Patents Represented by Attorney Roger Aceto
  • Patent number: 6319457
    Abstract: A method and apparatus is disclosed for lacing an extruded tube of a non derivatized cellulose through an S-wrap to collapse the tube to a flat width. The lacing to form the S-wrap is accomplished without slowing the extrusion speed. At the start of the extrusion operation, the extrusion path leads between a pair of horizontally lacing members. After the leading edge of the extruded tube has passed downwardly through the space between the lacing members, the members are rotated as a unit to bring them into contact with opposite sides of the extruded tube. This collapses the and creates the S-wrap.
    Type: Grant
    Filed: August 27, 1999
    Date of Patent: November 20, 2001
    Assignee: Viskase Corporation
    Inventors: Paul Edmund DuCharme, Jr., Owen Joseph McGarel
  • Patent number: 6279737
    Abstract: Disclosed is a package containing a plurality of cut lengths of fibrous casing which are moisturized to substantially soaked levels of moisture and are retained in an evacuated plastic bag wherein the moisture level of the casing is derived from free water added into the bag prior to evacuation. Also disclosed is a method of packaging cut lengths of casing which provides for the addition of soaked levels of moisture to the casing in the bag.
    Type: Grant
    Filed: August 4, 1997
    Date of Patent: August 28, 2001
    Assignee: Viskase Corporation
    Inventors: Larry Clyde Long, Frederick Maynard Merritt, II, Jeffery Allen Oxley
  • Patent number: 6264874
    Abstract: A method and apparatus for controlling the diameter of a clear extruded molten tube wherein the extruded tube contains a volume of a clear liquid and the level of the liquid is indicative of the tube diameter so the level rises as the tube diameter decreases. A light beam passing through the tube is refracted from a straight line path when the liquid level rises above the level of the beam. The refracting of the beam in turn triggers the introduction of air into the extruded tube to increase the diameter of the extruded, molten tube.
    Type: Grant
    Filed: April 22, 1999
    Date of Patent: July 24, 2001
    Assignee: Viskase Corporation
    Inventor: Niel Edwin Nielsen
  • Patent number: 6200510
    Abstract: A method of applying an indicia to the surface of a cellulose casing by non contact printing wherein the indicium is applied in-line with the casing manufacture at a location between the wet end and the dry end of the casing manufacturing process wherein the indicia comprises an ink that is cured and cross linked with the cellulose prior to the casing reaching the dry end of the process. The indicia preferably is in the form of a dot matrix pattern that is visible yet presents no barrier to the passage of smoke.
    Type: Grant
    Filed: October 13, 1998
    Date of Patent: March 13, 2001
    Assignee: Viskase Corporation
    Inventors: Paul Edmund DuCharme, Jr., Rama Ramagopal
  • Patent number: 6132779
    Abstract: The removal of a cellulosic casing from about a sausage, stuffed and processed in the casing, is accomplished by contacting the casing, either before or after stuffing, with a food grade enzyme, e.g.a. cellulase or cellulase enzyme complex, to metabolize the cellulosic casing on the sausage thereby producing a substantially casing-free sausage. Contacting the casing with the enzyme is accomplished prior to stuffing by applying an enzyme solution to the internal surface of the casing as part of an internal shirring spray or as a stripe to the exterior of the casing. Contacting with the enzyme after stuffing is accomplished by showering the stuffed casing with the enzyme solution. Also disclosed is the use of a combination of pre and post stuffing methods for applying the enzyme to the casing.
    Type: Grant
    Filed: November 19, 1999
    Date of Patent: October 17, 2000
    Assignee: Viskase Corporation
    Inventors: Jean-Francois Lacoste-Bourgeacq, Majed Fawaz
  • Patent number: 6096258
    Abstract: A method and apparatus is disclosed for forming a cellulose film suitable for direct food contact by precipitation from a solution of cellulose water and a tertiary amine oxide cellulose solvent. After precipitation of a cellulose gel from the solution, the gel is washed at ever increasing temperatures and then dried to provide a cellulose film having a solvent level to not more than 40 ppm. Portions of the wash water is collected and treated to recover the solvent for reuse.
    Type: Grant
    Filed: January 20, 1998
    Date of Patent: August 1, 2000
    Assignee: Viskase Corporation
    Inventors: Paul Edmund DuCharme, Jr., Edward Makoto Kajiwara, Norman Abbye Portnoy
  • Patent number: 6042853
    Abstract: The removal of a cellulosic casing from about a sausage stuffed and processed in the casing is accomplished by contacting the sausage with a cellulase or cellulase enzyme complex to metabolize the cellulosic casing on the sausage thereby producing a substantially casing-free sausage.
