Patents Represented by Attorney, Agent or Law Firm Daniel S. Ortiz
  • Patent number: 6447665
    Abstract: Anodized aluminum surfaces are advantageously sealed by an energy- and time-saving two step process, in which the first step is contact at not more than 75° C. with a solution containing lithium and fluoride ions and, optionally, surfactant. The second necessary step is treatment with hot water or steam, which may be completed in considerably less time when only hot water or steam is used for sealing. Conventional smut inhibitors and/or neutral buffers as used in hot water for single step sealing may advantageously be included in the second step of this process. 100-1000 ppm concentrations of nickel and/or cobalt ions in the treatment liquid for the second treatment step, if environmentally tolerable, make it possible to complete this step in as little as 10 minutes at a temperature as low as 88° C.
    Type: Grant
    Filed: May 17, 2000
    Date of Patent: September 10, 2002
    Assignee: Henkel Corporation
    Inventors: Philip M. Johnson, Lawrence R. Carlson, Scott A Wojciechowski
  • Patent number: 6448338
    Abstract: Hot-pumpable, heat-curing compositions based on solid ethylene/vinyl acetate copolymers and liquid reactive plasticizers containing olefinically unsaturated double bonds and at least one peroxidic crosslinking agent are suitable as sealing compounds for sealing fine and rough seams in vehicle manufacture. By adding expanding agents, the compositions may be used as lining adhesives. The preferred applications are at the white-shell stage of car manufacture.
    Type: Grant
    Filed: March 28, 2000
    Date of Patent: September 10, 2002
    Assignee: Henkel Teroson GmbH
    Inventors: Peter Born, Klaus Hoellriegel
  • Patent number: 6440231
    Abstract: A process for the production of a rubber-to-metal bond on steel, galvanized steel, aluminum and/or magnesium is provided The process comprises at least the following steps: a) chemical pretreatment of the metal parts, b) intermediate rinsing, and c) vulcanizing-on of natural or synthetic rubber using primers and/or binders. The chemical pretreatment in step a) is carried out with an aqueous solution with a pH value of 3.5 to 5.5 which contains: 4 to 20 g/l of phosphate ions, 0.1 to 1 g/l of free or complexed fluoride, and 0.04 to 1 g/l of nitrate ions.
    Type: Grant
    Filed: July 19, 1996
    Date of Patent: August 27, 2002
    Assignee: Henkel Kommanditgesellschaft auf Aktien
    Inventors: Wolf-Dieter Beiersdorf, Werner Gruber, Hans Scheer, Juergen Foell, Birgit Gies, Peter Kuhm, Franz-Josef Schueller
  • Patent number: 6432237
    Abstract: The uneven surfaces of wood-based materials such as chipboard may be improved by applying a formable coating material, smoothing and/or modelling the coating material to achieve a smoother surface, and heating the coating material to form closed pores while maintaining the smoothed surface intact.
    Type: Grant
    Filed: February 19, 1999
    Date of Patent: August 13, 2002
    Assignees: Henkel Kommanditgesellschaft auf Aktien, Dorus Klebetechik GmbH and Co. KG
    Inventors: Rainer Hasenkamp, Lothar Thiele
  • Patent number: 6432899
    Abstract: Cleaning and deoxidizing aluminum surfaces can be accomplished simultaneously by contacting the surfaces with an aqueous liquid composition that contains as its cleaning active ingredients (i) alcohols and/or ether alcohols, (ii) alkaline builders, and (iii) alkali stable surfactants, and, optionally but preferably, also contains fluoride and chelating agents.
    Type: Grant
    Filed: July 13, 2000
    Date of Patent: August 13, 2002
    Assignee: Henkel Corporation
    Inventor: Terry D. Sjostrom
  • Patent number: 6425955
    Abstract: Aqueous alkaline cleaning solutions are used to remove metal intermediate length carboxylate salts from a solid substrate. Foaming of the aqueous alkaline cleaning solution can be adequately reduced by treating the anions of the metal intermediate length carboxylate salts with cations. The anions of the metal intermediate length carboxylate salts constitute a separate solid phase layer that be readily separated from the cleaning solution, resulting in a regenerated aqueous alkaline cleaning solution.
