Patents Represented by Attorney Raymond C. Von Bodungen
  • Patent number: 4254005
    Abstract: High levels of durable-press appearance rating and conditioned wrinkle recovery angle together with improved abrasion-resistance, breaking strength, and tearing strength are the primary textile qualities imparted to cellulosic textile with aqueous solutions containing N-methylolacrylamide-type reagents, a salt of persulfuric acid, and an alkali metal phosphate, which may be supplemented with standard wetting agents and fabric softeners.
    Type: Grant
    Filed: February 6, 1980
    Date of Patent: March 3, 1981
    Assignee: The United States of America as represented by the Secretary of Agriculture
    Inventors: Stanley P. Rowland, Florine A. Blouin, Frederick F. Shih
  • Patent number: 4253841
    Abstract: A process for copolymerizing vinyl monomers with cotton to yield a product having encapsulated cotton fibers, the product in fabric form has improved durable-press properties, improved soil release, improved dyeability, improved abrasion resistance, and the product contains new multifunctional reactive groups which are useful in further textile modification. The reaction is carried out generally by treating cotton fabric with a vinyl monomer in a deoxygenated mixture of solvents, then irradiating the impregnated immersed fabric by exposure to near-ultraviolet-light radiation.
    Type: Grant
    Filed: February 23, 1979
    Date of Patent: March 3, 1981
    Assignee: The United States of America as represented by the Secretary of Agriculture
    Inventors: James A. Harris, Jett C. Arthur, Jr.
  • Patent number: 4253215
    Abstract: A plurality of lint cotton quality measurements is made on lint cotton which is to be fed into the lint cleaning process in a cotton ginning system. The plurality of cotton quality measurements in the form of individual electrical signals is communicated to a synchronizing means which translates the quality electrical signals into a single electrical output signal fed into a controller which controls the flow of lint cotton into the lint cleaning apparatus.
    Type: Grant
    Filed: February 23, 1979
    Date of Patent: March 3, 1981
    Assignee: The United States of America, as represented by the Secretary of Agriculture
    Inventor: Gino J. Mangialardi, Jr.
  • Patent number: 4249655
    Abstract: An apparatus for removing dust from a fiber sample for subsequent analysis is disclosed. A first upper cylindrical chamber containing a fiber sample has a tangential air jet and a radial air jet installed to swirl and tumble the fiber sample in a cyclonic fashion, thus liberating the dust from the sample when either a positive or a negative pressure is applied through the air jets. The liberated dust particles are then screened out through a 100 mesh screen filter and exhausted through a funnel. The device can be equipped with a second stage chamber containing a plurality of step-stage filters and a third stage plurality of microfilters to selectively screen the dust particles. A blow bottle containing an aqueous medium to absorb even the finest dust particles or gas can also be added as a fourth stage.
    Type: Grant
    Filed: June 29, 1979
    Date of Patent: February 10, 1981
    Assignee: The United States of America as represented by the Secretary of Agriculture
    Inventors: Myles A. Patureau, Michael F. Murray
  • Patent number: 4249017
    Abstract: The title compounds, having the formula (RO.sub.2 CNHCH.sub.2).sub.3 PY where Y=oxygen or sulfur, are prepared by reacting a tris(N-carbalkoxylaminomethyl)phosphine, having the formula (RO.sub.2 CNHCH.sub.2).sub.3 P, with an oxidizing or sulfurizing agent. The products, after methylolation with formaldehyde, are useful as finishing agents for imparting flame retardant properties to cotton fabrics.
    Type: Grant
    Filed: November 29, 1978
    Date of Patent: February 3, 1981
    Assignee: The United States of America as represented by the Secretary of Agriculture
    Inventor: Arlen W. Frank
  • Patent number: 4245494
    Abstract: An apparatus for analyzing volatile components from raw or processed food products using either direct gas chromatography or combined direct gas chromatography and mass spectrometry is disclosed. An inlet assembly containing a sample is appropriately affixed to a means of supplying helium carrier gas. Volatiles are driven off the sample and fed to a condenser assembly where the moisture is removed. The resultant moisture free volatiles are fed to a gas chromatograph or combined direct gas chromatograph and mass spectrograph for analysis.
    Type: Grant
    Filed: February 26, 1979
    Date of Patent: January 20, 1981
    Assignee: The United States of America as represented by the Secretary of Agriculture
    Inventors: Michael G. Legendre, Gordon S. Fisher
  • Patent number: 4246031
    Abstract: A flame retardant prepolymer composition for imparting flame retardance to cotton, cellulosic textiles, and certain other materials; the process for preparing the prepolymer composition; and the application technique of said prepolymer composition are disclosed. Tetrakis(hydroxymethyl)phosphonium sulfate, a THP salt, is acidified, ammonia gas is bubbled into the mixture to achieve a constant boiling, these steps are repeated a number of times, and the prepolymer mixture thus prepared is then applied to a substrate, followed by treatment with a caustic solution.