    Type: Grant
    Filed: August 28, 1998
    Date of Patent: March 28, 2000
    Assignee: Viskase Corporation
    Inventors: Jean-Francois Lacoste-Bourgeacq, Skeeter Meranda Bassue-Hyligar, Roger Aceto
  • Patent number: 6004599
    Abstract: Disclosed is a bag arrangement and packaging method for packaging bone-in cuts of meat using two bags to provide a double wall of film surrounding the cut of meat for bone puncture resistance. Both bags are bottom sealed bags formed of a heat shrink film, the inner bag has an interrupted bottom seal to provide an opening for venting air between the bags and the outer bag has a continuous bottom seal. The outer bag is longer than the inner bag so the outer bag can be closed without involving any portion of the inner bag in the closure. The bone-in cut of meat is inserted first into the first bag and then the first bag and its contents are inserted into the second bag, the bags are evacuated and then the outer bag is closed.
    Type: Grant
    Filed: August 10, 1998
    Date of Patent: December 21, 1999
    Assignee: Viskase Corporation
    Inventors: Roger Douglas Bert, John Stephen Siwinski
  • Patent number: 5962053
    Abstract: Described is an edible, water insoluble film which is a blend of polysaccharide and protein and, in particular, a ternary blend of konjac flour as a major constituent, agar and gelatin. Also, described is a method of forming the film including a deacetylating step to insolubilize the konjac flour.
    Type: Grant
    Filed: February 17, 1998
    Date of Patent: October 5, 1999
    Assignee: Viskase Corporation
    Inventor: Frederick Maynard Merritt, II
  • Patent number: 5942167
    Abstract: Disclosed is a method of extruding a solution of cellulose and an amine oxide cellulose solvent as a tube about a sizing mandrel which diametrically stretches the extruded tube. An aqueous poly(ethylene oxide) solution is introduced into the interior of the extruded tube to facilitate passage of the tube over the sizing mandrel and to extract the amine oxide cellulose solvent from the tube. After such extraction, the aqueous poly(ethylene oxide) solution containing the extracted amine oxide cellulose solvent is contacted with an anion exchanger to remove the poly(ethylene oxide) so the amine oxide cellulose solvent can be recovered.
    Type: Grant
    Filed: August 12, 1997
    Date of Patent: August 24, 1999
    Assignee: Viskase Corporation
    Inventor: Paul Edmund DuCharme, Jr.
  • Patent number: 5942354
    Abstract: A curl resistant battery separator of a noncellulosic nonwoven substrate extrusion coated on at least one surface with a cellulose film and process for making such separator by contacting a nonwoven noncellulosic textile substrate with a cellulose or cellulose derivative solution on at least one side of said substrate; converting the solution to a solid cellulose or cellulose derivative, preferably having a degree of polymerization of at least 350, more preferably at least 600, to form a coated substrate; washing said substrate in an aqueous solution; drying the coated substrate under biaxial tension to provide a battery separator having a moisture content of from about 4 to 25 wt. % based on the bone dry gauge of the separator(BDG); and then holding the separator for at least 8 hours at elevated temperatures of at least 40.degree. C. in the presence of a controlled amount of moisture to produce a separator which is stabilized against curling and has a moisture content between about 4 to 25 wt.
    Type: Grant
    Filed: December 2, 1997
    Date of Patent: August 24, 1999
    Assignee: Viskase Corporation
    Inventors: Jeffery Allen Oxley, Thomas Danko
  • Patent number: 5919534
    Abstract: A vented food casing having a plurality of die cut vent openings which are uniform and free-draining so as to provide the casing with a vent rate for air and liquids such as meat juices which is substantially constant around the periphery of the casing. The vent opening being formed by a die cutting operation by drawing flattened casing between rollers, one of which has made punches that mate with female die openings on another roller.
    Type: Grant
    Filed: November 27, 1996
    Date of Patent: July 6, 1999
    Assignee: Viskase Corporation
    Inventor: Jeffery Allen Oxley
  • Patent number: 5766540
    Abstract: The tubular extrusion of a thermoplastic nonderivatized cellulose solution about a mandrel and through a long air gap in excess of 304 mm is facilitated by use of a mandrel which is extensible from the extrusion die. On extrusion start-up, the mandrel extends a short length from the die. For steady-state operation, the mandrel is extended its full length from the die. Also disclosed is a mandrel structure to facilitate the introduction of a nonsolvent liquid into the interior of the extruded tube at a high location on start-up of extrusion and at a lower location during steady-state operation.