    Type: Grant
    Filed: April 26, 2000
    Date of Patent: July 30, 2002
    Assignee: Henkel Corporation
    Inventors: Kenneth J. Hacias, Richard J. Church
  • Patent number: 6379474
    Abstract: An acidic aqueous phosphating solution is presented having 0.2 to 3 g/l of zinc ions, 3 to 50 g/l of phosphate ions expressed as PO4−3, and 0.05 to 4 g/l of an organic N-oxide containing a saturated, unsaturated or aromatic 5- or 6-membered ring system, where the N atom of the N-oxide is part of said ring system, and where the ratio by weight of phosphate ions to zinc ions is from 3.7 to 30:1. The solution is free of hydroxylamine and useful in phosphating metal surfaces.
    Type: Grant
    Filed: January 10, 2001
    Date of Patent: April 30, 2002
    Assignee: Henkel Kommanditgesellschaft auf Aktien
    Inventors: Bernd Mayer, Peter Kuhm, Pietro Balboni, Markus Senner, Horst-Dieter Speckmann, Juergen Geke, Jan-Willem Brouwer, Annette Willer
  • Patent number: 6371993
    Abstract: The invention relates to the utilization of onium aldehydes and onium ketones of formula (1) or the derivatives thereof. In the formula, R1 represents a hydrogen atom, a (C1-C4)-alkyl group, an aryl group or a heteroaryl group. R2, R3, R4, independent of one another, each represent a hydrogen atom, a halogen atom, a (C1-C4)-alkyl group, a (C1-C4)-alkoxyl group, hydroxy-(C1-C4)-alkoxyl group, hydroxyl group, nitro group, aryl group, trifluoromethyl group, amino group or (C1-C4)-acyl group. Said amino group can be substituted by (C1-C4)-alkyl groups. Two of the residuals can be combined to form a fused benzene ring. R5 represents a (C1-C4)-alkyl group, aryl group, alkylaryl group or heteroaryl group.
    Type: Grant
    Filed: June 19, 2000
    Date of Patent: April 16, 2002
    Assignee: Henkel Kommanditgesellschaft auf Aktien
    Inventors: Hinrich Moeller, Horst Hoeffkes
  • Patent number: 6359023
    Abstract: Described is an NCO-group-containing polyurethane prepolymer madefrom polyisocanyates and polyols derived from natural oils. The invention is characterized in that the polyol is obtained by transesterification in the presence of basic lithium compounds. Together with a tertiary amine used to accelerate the moisture curing, the storage stability is thus increased considerably. Up to 4.0 mmol of the lithium compound is used per kilogram of polyol, and 0.1 to 2.0% by wt. of the amine, relative to the total weight of the composition, is used as the accelerator. The polyurethane prepolymer is suitable not only for the production of adhesives but also for the production of foamed materials, in particular those dispensed from throw-away pressure vessels.
    Type: Grant
    Filed: February 10, 1998
    Date of Patent: March 19, 2002
    Assignee: Henkel Kommanditgesellschaft auf Aktien
    Inventors: Hermann Kluth, Wolfgang Klauck, Johann Klein, Wilfried Huebner
  • Patent number: 6303672
    Abstract: A self-dispersing curable epoxy composition is prepared upon contacting an epoxy resin with a polyoxyalkylenemonoamine having a molecular weight of from about 3,000 to about 15,000 in a ratio of about 0.001 to 0.060 reactive equivalents of polyoxyalkylenemonoamine to about 1.0 reactive equivalents of epoxy resin. The self-dispersing curable epoxy resin forms an aqueous dispersion upon mixing with water. When cured, the dispersion is useful as a coating composition.