    Type: Grant
    Filed: October 11, 1978
    Date of Patent: January 20, 1981
    Assignee: The United States of America as represented by the Secretary of Agriculture
    Inventors: Galoust M. Elgal, Rita M. Perkins, Nestor B. Knoepfler
  • Patent number: 4239701
    Abstract: Novel ternary salts of tris(aminomethyl) phosphines and their oxides having the formula (R.sub.2 NH.sup.+ CH.sub.2).sub.3 P(0).sub.n 3X.sup.-, wherein R is hydrogen, an alkylradical having from 1 to 6 carbon atoms, or an aryl radical n is an integer from 0 to 1, and X is a halogen, are prepared by the reaction of a hydrohalic acid, HX, with various nitrogen- and phosphorus-containing compounds including tris(aminomethyl)phosphines and their oxides, tris(N-carbalkoxylaminomethyl)phosphines oxides, and 1,3,5-triaza-7-phosphaadamantane and its 7-oxide.
    Type: Grant
    Filed: July 26, 1979
    Date of Patent: December 16, 1980
    Assignee: The United States of America as represented by the Secretary of Agriculture
    Inventors: Arlen W. Frank, Donald J. Daigle, Russell M. H. Kullman
  • Patent number: 4236890
    Abstract: A pretreatment system composed of hexamethoxymethyl melamine, p-toluene sulfonic acid, 2-amino-2-methyl-1-propanol, triethylamine, butoxy triglycol, and carboxy vinyl polymeric thickener is disclosed, which through application to the fabric surface by a screen printing technique is highly effective in improving the affinity of cellulose-containing textiles for disperse dyestuffs. Fabrics with prints that are durable to washing are produced by simultaneously heat transfer printing and curing at about 190.degree. C. to 220.degree. C. for 20-30 seconds.
    Type: Grant
    Filed: June 7, 1978
    Date of Patent: December 2, 1980
    Assignee: The United States of America as represented by the Secretary of Agriculture
    Inventors: Eugene J. Blanchard, Gloria A. Gautreaux, Robert J. Harper, Jr.
  • Patent number: 4228100
    Abstract: Novel quaternary ureidomethyl phosphonium salts having the general formula ##STR1## are prepared by condensing a urea having the formula RNHC(O)NR'R" with a quaternary hydroxymethyl phosphonium salt having the formula (HOCH.sub.2).sub.4 P.sup.+ X.sup.- in a molar ratio of at least 2:1. The products, which are characterized by the absence of residual hydroxymethyl groups, are useful as finishing agents for imparting flame retardant properties to cotton fabrics.
    Type: Grant
    Filed: April 6, 1979
    Date of Patent: October 14, 1980
    Assignee: The United States of America as represented by the Secretary of Agriculture
    Inventor: Arlen W. Frank
  • Patent number: 4225512
    Abstract: Novel ternary salts of tris(aminomethyl)phosphines and their oxides having the formula (R.sub.2 NH.sup.+ CH.sub.2).sub.3 P(O).sub.n 3X.sup.-, wherein R is hydrogen, an alkyl radical having from 1 to 6 carbon atoms or an aryl radical, n is an integer from 0 to 1, and X is a halogen, are prepared by the reaction of a hydrohalic acid, HX, with various nitrogen- and phosphorus-containing compounds including tris(aminomethyl)phosphines and their oxides, tris(N-carbalkoxylaminomethyl)phosphines oxides, and 1,3,5-triaza-7-phosphaadamantane and its 7-oxide.
    Type: Grant
    Filed: July 26, 1979
    Date of Patent: September 30, 1980
    Assignee: The United States of America as represented by the Secretary of Agriculture
    Inventors: Arlen W. Frank, Donald J. Daigle, Russell M. H. Kullman
  • Patent number: 4224030
    Abstract: An aluminum acetate salt solution containing sodium and chloride ions is prepared by reaction of aqueous aluminum chloride and sodium acetate. It is suitable for use as a catalyst in the treatment of cellulosic-containing textiles with formaldehyde or a formaldehyde-amide adduct crosslinking agent to produce durable press properties in the finished material. There is no discoloration in the thus-treated fabric which also exhibits greater strength than is normally present in fabric treated to the same level of wrinkle resistance with an aluminum salt catalyst.
    Type: Grant
    Filed: January 5, 1979
    Date of Patent: September 23, 1980
    Assignee: The United States of America as represented by the Secretary of Agriculture
    Inventors: Robert M. Reinhardt, Russell M. H. Kullman
  • Patent number: 4219964
    Abstract: A new apparatus and system for the systematic application of liquid chemicals to plants is disclosed. A soft woven nylon rope wick is used to convey chemical solution from a reservoir by means of capillary action. The rope apparatus, which is physically supported, is leveled and positioned to selectively contact certain plants as the wick is moved across an agricultural field. Thus chemical solution is deposited selectively only on contact with the wick.
