Abstract: A castable refractory composition comprising: (a) 50-90 vol. % coarse particulates having a particle size between about 1 and 60 mm; and (b) 10-40 vol. % fine filler materials having a particle size distribution of between 0.0001 to 3 mm.

Abstract: A process for fabricating an aluminum alloy rolled sheet particularly suitable for use for an automotive body, the process comprising: (a) providing a body of an alloy comprising: about 0.8 to about 1.5 wt. % silicon, about 0.15 to about 0.65 wt. % magnesium, about 0.00 to about 0.1 wt. % copper, about 0.01 to about 0.1 wt. % manganese, about 0.05 to about 0.3 wt. % iron; and the balance being substantially aluminum and incidental elements and impurities; (b) working the body to produce a the sheet; (c) solution heat treating the sheet; and (d) rapidly quenching the sheet. In a preferred embodiment, the solution heat treat is preformed at a temperature greater than 460.degree. C. and the sheet is quenched by a water spray. The resulting sheet has an improved combination of formability, strength and corrosion resistance.

Abstract: A method is disclosed of making a braze sheet for a brazed assembly. The method includes the steps of providing a sheet of a core material and a composition cladding and mechanically embedding a flux into the sheet.

Abstract: Disclosed is a method of making lithium-containing aluminum base alloy extrusion having at least a section thereof having a low aspect ratio or which is generally axisymmetrical, the extrusions having improved properties in sections thereof having the low aspect ratio or which are axisymmetrical. The method comprises providing a body of a lithium-containing aluminum alloy, pressing a portion of the body which is to form the axisymmetrical or low aspect ratio section through a tortuous path and extruding an axisymmetrical or a low aspect ratio extrusion section. The axisymmetrical or low aspect ratio section of the extrusion has a tensile strength of at least 60 ksi and an ultimate yield strength at least 4.5 ksi greater than the tensile yield strength.

Abstract: A novel product composed of a ceramic phase particle dispersoid in metal, including uniformly distributed, finely sized carbide phase particles formed in situ in a molten metal and a novel method for producing such a ceramic phase particle dispersoid in metal are disclosed. A salt-based liquid state reaction involving a liquid metal/alloy containing a liquid Ti, B, Si, Sc, Hf, Nb, Ta, Zr, Mo, Al (when the molten metal matrix is not aluminum), or V and a halide salt containing carbon particles forms a uniform distribution of finely sized ceramic phase particles formed and dispersed in-situ in the metal matrix. The ceramic dispersoid in metal product of the present invention includes at least about 50 volume percent of a matrix metal of aluminum; and up to about 50 volume percent of a uniform distribution of finely sized ceramic phase particles formed and dispersed in-situ in the aluminum metal matrix, wherein the finely sized ceramic phase particles have an average particle diameter of less than about 2.

Abstract: An aluminum alloy containing dispersoid-forming elements selected from the group consisting of Zr, Mn, Cr, V, Hf, Ti, Nb, Y, Sc and combinations thereof. The improved alloy comprises the dispersoid-forming elements partially in solid solution above the saturation limit and partialy in a form of aluminide particles having an average particle size of less than 1 micron.

Abstract: A novel method for producing a ceramic phase particle dispersoid in metal and a novel product composed thereof. The method includes (a) providing a molten composition consisting essentially of molten aluminum alloy containing molten metal selected from the group consisting of Zr, V and combinations thereof, (b) providing a chloride salt containing fine carbon particles; and (c) reacting the chloride salt containing fine carbon particles in the molten aluminum metal with the molten metal to form a uniform distribution of finely sized carbide particles formed and dispersed in-situ in an aluminum alloy matrix.

Abstract: A method of fabricating a plurality of multilayer structures which includes at least one recess defined by a nonplanar surface. The method including the steps of: (a) providing a resilient, compliant material on over one or more stacks of layers including the area over the recess; (b) applying sufficient pressure to the stacks to cause the resilient, compliant material to fill the recess and laminate said stacks; (c) lifting the resilient, compliant material off the stack subsequent to the application of pressure; (d) providing one or more stacks of layers that have not been subjected to step (b); and (e) repeating steps (a)-(d). In a preferred embodiment of the invention steps (a)-(d) are repeated at least ten times without the need to change the resilient compliant material. In a most preferred embodiment of the invention steps (a)-(d) are repeated at least one hundred times.

