Oxidation Of Impurities Patents (Class 554/181)
  • Publication number: 20140135514
    Abstract: Vegetable oils having a low level of glycidol esters are disclosed.
    Type: Application
    Filed: December 20, 2013
    Publication date: May 15, 2014
    Applicant: Archer Daniels Midland Company
    Inventors: Phil Hogan, John Inmok Lee, Mark Matlock, Leif Solheim, Lori E. Wicklund
  • Patent number: 7989647
    Abstract: A method for producing a vegetable oil-derived polyol having increased hydroxyl functionality by reacting a vegetable oil with an oxidizing agent in the presence of an organometallic catalyst is provided. The resulting higher functionality polyols derived from vegetable oil produced by the process are also provided. Also provided is a method for decreasing the acid value of a vegetable oil-derived polyol by reacting the vegetable oil-derived polyol with an epoxide component in the presence of a Lewis base catalyst. Urethane products produced using higher functional vegetable oil-derived polyols and/or lower acid vegetable oil-derived polyols are also provided.
    Type: Grant
    Filed: March 3, 2006
    Date of Patent: August 2, 2011
    Assignee: South Dakota Soybean Processors, LLC
    Inventors: Eric J. Geiger, Nicole M. Becker, Lawrence A. Armbruster
  • Patent number: 7262311
    Abstract: A method for partially refining a crude vegetable oil utilizing physical refining techniques is described. The crude vegetable oil is first degummed by either (1) allowing the crude oil to settle over a period of time, such as twenty days, so that the oil becomes stratified into at least two layers, wherein one layer comprises gums with low oil content and a second layer comprises oil containing only a fraction of the gums originally present and then separating the oil layer from the gum layer, or (2) heating the crude oil to a temperature of about 270-300° F. with agitation and then allowing the crude oil to settle for a period of time until the oil becomes stratified into the at least two layers. The degummed oil is then aerated and agitated while being maintained at a temperature of 170-180° F. for a time period sufficient to obtain a desired oil viscosity. The resulting partially refined oil is suitable for use in industrial applications such as the preparation of urethane foams.
    Type: Grant
    Filed: April 29, 2004
    Date of Patent: August 28, 2007
    Assignee: South Dakota Soybean Processors
    Inventors: Rodney Christianson, Michael Noble, Andrew Rourke, Eric Geiger, Larry Mahlum
  • Patent number: 6759542
    Abstract: A method for partially refining a crude vegetable oil utilizing physical refining techniques is described. The crude vegetable oil is first degummed by either (1) allowing the crude oil to settle over a period of time, such as twenty days, so that the oil becomes stratified into at least two layers, wherein one layer comprises gums with low oil content and a second layer comprises oil containing only a fraction of the gums originally present and then separating the oil layer from the gum layer, or (2) heating the crude oil to a temperature of about 270-300° F. with agitation and then allowing the crude oil to settle for a period of time until the oil becomes stratified into the at least two layers. The degummed oil is then aerated and agitated while being maintained at a temperature of 170-180° F. for a time period sufficient to obtain a desired oil viscosity. The resulting partially refined oil is suitable for use in industrial applications such as the preparation of urethane foams.
    Type: Grant
    Filed: November 4, 2002
    Date of Patent: July 6, 2004
    Assignee: South Dakota Soybean Processors
    Inventor: Larry Mahlum
  • Patent number: 6476244
    Abstract: A method for partially refining a crude vegetable oil utilizing physical refining techniques is described. The crude vegetable oil is first degummed by either (1) allowing the crude oil to settle over a period of time, such as twenty days, so that the oil becomes stratified into at least two layers, wherein one layer comprises gums with low oil content and a second layer comprises oil containing only a fraction of the gums originally present and then separating the oil layer from the gum layer, or (2) heating the crude oil to a temperature of about 270-300° F. with agitation and then allowing the crude oil to settle for a period of time until the oil becomes stratified into the at least two layers. The degummed oil is then aerated and agitated while being maintained at a temperature of 170-180° F. for a time period sufficient to obtain a desired oil viscosity. The resulting partially refined oil is suitable for use in industrial applications such as the preparation of urethane foams.
    Type: Grant
    Filed: February 21, 2001
    Date of Patent: November 5, 2002
    Assignee: South Dakota Soybean Processors
    Inventor: Larry Mahlum
  • Patent number: 5371254
    Abstract: This invention relates to a new process for refining and deodorizing the oil from the seeds of the neem tree by refining a neem oil solution with an alkaline solution of hydrogen peroxide to provide an edible grade of vegetable oil.
    Type: Grant
    Filed: July 27, 1992
    Date of Patent: December 6, 1994
    Assignee: Rohm and Haas Company
    Inventor: Zev Lidert
  • Patent number: 5312935
    Abstract: Fluorinated carboxylic acids which do not have the required purity for use as emulsifier in the polymerization of fluorinated monomers can, if necessary after prior de-watering, be treated with oxidants, whereupon the isolation of the pure product is carried out by crystallisation or, preferably, by distillation.
    Type: Grant
    Filed: April 21, 1993
    Date of Patent: May 17, 1994
    Assignee: Hoechst Aktiengesellschaft
    Inventors: Ludwig Mayer, Gernot Lohr
  • Patent number: 5256613
    Abstract: The present invention relates to a process for the regeneration of spent bleaching earth, comprising an oxidative heat treatment in which the amount of oxygen supplied exceeds the stoichiometrical requirement of complete oxidation of all organics present in the spent bleaching earth, wherein the spent bleaching earth and the oxygen are blown through a stationary fluidized bed of inert granulate material. The stationary fluidized bed should be as high as to limit the temperature in the freeboard to less than 1000.degree. C. As a matter of fact, it has been found that, if the fluidized bed is not high enough, the oxygen required to burn off the organics content of the spent bleaching earth would blow out the powdered bleaching earth from the bed at the stage of incomplete oxidation of the organics present on the earth, resulting in an uncontrolled temperature rise in the freeboard and local overheating of the bleaching earth.
    Type: Grant
    Filed: August 27, 1992
    Date of Patent: October 26, 1993
    Assignee: N.V. Vandemoortele International
    Inventors: Pieter J. A. Maes, Albert J. Dijkstra
  • Patent number: 5183911
    Abstract: Production of stable ozonized oils from unsaturated vegetable oils by introducing an ozone-oxygen mixture into the oil until it reaches saturation, and following the ozonization, an extraction process in acid medium is carried out in the presence of a redox reaction system, which is capable of moderately reacting the radicals in the presence of a synthetic or natural anti-oxidation medium or reducing medium.
    Type: Grant
    Filed: April 6, 1992
    Date of Patent: February 2, 1993
    Assignee: Dr. J. Hansler GmbH
    Inventors: Josef Washuttl, Renate Viebahn