    Type: Grant
    Filed: June 7, 1995
    Date of Patent: October 16, 2001
    Assignee: Henkel Corporation
    Inventors: John G. Papalos, Shailesh Shah, Reuben H. Grinstein, Joseph L. Mulvey, Brian G. Jewell
  • Patent number: 6294596
    Abstract: A self-dispersing curable epoxy composition is prepared upon contacting an epoxy resin with a polyoxyalkyleneamine having a molecular weight of from about 3,000 to about 15,000 in a ratio of about 0.001 to 0.060 reactive equivalents of polyoxyalkyleneamine to about 1.0 reactive equivalents of epoxy resin. The self-dispersing curable epoxy resin forms an aqueous dispersion upon mixing with water. When cured, the dispersion is useful as a coating composition.
    Type: Grant
    Filed: September 15, 1995
    Date of Patent: September 25, 2001
    Assignee: Henkel Corporation
    Inventors: John G. Papalos, Shailesh Shah, Reuben H. Grinstein, Joseph L. Mulvey, Brian G. Jewell
  • Patent number: 6238509
    Abstract: The invention relates to an adhesive system for labeling containers, more especially hollow containers, with wrap-around labels. The adhesive system comprises a pick-up adhesive and an overlap adhesive. It is characterized in that, in the wet state, the pick-up adhesive has sufficient wet bond strength for labeling and, in the dried state, does not adhere to at least one of the substrates. The pickup adhesive contains 5 to 85% by weight and preferably 5 to 60% by weight of at least one water-soluble polymer based on casein, starch, dextrin, glucose, polyvinyl alcohol, polyurethane or polyacrylic acid, 0.00 to 1.00% by weight and preferably 0.01 to 0.30% by weight of at least one defoamer, 0.00 to 1.00% by weight and preferably 0.01 to 0.30% by weight of at least one preservative and water as the balance to 100% by weight.
    Type: Grant
    Filed: December 15, 1997
    Date of Patent: May 29, 2001
    Assignee: Henkel Kommanditgesellschaft auf Aktien
    Inventors: Bernhard Herlfterkamp, Hermann Onusseit, Horst Buxhofer, Ludwig Broich, Ralf Grauel, Jan Auris
  • Patent number: 6228833
    Abstract: Scent intensifying washing and cleaning detergents or components for these detergents are manufactured in which a solid and essentially water-free premix is produced, said premis being comprised of washing and cleaning detergent compounds and/or washing and cleaning detergent materials. The premix contains at least 0.1 wt. % perfume referring to the premix and is subjected to granulation or compacted agglomeration. By virtue of the water-free method, subsequent drying steps do not apply in which the prefume is entirely or partially vaporized. The homogenous incorporation of the prefume leads to a substantially increased fragrance of both the product as well as the articles which are dampened or dried, especially textiles.
    Type: Grant
    Filed: August 7, 2000
    Date of Patent: May 8, 2001
    Assignee: Henkel Kommanditgesellschaft Auf Aktien
    Inventors: Kathleen Paatz, Wolfgang Lahn
  • Patent number: 6221827
    Abstract: The invention relates to new bleaching and disinfecting compositions containing—based on the composition (a) 1 to 8% by weight of alkali metal hypochlorites, (b) 0.1 to 2% by weight of alkali metal hydroxides, (c) 0.1 to 2% by weight of betaines, (d) 0.1 to 1% by weight of hydrotropes and (e) 0.05 to 1% by weight of sequestrants, with the proviso that the quantities add up to 100% by weight with water and optionally other auxiliaries and additives. The clear compositions are viscoelastic and show inter alia high stability in storage in addition to excellent washing and bleaching performance.
    Type: Grant
    Filed: December 17, 1999
    Date of Patent: April 24, 2001
    Assignee: Henkel Kommanditgesellschaft auf Aktien
    Inventors: Mercedes Mendoza Cruz, Elisabet de Jorge
  • Patent number: 6197731
    Abstract: Ester base stocks for two-cycle gasoline engine lubricant compositions are disclosed which produce lower amounts of observable smoke in the exhaust emitted as a result of combustion in a two-cycle gasoline engine, require no miscibility-enhancing solvents, have a viscosity of 3.0 cSt to 20.0 cSt at 100° C. and a smoke index of at least 75. Some of the esters are biodegradable.