Abstract: Methods for making an aluminum drive shaft for automobiles or trucks or other drive shaft applications from aluminum alloy tube and methods for making drive shafts. The method includes providing an aluminum tube member is joined to drive shaft end members. The method includes the steps of (a) providing a 6000 series type alloy; (b) extruding the alloy within about 500.degree. to 800.degree. F. into a hollow elongate tube; (c) drawing the tube to a reduction of at least 15% in metal cross-sectional area; (d) solution heat treating the alloy at a temperature of at least about 990.degree. F. and then quenching; and (e) reducing the diameter of the tube and increasing the tube wall thickness to provide a relatively short tube length of reduced diameter, a transition section and thicker wall thickness at one or both ends of a drive shaft suitable length of said tube. The transition section has a non-linear wall. In a preferred embodiment, the transition section has central circumferential stiffener section.

Abstract: A novel aluminum-lithium negative electrode and method for making such a novel aluminum-lithium negative electrode, including providing an admixture of aluminum powder and lithium halide electrolyte salts to form an aluminum lithium halide mixture, pressing the aluminum lithium halide mixture to form an aluminum lithium halide mixture negative electrode, placing the aluminum lithium halide mixture negative electrode next to a separate electrode composed of MgO and lithium halide electrolyte salts, providing a positive electrode of iron sulfide, lithium carbonate, and carbon, assembling the electrodes into a battery, and reacting lithium carbonate, carbon, and aluminum in situ in the battery to form an aluminum-lithium alloy negative electrode.

Abstract: A process for fabricating an aluminum alloy rolled sheet particularly suitable for use for an automotive body, the process comprising: (a) providing a body of an alloy comprising: about 0.8 to about 1.5 wt. % silicon, about 0.15 to about 0.65 wt. % magnesium, about 0.00 to about 0.1 wt. % copper, about 0.01 to about 0.1 wt. % manganese, about 0.05 to about 0.3 wt. % iron; and the balance being substantially aluminum and incidental elements and impurities; (b) working the body to produce a the sheet; (c) solution heat treating the sheet; and (d) rapidly quenching the sheet. In a preferred embodiment, the solution heat treat is preformed at a temperature greater than 460.degree. C. and the sheet is quenched by a water spray. The resulting sheet has an improved combination of formability, strength and corrosion resistance.

Abstract: A novel fixed block polarized, specular reflective accessory apparatus and method are disclosed, including providing an infrared light generator, a polarizer to polarize infrared light generated by the infrared light generator, a fixed block having an aperture for receiving a sample, a first fixed position mirror on one side of the fixed block wherein the first fixed position mirror is positioned to receive incident infrared light parallel to the plane of reflection at a fixedly set angle, and a second fixed position mirror positioned to receive infrared light reflected from said sample. In one aspect, the fixedly set angle preferably is fixed at about 55.degree.. The novel fixed block polarized, specular reflective accessory apparatus and method provide a high efficiency, high accuracy, high quality and quantitative process control coating measurements for coating operations in manufacturing coated aluminum alloy sheet.

Abstract: A method for manufacturing a reinforced cementitious columnar structure comprising: (a) providing a mold having a cavity which corresponds to a shape and size of the columnar structure; (b) filling the cavity with dry coarse particulates to form a formed dry body comprising 50-90 volume percent coarse particulates having a particle size between about 1 and 60 mm so as to form a core volume; (c) introducing a slurry of cementitious material containing an amount of fine material which has been determined beforehand, the fine material having a particle size smaller than the size of interstitial voids of the coarse particulates into the core volume, the fine material and the cementitious material filling the core volume and the cementitious material infiltirating and encapsulating the coarse particulates, and the fine material remaining within the core volume; (d) curing the slurry of cementitious material to form the reinforced cementitious columnar structure; and (e) separating the mold from the reinforced ceme

Abstract: A method of quenching a metal object having steps of: (a) providing a liquid coolant having a temperature from about 100.degree. F. to about 180.degree. F. and containing about 0.01 to about 0.1 standard cubic feet of carbon dioxide gas per gallon of water dissolved therein; and (b) spraying the liquid coolant on the metal object to quench the metal object.

