polyethylene and/or polypropylene (A) and a tackifier resin (B), component (A), component (B) and wax (C), an ethylene-vinyl acetate copolymer (D) and component (B), or component (D), component (B) and component (C); and moistureproof paper excellent in moistureproof properties and recyclability, low in cost and excellent in productivity, which paper is coated with the above composition.Type: ApplicationFiled: May 24, 2001Publication date: February 7, 2002Applicant: YASUHARA CHEMICAL CO. LTDInventors: Tatsuhiro Kuno, Takaichiro Shimokado, Yoshitada Nishikiori
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Patent number: 6337365Abstract: An electronic/electric part used in a clean room in which the atmosphere is controlled to process a substrate in a semiconductor device industry, which contains a resin base material and additives added to the resin base material. The additives contain one or more materials selected from the group consisting of an anti-electrostatic agent made of a nonionic compound of a molecular weight of 350 or higher, an anti-oxidizing agent made of a phenolic compound of a molecular weight of 300 or higher, a lubricant, a plasticizer, a fire retardant, and a water repellent. The additives hardly releases gaseous organic substances from the resin base material under a condition where the part is used.Type: GrantFiled: September 24, 1999Date of Patent: January 8, 2002Assignees: Tokyo Electron Limited, Taisei CorporationInventors: Takenobu Matsuo, Tsuyoshi Wakabayashi, Misako Saito, Sadao Kobayashi, Yoshihide Wakayama, Masayuki Imafuku
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Patent number: 6319979Abstract: Disclosed are packages, cartons, cases, and trays comprising a hot melt adhesive, in turn comprising at least one first homogenous linear or substantially linear ethylene polymer having a particular density and melt viscosity at 350° F. (177° C.), up to 60 weight percent wax and up to 40 weight percent tackifier. In particular, disclosed are packages, cartons, cases, and trays comprising a hot melt adhesive characterized by: a) at least one homogeneous linear or substantially linear interpolymer of ethylene with at least one C3-C20 &agr;-olefin interpolymer having a density from 0.850 g/cm3 to 0.895 g/cm3; and b) up to 60 weight percent of at least one tackifying resin; and c) up to 40 weight percent of at least one wax, wherein the hot melt adhesive has a viscosity of less than about 5000 cPs (50 grams/(cm.second)) at 150° C.Type: GrantFiled: February 2, 2000Date of Patent: November 20, 2001Assignees: The Dow Chemical Company, H. B. Fuller Licensing & Financing, Inc.Inventors: Robert A. Dubois, Cynthia L. Rickey, Steven W. Albrecht, Thomas F. Kauffman, Beth M. Eichler, Maynard Lawrence, Thomas H. Quinn
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Patent number: 6300398Abstract: The subject invention is directed to polymer compositions which comprise a homogeneous ethylene/&agr;-olefin interpolymer, a wax and a nucleating agent, wherein the nucleating agent is provided in an effective amount such that the percent elongation at break of the polymer composition is at least about fifty percent greater than the percent elongation at break of a comparative composition which lacks the nucleating agent. The polymer compositions of the invention will find utility in applications r equiring high elongation at break, while maintaining a high onset of crystallization temperature, such as in the high-speed coating of fabrics, carpet backing, floor tile and sheeting, and adhesives.Type: GrantFiled: April 14, 1998Date of Patent: October 9, 2001Assignee: The Dow Chemical CompanyInventors: Gary Lee Jialanella, Thomas J. McKeand, Jr., Kalyan Sehanobish
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Patent number: 6294594Abstract: A denture adhesive base composition consisting essentially of polyvinyl pyrrolidone and ethylene oxide polymer. A denture adhesive composition including this base composition is also provided with other optional adhesive components. Also is provided a method for formulating a novel denture adhesive base composition consisting essentially of polyvinyl pyrrolidone and ethylene oxide polymer.Type: GrantFiled: September 12, 2000Date of Patent: September 25, 2001Assignee: Block Drug Company, Inc.Inventors: Michael J. Borja, Alan A. Halecky
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Patent number: 6258882Abstract: Polish formulations are provided which comprise: a) an aliphatic hydrocarbon solvent comprising 0-10% aromatic hydrocarbons; b) an acrylic resin; and c) a wax product that is thermoplastic, transparent, a solid at room temperature and has a melting/softening point of about 60° to about 90° C.; wherein wt:wt ratio of said acrylic resin and wax is about 1:3 to about 1:8 and the wt:wt ratio of said resin and wax to said solvent is about 1:1 to about 1:9. The formulations function as surface polishes that can be used on any hard surface including wood, metal, stone, and other non-porous surfaces.Type: GrantFiled: December 23, 1998Date of Patent: July 10, 2001Assignee: The Smithsonian InstitutionInventor: Melvin Joseph Wachowiak, Jr.