    Type: Grant
    Filed: December 13, 1978
    Date of Patent: September 2, 1980
    Assignee: The United States of America as represented by the Secretary of Agriculture
    Inventor: Jim E. Dale
  • Patent number: 4219469
    Abstract: The undesirable coloration generally found in cottonseed and other oilseed protein isolates prepared from oilseed flours or concentrates is substantially eliminated or improved by treatment of the flours with a specific solvent mixture containing a non-polar solvent, a polar solvent, a quantity of water, and a small quantity of a food-grade organic acid. The improved isolates render the consumer product more acceptable from the point of view of improved coloration.
    Type: Grant
    Filed: September 19, 1978
    Date of Patent: August 26, 1980
    Assignee: The United States of America as represented by the Secretary of Agriculture
    Inventors: Ranjit S. Kadan, George M. Ziegler, Jr., James J. Spadaro
  • Patent number: 4214873
    Abstract: The title compounds, having the formula (RO.sub.2 CNHCH.sub.2).sub.3 PY where Y=oxygen or sulfur, are prepared by reacting a tris(N-carbalkoxylaminomethyl)phosphine, having the formula (RO.sub.2 CNHCH.sub.2).sub.3 P, with an oxidizing or sulfurizing agent. The products, after methylolation with formaldehyde, are useful as finishing agents for imparting flame retardant properties to cotton fabrics.
    Type: Grant
    Filed: April 30, 1979
    Date of Patent: July 29, 1980
    Assignee: The United States of America as represented by the Secretary of Agriculture
    Inventor: Arlen W. Frank
  • Patent number: 4208920
    Abstract: An apparatus for automatically testing the breaking strength of textiles during the spinning process is disclosed. A yarn clamping means affixed to a breaking assembly is rotatably mounted to an automatic timer which is pre-programmed to break yarn at set intervals. The spinning yarn is passed through a tension sensing device which measures the strength of the yarn at the breaking point, after the clamping means rotates, catches, and breaks the yarn. The clamping means then rotates back to the original position and restores and recombines the yarn as new feed yarn.
    Type: Grant
    Filed: April 30, 1979
    Date of Patent: June 24, 1980
    Assignee: The United States of America as represented by the Secretary of Agriculture
    Inventor: John S. Graham
  • Patent number: 4207068
    Abstract: A process is disclosed for producing dyed fabrics by treating cotton with inorganic phosphorylating agent, curing, and then dyeing to develop the pattern.
    Type: Grant
    Filed: October 16, 1978
    Date of Patent: June 10, 1980
    Assignee: The United States of America as represented by the Secretary of Agriculture
    Inventors: Eugene J. Blanchard, Joseph S. Bruno, Gloria A. Gautreaux
  • Patent number: 4204072
    Abstract: The title compounds, having the formula (RO.sub.2 CNHCH.sub.2).sub.3 P, are prepared by reacting a quaternary phosphonium salt, having the formula (RO.sub.2 CNHCH.sub.2).sub.4 P.sup.+ X.sup.-, with a base, preferably one that is capable of reacting with and thereby inactivating the by-product formaldehyde or formaldehyde derivative. The products are useful as intermediates for the preparation of finishing agents that impart flame retardant properties to cotton fabrics.
    Type: Grant
    Filed: November 29, 1978
    Date of Patent: May 20, 1980
    Assignee: The United States of America as represented by the Secretary of Agriculture
    Inventor: Arlen W. Frank
  • Patent number: 4199322
    Abstract: The preparation of bacteriostatic, water-insoluble peroxide-containing complexes of zinc acetate, by reaction of zinc acetate with hydrogen peroxide in the presence of acetic acid, is disclosed. A process for in situ formation and deposition of these complexes on cellulosic and polyester textiles is described. The textile finishes so produced inhibit the growth and spreading of odor- and infection-producing gram-positive and gram-negative bacteria on the treated textiles. The antibacterial activity of the finished textiles is durable to repeated launderings.
    Type: Grant
    Filed: December 28, 1978
    Date of Patent: April 22, 1980
    Assignee: The United States of America as represented by the Secretary of Agriculture
    Inventors: Gary F. Danna, Tyrone L. Vigo, Clark M. Welch
  • Patent number: 4182673
    Abstract: A selective and effective collection of noninhalable and/or nonrespirable particulates employs inertial impaction to separate particles larger than a specified size from smaller particulates in an airstream and to collect them on a moving adhesive collection surface. A unique U-type impaction configuration is used.
    Type: Grant
    Filed: August 31, 1978
    Date of Patent: January 8, 1980
    Assignee: The United States of America as represented by the Secretary of Agriculture
    Inventors: Eric W. Schmidt, Lawrence W. Miga, James A. Gieseke