Abstract: A composition is disclosed of a metal acetylacetonate, a resinous carrier, and a solvent. The composition is applied to a portion of an electrical apparatus which is exposed to a gas stream. The solvent in the composition is evaporated to produce a thermoparticulating coating. When the electrical apparatus overheats the metal acetylacetonate in the coating forms particles in the gas stream which are detected by a monitor.

Abstract: A composition is disclosed of malonic acid, a resinous carrier, and a solvent. The composition is applied to a portion of an electrical apparatus which is exposed to a fluid stream. The solvent in the composition is evaporated to produce a thermo-particulating coating. When the electrical apparatus overheats the malonic acid in the coating forms particles in the fluid stream which are detected by a monitor.

Abstract: Liquid modified epoxy resins are prepared by reacting a drying oil with a diepoxide in the presence of certain alkali or alkaline earth metal compounds, preferably a lithium soap such as lithium ricinoleate. The drying oil may be modified by reacting it with maleic acid, maleic anhydride, or fumaric acid to increase the drying rate.

Abstract: A die is internal for forming shapes of polygonal cross-section, which has all internal surfaces which are parallel to the die axis of equal length. The die is primarily used in hydrostatic extrusion. It can be made in two parts for ease in cleaning. A billet having a pointed, faceted nose for use with the die is also disclosed.

Abstract: A sampling system monitors a gas stream of a power generator and automatically samples the gas stream if its characteristics indicate that a material in the power generator is being thermally degraded. A gas stream monitoring device generates a first signal if it detects degradation occurring. A time-delay relay determines whether the first signal is continuous, and if it is the relay acts to prevent the monitor from monitoring the gas stream. If the first signal then terminates, a second signal is generated which activates an alarm and permits gas to flow into a sampling device. The sampling device has three sections which collect large particles, small particulates, and vapors and gases. The products collected can be analyzed to determine which material in the power generator was thermally degraded.

Abstract: A crystal resonator is disclosed of a single crystal of the approximate composition Tl.sub.3 BX.sub.4 having two parallel surfaces normal to a zero temperature coefficient of frequency direction and having an electrode mounted on each surface, where B is vanadium, niobium, or tantalum, and X is sulfur or selenium. A filter is disclosed of a crystal resonator coupled to a capacitor or more than one crystal resonator in series each coupled to a capacitor. A voltage controlled crystal oscillator resonator is disclosed of a crystal resonator in parallel with an inductor and a varactor.

Abstract: Uranium is separated from contaminating cations in an aqueous liquor containing uranyl ions. The liquor is mixed with sufficient recycled uranium complex to raise the weight ratio of uranium to said cations preferably to at least about three. The liquor is then extracted with at least enough non-interfering, water-immiscible, organic solvent to theoretically extract about all of the uranium in the liquor. The oganic solvent contains a reagent which reacts with the uranyl ions to form a complex soluble in the solvent. If the aqueous liquor is acidic, the organic solvent is then scrubbed with water. The organic solvent is stripped with a solution containing at least enough ammonium carbonate to pecipitate the uranium complex. A portion of the uranium complex is recycled and the remainder can be collected and calcined to produce U.sub.3 O.sub.8 or UO.sub.2.

Abstract: Uranium is separated from contaminating metal ions in an aqueous feed liquor containing the uranyl ion. The liquor is extracted with a first, non-interfering, waterimmiscible, organic solvent containing a reagent which reacts with the uranyl ion to form a complex soluble in the organic solvent. The organic solvent is scrubbed with water if necessary, then stripped with a stripping liquor of an aqueous sulfuric acid liquor having a pH of about 0.5 to about 6 containing a reducing ion or an aqueous carbonate solution having a pH of about 8 to about 9. If the sulfuric acid liquor is used the stripped uranous ion is oxidized and the sulfuric acid liquor is diluted to prevent the precipitation of a uranium complex. The stripping liquor is extracted with an amine liquor comprising a second, noninterfering, water-immiscible, organic solvent and a tertiary or quaternary amine. The amine liquor is stripped with an ammonium carbonate solution to precipitate a uranium complex.

Abstract: Single crystals of Tl.sub.3 TaS.sub.4 and Tl.sub.3 TaSe.sub.4 are disclosed which have useful acousto-optical properties, including low acoustic velocities and high acousto-optical figures of merit. They are used in acousto-optical devices such as a display device, a laser modulator, a non-collinear tunable filter, an acousto-optical delay line, and an acousto-optical waveguide modulator.