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Patent number: 6214913Abstract: A method and product which provides a solid, non-powdered homogeneous form to liquid and low melting point solid compounds which facilitates stability, storage, dispersability and handling and which may be added directly to formulations requiring the liquid compound or low melting point solid compound. The liquid or low melting point solid ingredient is combined with a binder which is comprised of at least a wax and thermoplastic polymer. During the method of forming the product, both the binder and the liquid compound (or low melting point solid compound) pass through a liquid phase during which they are mixed. The product is then formed and cooled.Type: GrantFiled: February 24, 1997Date of Patent: April 10, 2001Assignee: Rhein Chemie CorporationInventors: Richard D. Cortelezzi, Clifford C. Martin
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Patent number: 6187849Abstract: Disclosed is a temporary, protective dry lubricating coating composition which when deposited and dried on a metallic substrate, is removable by contacting with an aqueous alkaline cleaning solution. The coating composition comprises (a) a wax present in an amount up to 20 weight percent; (b) a base-neutralized, acid functional polymer which is the polymerization reaction product of (i) a polymerizable, ethylenically unsaturated monomer having acid functionality and (ii) at least one polymerizable, ethylenically unsaturated monomer different from (i); and (c) an amine containing an acyclic moiety of from 8 to 30 carbon atoms, the amine being different from the base used to neutralize the acid functional polymer (b). The temporary protective coating is compatible with a wide range of adhesives and sealants used in the assembly of automobiles.Type: GrantFiled: March 25, 1999Date of Patent: February 13, 2001Assignee: PPG Industries Ohio, Inc.Inventors: Richard M. Nugent, Jr., Dennis W. Jones, Michael J. Pawlik, Ralph C. Gray
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Patent number: 6183849Abstract: A quality composite board can be manufactured by combining natural fibrous material, resin and a waxy hydrocarbonaceous material wherein the waxy hydrocarbonaceous material is a natural, synthetic or petroleum wax containing from greater than 30 wt % to up to 98 wt % oil content.Type: GrantFiled: September 17, 1999Date of Patent: February 6, 2001Assignee: Exxon Research and Engineering CompanyInventors: Alan R. Lindsay, John A. Ciruna
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Patent number: 6159265Abstract: The object is to provide a powdered metal injection compacting composition adapted to give compacts free from deformation, cracking or blistering without being compromised in compactability or debinder characteristic and without the aid of a special jig.This composition comprises a metal powder and an organic binder comprising (A) a crystalline resin having a melting point of not less than 150.degree. C., (B) an organic compound the weight loss on heating of which begins at a temperature below 150.degree. C. and (C) a composite acrylic resin, the composite acrylic resin mentioned above being a resin obtainable by dispersing a solution comprising the following components (C1).about.(C3) in an aqueous medium containing a dispersant and carrying out a suspension polymerization reaction:(C1) an ethylene-vinyl acetate copolymer or an ethylene-ethyl acrylate copolymer,(C2) a (meth)acrylic ester monomer or a mixture of a (meth)acrylic ester monomer and a styrenic monomer, and(C3) a polymerization initiator.Type: GrantFiled: February 11, 2000Date of Patent: December 12, 2000Assignees: Dai-Ichi Kogyo Seiyaku Co., Ltd., Dai-Ichi Ceramo Ltd.Inventors: Hiromitsu Kinoshita, Tetsuo Shiraiwa, Hidetaka Uraoka, Nobuo Ochiai
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Patent number: 6133355Abstract: A novel thermopolymer material adapted for use in thermal stereolithography. More particularly, a thermopolymer material comprising a mixture of: a low shrinkage polymer resin; a low viscosity material such as paraffin wax; at least one microcrystalline wax; a toughening polymer; a plasticizer. Alternative embodiments further include components to improve the materials ability to transfer heat and to improve strength. The subject material, together with the described process greatly reduce part building distortions while retaining desirable toughness, strength and jetting properties.Type: GrantFiled: June 12, 1997Date of Patent: October 17, 2000Assignee: 3D Systems, Inc.Inventors: Richard N. Leyden, Charles W. Hull, Dinh Ton That