Abstract: A method is disclosed for treating an aluminum alloy product in order to impart a fine grain structure and thereby improve formability and surface finish characteristics. According to this method, the product is first heated to a first temperature high enough to dissolve soluble constituent phase particles into solid solution. The product is maintained at this first temperature long enough to dissolve a major portion of the soluble constituent phase particles. Thereafter, the product is subjected to a controlled cooling process. The product is first cooled from the first temperature, at a first rate that is rapid enough to minimize the precipitation of coarse-grained constituent phase particles, to a second temperature that is below the temperature at which such coarse-grained constituent phase particles will precipitate out. Then, the product is cooled from the second temperature, at a second rate that is within a range of about 1-300 degrees F. per hour, to a third temperature that is at least 50 degrees F.

Abstract: A novel gelation-resistant alumina and process for producing such a product and aqueous slurries composed thereof are disclosed, including grinding aluminum oxide of .alpha.-Al.sub.2 O.sub.3 in the presence of about 0.5 to 3.0 wt. % water. The grinding preferably is performed in a sealed ball mill. Dual phase alumina particles have an aluminum oxide inner core of .alpha.-Al.sub.2 O.sub.3 and an aluminum oxide hydroxide outer phase of .gamma.-AlOOH on the .alpha.-Al.sub.2 O.sub.3, including to a nominal depth, e.g., by way of example, of about 5 to 100 nanometers on the inner core of .alpha.-Al.sub.2 O.sub.3, and having up to 40% higher surface area than the initial aluminum oxide of .alpha.-Al.sub.2 O.sub.3. The novel gelation-resistant alumina can be dispersed in an aqueous slurry having a solids content of 65 wt. % and higher, and the resulting slurry has significantly extended shelf life.

Abstract: Metal matrix composites are manufactured in a vacuum die casting machine. Solid aggregate material is placed in a die, the die is evacuated, and molten metal is driven by a piston to infiltrate the solid aggregate material where it subsequently solidifies to form a metal matrix composite.

Abstract: A novel method for producing a ceramic phase particle dispersoid in metal and a novel product composed thereof are disclosed, including finely sized carbide phase particles formed in situ in a molten metal by salt-based liquid state reaction with Ti, B, Si, Sc, Hf, Nb, Ta, Zr, Mo, Al (when the molten metal matrix is not aluminum), or V and a halide salt containing carbon particles to form a uniform distribution of finely sized ceramic phase particles formed and dispersed in-situ in the metal matrix. The step of reacting includes vigorously stirring to form a reaction mixture at an elevated temperature for a residence time less than one hour to form a uniform distribution of particles sized less than 2.5 microns uniformly dispersed in-situ in the metal matrix.

Abstract: A novel gelation-resistant alumina and process for producing such a product and aqueous slurries composed thereof are disclosed, including grinding aluminum oxide of .alpha.-Al.sub.2 O.sub.3 in the presence of about 0.5 to 3.0 wt. % water. The grinding preferably is performed in a sealed ball mill. Dual phase alumina particles have an aluminum oxide inner core of .alpha.-Al.sub.2 O.sub.3 and an aluminum oxide hydroxide outer phase of .gamma.-AlOOH on the .alpha.-Al.sub.2 O.sub.3, including to a nominal depth, e.g., by way of example, of about 5 to 100 nanometers on the inner core of .alpha.-Al.sub.2 O.sub.3, and having up to 40% higher surface area than the initial aluminum oxide of .alpha.-Al.sub.2 O.sub.3. The novel gelation-resistant alumina can be dispersed in an aqueous slurry having a solids content of 65 wt. % and higher, and the resulting slurry has significantly extended shelf life.

Abstract: A method of quenching a metal object comprising: (a) providing a reservoir of liquid coolant containing gas that has been dissolved therein; and (b) immersing the metal object in the reservoir to quench the metal. The gas is selected from the group consisting of nitrogen and carbon dioxide and is preferably carbon dioxide. The gas is preferably maintained within the range of 0.001 to 0.2 standard cubic feet of gas per gallon of coolant. The liquid coolant is preferably water. In a preferred embodiment, the reservoir of liquid coolant is open to ambient pressure and temperature.