    Type: Grant
    Filed: May 17, 1999
    Date of Patent: March 6, 2001
    Assignee: Henkel Corporation
    Inventors: Eugene R. Zehler, Bruce J. Beimesch
  • Patent number: 6197126
    Abstract: The invention is a process for applying a nickel-free, copper-containing phosphate coating to a metal surface by contacting the metal surface with a phosphate solution containing 0.2 to 2.0 g/l zinc ions, 0.5 to 25 mg/l copper ions, and 5-30 g/l phosphate ions.
    Type: Grant
    Filed: September 30, 1994
    Date of Patent: March 6, 2001
    Assignee: Henkel Kommanditgesellschaft auf Aktien
    Inventors: Wolf-Achim Roland, Karl-Heinz Gottwald, Matthias Hamacher, Jan-Willem Brouwer
  • Patent number: 6187731
    Abstract: Naphthalene sulfonic acid/formaldehyde condensates (i) may be used in a composition for cleaning hard surfaces to reduce the rain effect and/or the film effect, (ii) may be present in a cleaning composition for hard surfaces in combination with one or more other anionic and/or nonionic surfactants and (iii) may be used in a process for reducing the rain effect and/or the film effect on a hard surface treated with a liquid cleaning composition, the surface being treated with a liquid cleaning composition in concentrated or diluted form containing one or more naphthalene sulfonic acid/formaldehyde condensates.
    Type: Grant
    Filed: December 22, 1999
    Date of Patent: February 13, 2001
    Assignee: Henkel Kommandigesellschaft Auf Aktien (KGaA)
    Inventors: Thomas Moeller, Heinz-Dieter Soldanski, Stefanie Kuech, Juergen Noglich
  • Patent number: 6180172
    Abstract: A process and apparatus for edge coating a substrate is provided. A process provides a layer of a formable coating material on a transfer belt which layer of formable material has a variable thickness over the width of the layer, applying a layer of the formable coating material on the transfer belt to the edge surface to produce a coated edge surface and smoothing the coated edge surface by contact with a smoothing belt. The coating on the edge surface is sufficiently thick to cover and smooth irregularities in the edge surface of the substrate. The coated edge surface can be further treated by the usual methods for coating edge surfaces of flat substrates. The apparatus comprises the roller or nozzle to provide the layer of formable material of variable thickness on the transfer belt, the transfer belt carries the coating material to the edge surface and the transfer belt can act as a smoothing belt to provide an edge surface with the coating material with all of the irregularities obscured.
    Type: Grant
    Filed: May 29, 1997
    Date of Patent: January 30, 2001
    Assignee: Henkel Kommanditgesellschaft auf Aktien
    Inventors: Rainer Hasenkamp, Wigand Staehlin
  • Patent number: 6162839
    Abstract: A composition for producing light plaster contains as main constitutive elements particles of plaster in anhydride or hemihydrate form and at least one foaming agent. The composition is characterized in that the foaming agent generates gas after a delay of 1 minute to 24 hours and constitutes 0.1 to 50% by weight of the total dry mixture. Also disclosed is the use of said composition to produce in-situ cellular plastic and low density plaster moldings.
    Type: Grant
    Filed: August 11, 1998
    Date of Patent: December 19, 2000
    Assignee: Henkel Kommanditgesellschaft auf Aktien
    Inventors: Wolfgang Klauck, Hermann Kluth, Wilfried Huebner, Felicitas Kolenda
  • Patent number: 6138853
    Abstract: A portable container for fuel is provided which has a sealable opening sufficiently large to permit access to the interior for a swab or cleaning device to wipe or vacuum the interior of the container.
    Type: Grant
    Filed: July 18, 1997
    Date of Patent: October 31, 2000
    Inventor: Ronald J. Frechette