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Patent number: 6132665Abstract: Phase change compositions that are solid at ambient temperature and liquid at an elevated temperature above ambient temperature are disclosed for advantageous use in selective deposition modeling methods for building three-dimensional objects. A phase change composition according to the disclosed invention is a semi-crystalline component mixture having a freezing point of at least about 68.degree. C., a melting point of at least about 88.degree. C. and a viscosity of about 13 centipoise at 135.degree. C. The composition includes a plurality of waxes having a broad melting point range and molecular weight range. Three-dimensional objects having minimal curl, delamination and stress cracks can be produced at a faster rate than heretofore known by using selective deposition modeling techniques employing the disclosed compositions.Type: GrantFiled: February 25, 1999Date of Patent: October 17, 2000Assignee: 3D Systems, Inc.Inventors: Loc V. Bui, Vu Doan, Kelly Kwo
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Patent number: 6107430Abstract: Disclosed are hot melt adhesives comprising at least one first homogeneous linear etylene polymer having a particular density and melt viscosity at 350.degree.F. (177.degree.C.), and an optional wax and tackifier. In particular, disclosed is a hot melt adhesive characterized by: a) at least one homogeneous linear or substantially linear interpolymer of ethylene with at least ibe C.sub.2 --C.sub.20 .alpha.-olefin interpolymer having a density from 0.850 g/cm.sup.3 to 0.895 g/cm.sup.3 ; and b) optionally at least one tackifying resin; and c) optionally at least one wax wherein the hot melt adhesive has a viscosity of less than about 5000 cPs (50 grams/cm.second) at 150.degree.C. Preferred hot melt adhesives for use in adhering cardboard or paperboard are disclosed, as well as the resultant adhered products. Also disclosed is a dual reactor process for the preparation of the inventive hot melt adhesives.Type: GrantFiled: January 8, 1998Date of Patent: August 22, 2000Assignees: The Dow Chemical Company, H.B. Fuller Licensing & Financing Inc.Inventors: Robert A. Dubois, Cynthia L. Rickey, Steven W. Albrecht, Beth M. Eichler, Thomas F. Kauffman, Maynard Lawrence, Thomas H. Quinn
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Patent number: 6075090Abstract: The present invention is a method of making a stable colloidal non-aqueous wax particle dispersion. The method includes the steps of forming a mixture of a first vinyl monomer of a polymerizable mono-alpha, beta-ethylenically unsaturated compound free of ionic charge groups and capable of addition polymerization and a second vinyl monomer capable of addition polymerization and wax particle in a aqueous medum. The mixture is polymerized using an azo or diazo initiator to form an aqueous dispersion of composite wax particles. The wax particles are redispersed in an organic solvent.Type: GrantFiled: December 28, 1998Date of Patent: June 13, 2000Assignee: Eastman Kodak CompanyInventors: Yongcai Wang, James L. Bello, David E. Decker, Dennis E. Smith
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Patent number: 6068910Abstract: A polyester resin composition is calendered to produce a film or a sheet. The polyester resin composition is a polyester having a crystallization half time from a molten state of at least 5 minutes combined with an additive for preventing sticking of the polyester to calendering rolls.Type: GrantFiled: February 26, 1999Date of Patent: May 30, 2000Assignee: Eastman Chemical CompanyInventors: Paul Mary Flynn, Richard Leon McConnell, Hubertus Jacobus Wilhelmus Moolenaar, Timothy Michael Sanders
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Patent number: 6043298Abstract: A solid fritted bonding material consisting essentially of a blended wax composition and a powder is provided. The solid fritted bonding material is used to secure at least two articles together by applying the solid fritted bonding material to mating surfaces of each article; joing the mating surfaces of each article together; and heating the joined articles to a temperature wherein the blended wax composition burns away and the powder becomes activated to form a permanent bond between each article.Type: GrantFiled: January 21, 1998Date of Patent: March 28, 2000Inventor: David W. Prouse
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Patent number: 6040354Abstract: An impression composition which is based on an aziridine-free composition which can be vulcanized at room temperature, and which comprises wax is provided according to the invention. The wax increases the dimensional stability of the composition during mixing and curing. The invention furthermore provides a kit for the preparation of such compositions and a process for the preparation of the wax-containing components of these kits. The wax is dispersed throughout the composition and is prepared by shock-cooling. The wax forms a crystalline network.Type: GrantFiled: August 21, 1997Date of Patent: March 21, 2000Assignee: Ernst Muhlbauer KGInventors: Heijo Hubner, Dierk Lubbers, Wolfgang Muhlbauer