Abstract: A thermoparticulating tape is disclosed which comprises a flexible fibrous material, a compound which thermoparticulates at a temperature below 200.degree.C dispersed throughout the flexible fibrous material, and a flexible outer coating over the flexible fibrous material through which the products formed when the compound thermoparticulates can pass. The tape is best made by dissolving the thermoparticulating compound in a solvent, immersing the fibrous material in the solution, evaporating the solvent, and applying the outer coating to the fibrous material. An adhesive backing can be applied to the tape if desired. The tape is placed in an electrical apparatus cooled by a gas stream, in a position exposed to the gas stream. When overheating occurs the tape darkens and emits particles into the gas stream which are detected by a monitor.

Abstract: Crystals or Tl.sub.3 VS.sub.4, Tl.sub.3 VSe.sub.4, Tl.sub.3 NbS.sub.4, Tl.sub.3 NbSe.sub.4, Tl.sub.3 TaS.sub.4, and Tl.sub.3 TaSe.sub.4 are disclosed which have a surface containing of normal to a zero temperature coefficient of delay direction. The crystals are used to transmit acoustic waves in surface and bulk wave devices.

Abstract: A grease of a telomer of polytetrafluoroethylene and a perfluoroalkyl polyether is used to protect electrical apparatus from overheating. The grease is applied to a portion of an electrical apparatus which is exposed to a gas stream, particularly to portions subjected to operating temperatures of about 100.degree. to about 130.degree.C. When the coated portion of the electrical apparatus overheats the grease forms particles in the gas stream which are detected by a monitor. The apparatus can then be shut down or its load reduced.

Abstract: A solution is prepared of about 30 to about 60 mole percent of a mono-ester of a tricarboxylic anhydride or a diester of a tetracarboxylic acid and about 40 to about 70 mole percent of a dianhydride. An aromatic diisocyanate is added and the solution heated until the viscosity no longer increases. The precursor can be precipitated by the addition of a non-solvent, collected, and re-dissolved in a solvent. The solution of the precursor can be applied to a sheet and cured to form a polyimide or polyamide-imide film, or it can be applied to a wire and cured to form a polyimide or polyamide-imide wire enamel.

Abstract: Monomers having both an amine group and an anhydride or two carboxylic acid or salt groups are electropolymerized in solution. In an alcohol solvent the polymer forms as a coating on the anode, and in an aprotic solvent the polymer remains in solution. The polymer is cured to form a polyimide.

Abstract: An acoustic surface wave device is disclosed which comprises a crystal of Tl.sub.3 TaS.sub.4, Tl.sub.3 TaSe.sub.4, or mixtures thereof having at least one surface suitable for the propagation of surface waves, a surface wave generating transducer mounted on the surface, and a surface wave receiving transducer mounted on the surface positioned to receive a surface wave generated by the surface wave generating transducer.The device transmits surface waves at a low velocity and high coupling efficiency and can be used in a delay line, a filter, an FM discriminator, an oscillator, or other device.

Abstract: An optical waveguide modulator is disclosed which uses single crystals of TlGaSe.sub.2 or TlInS.sub.2. The optical waveguide modulator is used to impress a signal upon a light beam traveling in a waveguide. Monochromatic light is guided along a thin plate of the crystal. Acoustic waves are generated which move across the thickness of the crystal, modulating the light. The frequency, polarization, or mode of the light can be modulated by the acoustic waves.

Abstract: A printed circuit board is prepared by connecting electronic components to the circuit, coating the board with a layer up to about 0.1 mil thick of a compound of the formula C.sub.n F.sub.2n.sub.+1 C.sub.m X.sub.2m.CHY--OOC--C(R)=CH.sub.2 or its prepolymer, replacing at least one of the electronic components, thermally bonding another electronic component to the circuit, and recoating the area around the new component with a layer of the compound or its prepolymer. In the formula n is 2 to 9, m is 1 to 9, X and Y are H, F Cl, or Br and R is --H or --CH.sub.3. This method enables a printed circuit board to be easily repaired since the coating on the board can be soldered or welded through without first removing the coating or protecting the surrounding coating.

Abstract: A binding tape is made by coating a ribbon having glass fibers in the fill direction and a flexible, thermally stable fiber in the warp direction, with a swellable resin composition and removing the excess composition. The tape is lap-wound over an electrical conductor which is then immersed in solventless resin under pressure. The conductor is removed from the solventless resin and the tape prevents the solventless resin from seeping out before it is cured.