    Type: Grant
    Filed: March 27, 1997
    Date of Patent: June 16, 1998
    Assignee: Viskase Corporation
    Inventors: Edward Makoto Kajiwara, Joseph Robert Walta, Ronald Joseph Jerantowski
  • Patent number: 5759478
    Abstract: The tubular extrusion of a thermoplastic nonderivatized cellulose solution about a mandrel and through a long air gap in excess of 304 mm is facilitated by use of a mandrel which is extensible from the extrusion die. On extrusion start-up, the mandrel extends a short length from the die. For steady-state operation, the mandrel is extended its full length from the die. Also disclosed is a mandrel structure to facilitate the introduction of a nonsolvent liquid into the interior of the extruded tube at a high location on start-up of extrusion and at a lower location during steady-state operation. The mandrel also includes a sizing portion having circumferential grooves which gather gas bubbles that may evolve at the interface between the extruded tube and the sizing portion. Vertical channels in the sizing portion connect these grooves and provide the passage of gas bubbles into a volume below the mandrel.
    Type: Grant
    Filed: March 27, 1997
    Date of Patent: June 2, 1998
    Assignee: Viskase Corporation
    Inventors: Edward Makoto Kajiwara, Brant Anton Loichinger
  • Patent number: 5747125
    Abstract: A crosslinked cellulose composite film including a regenerated cellulose matrix containing a uniform dispersion of hemp fibers and a poly(ethylene oxide) plasticizer. A method for forming the film includes mixing a slurry of the hemp, poly(ethylene oxide) and a cellulose solvent with a cellulose solution, extruding the mixture, regenerating the cellulose from the solution to form the matrix containing hemp fibers, contacting with a crosslinking agent and then drying.
    Type: Grant
    Filed: July 18, 1996
    Date of Patent: May 5, 1998
    Assignee: Viskase Corporation
    Inventor: John Markulin
  • Patent number: 5744251
    Abstract: The present invention relates to compounded fibrous dope compositions of amine oxide cellulose solutions having a uniformly dispersed second fibrous material, methods of producing the compositions, and shaped articles such as fibers, paper, films, and food casings produced from the compositions.
    Type: Grant
    Filed: April 15, 1996
    Date of Patent: April 28, 1998
    Assignee: Viskase Corporation
    Inventors: Paul Edmund DuCharme, Jr., Norman Abbye Protnoy, John Markulin, Myron Donald Nicholson
  • Patent number: 5702783
    Abstract: A cellulose food casing comprising a nonderivatized cellulose film precipitated in tubular form from an extruded thermoplastic solution of cellulose, an amine oxide cellulose solvent and water.
    Type: Grant
    Filed: August 16, 1995
    Date of Patent: December 30, 1997
    Assignee: Viskase Corporation
    Inventors: Myron Donald Nicholson, Edward Makoto Kajiwara, Paul Edmund DuCharme, Jr.
  • Patent number: 5695800
    Abstract: Disclosed is a food product encased in a water insoluble film of glucomannan and a method for its manufacture. In the process an aqueous solution of glucomannan is cast onto the food product surface and then is deacetylated and coagulated in sire by contact with a saturated salt solution having either an acidic or basic pH. The coagulated solution is cured and dried in the presence of salt and subsequently washed and further dried to provide the water insoluble film.
    Type: Grant
    Filed: March 13, 1996
    Date of Patent: December 9, 1997
    Assignee: Viskase Corporation
    Inventor: Frederick Maynard Merritt, II
  • Patent number: 5658525
    Abstract: In a method for forming a cellulose tube suitable for use as a food casing, in which a solution of nonderivatized cellulose, tertiary amine N-oxide and water is extruded through a die gap and the extruded tube is downwardly drawn through an air gap while being internally cooled and then is passed into a water bath, the tube transverse direction tensile strength being increased by drawing the extruded tube through an air length of at least about five inches and exposing the exterior surface of the extruded tube to cooling air in the air gap.
    Type: Grant
    Filed: August 4, 1995
    Date of Patent: August 19, 1997
    Assignee: Viskase Corporation
    Inventors: Edward Makoto Kajiwara, Norman Abbye Portnoy, Paul Edmund Ducharme, Jr.
  • Patent number: 5658524
    Abstract: In a method for forming a cellulose tube suitable for use as a food casing or as cellophane film, in which a solution of nonderivatized cellulose, tertiary amine N-oxide and water is extruded through an air gap of at least five inches, and into a water bath, such that a wet cellulose tube is formed. The wet tube is inflated from about 55% to 140% or more and dried thereby substantially retaining its work-to-rupture characteristics, especially when compared to viscose-derived tubes.
    Type: Grant
    Filed: May 4, 1995
    Date of Patent: August 19, 1997
    Assignee: Viskase Corporation
    Inventors: Norman Abbye Portnoy, Edward Makoto Kajiwara, Paul Edmund Ducharme, Jr.