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Patent number: 6037396Abstract: A hot-melt ink for ink-jet recording comprises C.I. Solvent Yellow 162 or C.I. Solvent Blue 70 used as a colorant; four components (a) to (d) used as a medium, where the component (a) is selected from an amide resin, a C5 type synthetic petroleum resin, a C9 type synthetic petroleum resin and a C5-C9 type synthetic petroleum resin, the component (b) is a resin selected from a rosin resin, a terpene resin and a terpene phenol resin, the component (c) is a wax selected from a paraffin wax, a ketone wax and a polyethylene oxide wax and the component (d) is a wax selected from a monoamide wax and a diamide wax; and an antioxidant.Type: GrantFiled: March 24, 1998Date of Patent: March 14, 2000Assignee: Brother Kogyo Kabushiki KaishaInventor: Hidemasa Sawada
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Patent number: 6034158Abstract: This invention relates to a dispersions of polymeric colorants having poly(oxyalkylene) moieties mixed with unsubstituted sorbitan monooleate alone or ethoxylated dodecanol admixed with unsubstituted sorbitan monooleate. Such colorant dispersions are easy to handle and are effectively introduced into wax media, thereby providing significant improvements over other dyestuffs, pigments, and colorants.Type: GrantFiled: March 30, 1999Date of Patent: March 7, 2000Assignee: Milliken & CompanyInventors: Michael O. Hunt, John D. Bruhnke
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Patent number: 6028133Abstract: A phenolic resin modified with an alkali salt of sulfite or bisulfite in order to provide compatibility with a wax emulsion sizing agent, an adhesive prepared from the phenolic resin and wax emulsion, and the use of the adhesive in making bonded composites such as wood products, including, parallel strand lumber, oriented strand board (OSB), laminated veneer lumber (LVL), medium density fiberboard, wafer board and particle board, and textile products.Type: GrantFiled: March 20, 1998Date of Patent: February 22, 2000Assignee: Georgia-Pacific Resins, Inc.Inventors: Brian M. Peek, Barry W. Sewell
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Patent number: 6025431Abstract: The present invention relates to thickened personal care compositions which utilize a thickening amount of an acrylate-based polymeric rheology modifier prepared by polymerization of a C.sub.1 -C.sub.6 alkyl ester of acrylic acid and/or a C.sub.1 -C.sub.6 alkyl ester of methacrylic acid, a monomer chosen from a vinyl-substituted heterocyclic compound containing at least one of a nitrogen or sulfur atom, (meth)acrylamide, a mono- or di-(C.sub.1 -C.sub.4)alkylamino (C.sub.1 -C.sub.4)alkyl (meth)acrylate, a mono or di-(C.sub.1 -C.sub.4)alkylamino (C.sub.1 -C.sub.4)alkyl (meth)acrylamide, and, optionally, an associative monomer.Type: GrantFiled: March 17, 1997Date of Patent: February 15, 2000Assignee: National Starch and Chemical Investment Holding CorporationInventors: Martin S. Cardinali, Daniel W. Verstrat
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Patent number: 6022910Abstract: A hot-melt solid ink composition comprises at least one polyamide and at least one terpene resin. The terpene resin is present in an amount of from 0.5% by weight to 15% by weight based on the total weight of the ink composition. This hot-melt solid ink composition can be stable to heat upon recording using ink-jet recording apparatus where ink is heated to melt at a temperature higher than ordinary temperature to make a record, and has a superior transparency and a superior adhesion to printing mediums.Type: GrantFiled: November 21, 1997Date of Patent: February 8, 2000Assignee: Brother Kogyo Kabushiki KaishaInventors: Masahiro Nishizaki, Naomichi Kobayashi
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Patent number: 6022918Abstract: The present invention relates to a wire enamel formulation comprising components which are known per se and an internal lubricant consisting of a polyethylene wax, preferably having a molecular mass of from 3000 to 6000 g/mol, and a wetting agent, preferably fatty alcohol ethoxylate.Type: GrantFiled: January 13, 1998Date of Patent: February 8, 2000Assignee: BASF Coatings AGInventors: Klaus-Wilhelm Lienert, Irmgart Gebert, Helmut Lehmann, Michael W. Muller
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Patent number: RE36754Abstract: Hot-melt silicone pressure sensitive adhesive compositions containing organic waxes, methods of using the compositions and devices made using the compositions are disclosed. The hot-melt silicone pressure sensitive adhesive compositions include a mixture of (i) a silicate resin, (ii) a silicone fluid, and (iii) an organic wax having a melting point of between 30.degree. C. and 150.degree. C. The organic wax decreases dynamic viscosity of the adhesive at temperatures equal to or below about 200.degree. C.Type: GrantFiled: June 6, 1996Date of Patent: June 27, 2000Assignee: Dow Corning CorporationInventor: Ross Alan Noel