Abstract: A superconducting magnet coil system comprising a main field coil which is formed from series-connected sections, wherein the conductors of the radially inner sections contain a first superconducting material and have first electric voltage insulation, the conductors of the radially outer sections comprise a second superconducting material and are provided with second electric voltage insulation, wherein the first superconducting material has a higher critical magnetic field than the second superconducting material, and the first voltage insulation has a smaller dielectric strength than the second voltage insulation, and a shielding coil which is connected in series with the main field coil, radially surrounds the main field coil, and comprises conductors of the second superconducting material having the second electric voltage insulation, wherein the main field coil and the shielding coil are superconductingly short-circuited during operation and are protected through several ohmic resistances and/or diodes

Abstract: A superconducting magnet coil configuration comprising at least one section of a superconducting strip conductor, which is continuously wound in a cylindrical winding chamber (1) between two end flanges (2, 3) in several solenoid-like layers is characterized in that the section comprises an axial region of reduced current density (=notch region (12)), and the winding chamber (1) in the notch region (12) contains a first separating body (4) with a truncated conical envelope (5) which axially divides the winding chamber (1) into two partial chambers (6, 7), the superconducting strip conductor being guided over the truncated conical envelope (5) of the first separating body (4) from one partial chamber (6) into the other partial chamber (7) via a single-layer transfer winding (9), and a second separating body (10) is provided which supplements the first separating body (4) in the notch region (12) in a radial outer direction to form a circular cylinder, wherein the single-layer transfer winding (9) is disposed b

Abstract: A coupling configuration (1; 30) comprising a coupling element (3) and a supply capillary (2), wherein the coupling element (3) has a funnel-shaped section (5) which clamps an end (6) of the supply capillary (2), is characterized in that an envelope capillary (10) is provided into which the supply capillary (2) is inserted, wherein the end (6) of the supply capillary (2) projects past an end (11) of the envelope capillary (10), and the end (11) of the envelope capillary (10) is also clamped in the funnel-shaped section (5). The supply capillary is properly fixed in the coupling element and safely protected from capillary breakage.

Abstract: A cryostat (1) with a first helium tank (4) which contains helium at an operating temperature T1<3K, and a second helium tank (2) which is connected to the first helium tank (4) and contains liquid helium at an operating temperature T2>3K, wherein a cooling means (6) is provided in the first helium tank (4) which generates an operating temperature T1<3K in the first helium tank (4), wherein the cooling means (6) is designed as a Joule-Thomson valve with downstream heat exchanger from which pumped helium is transported to a room temperature region outside of the cryostat (1) is characterized in that a refrigerator (11) is provided whose cold end (19) projects into the second helium tank (2) and the supplied helium is returned during normal operation in a closed loop along the refrigerator (11) and into the second helium tank (2), thereby being pre-cooled and liquefied at the cold end (19) of the refrigerator (11).

Abstract: A superconducting magnet coil system comprising a main field coil which is formed from series-connected sections, wherein the conductors of the radially inner sections contain a first superconducting material and have first electric voltage insulation, the conductors of the radially outer sections comprise a second superconducting material and are provided with second electric voltage insulation, wherein the first superconducting material has a higher critical magnetic field than the second superconducting material, and the first voltage insulation has a smaller dielectric strength than the second voltage insulation, and a shielding coil which is connected in series with the main field coil, radially surrounds the main field coil, and comprises conductors of the second superconducting material having the second electric voltage insulation, wherein the main field coil and the shielding coil are superconductingly short-circuited during operation and are protected through several ohmic resistances and/or diodes

Abstract: A superconducting magnet coil configuration comprising at least one section of a superconducting strip conductor, which is continuously wound in a cylindrical winding chamber (1) between two end flanges (2, 3) in several solenoid-like layers is characterized in that the section comprises an axial region of reduced current density (=notch region (10)), and the winding layers (6, 9) have hollow cylindrical blind regions (4a, 4b, 4c) which are filled with filler and which have different axial lengths, and radially sequential blind regions (4a, 4b, 4c) each alternately abut one of the two end flanges (2, 3) and are each radially separated from each other by at least one continuous winding layer (7), wherein the axial overlapping region of the blind regions (4a, 4b, 4c) forms the notch region (10). The inventive device thereby realizes a magnet coil configuration comprising a strip conductor which has a notch region for correcting inhomogeneities, wherein the mechanical load on the strip conductor is minimized.

Abstract: A superconducting magnet coil configuration has at least one section containing a superconducting strip conductor which is wound in several layers like a solenoid in a cylindrical winding chamber (1) between two end flanges (2, 3), characterized in that the radially innermost layers of the section consist of metallic low-temperature superconductors (LTS) (LTS layers (8)) and radially adjacent layers of the section are formed from high-temperature superconductor (HTS) material (HTS layers (9)). The invention proposes a magnet coil configuration using HTS material which has a notch structure for correcting inhomogeneities and homogenizing a compact high-field magnet, wherein the mechanical load on the HTS strip conductor is minimized.

Abstract: A radio frequency coil arrangement for magnetic resonance measurements as well as a probe head for measuring resonance signals by utilizing such a radio frequency arrangement are disclosed. The radio frequency coil arrangement comprises a scroll coil having a stripe being spirally wound about a longitudinal axis, and having ends being provided with terminals for feeding and/or receiving radio frequency signals. The stripe, as seen in a plane unwound view, is configured in a Z-shape with a middle, broad section as well as two lateral, narrow sections being offset with respect to each other in a lateral direction, such that the lateral sections do not overlap in the lateral direction when the stripe is wound.

Abstract: A winding machine (1) for winding solenoid-shaped coils (21) with band-shaped conductors (6), comprising a winding means (3) which holds a circular-cylindrical coil core (2) of a coil (21) to be wound, and a winding drive which rotates a coil core (2), which is held in the winding means (3), about a winding axis W, wherein the winding means (3) can be moved in a first direction A by an axial drive, the direction A preferably extending approximately parallel to the winding axis W, is characterized in that the winding means (3) can be rotated about a pivot axis S by a pivot drive, wherein the pivot axis S extends perpendicularly to the direction A. The winding machine winds a solenoid-shaped coil with several layers of a band-shaped conductor without damaging the band-shaped conductor, in particular, when the band-shaped conductor contains brittle superconducting material.

Abstract: A method for coupling a gas chromatograph (21) to an NMR spectrometer, wherein the carrier gas present at the outlet of a separating column (23) of the gas chromatograph (21) including a sample contained in the carrier gas is supplied via a heated transfer line (1) to a collecting device (2) for the sample contained in the carrier gas, is characterized in that the carrier gas containing the sample is introduced into a collecting liquid (8) in the collecting device (2), and the sample is collected in the collecting liquid (8), wherein the collecting liquid (8) is suitable as an NMR solvent for the sample. The sample loss of the coupling method is reduced.

Abstract: An apparatus for analyzing a measuring substance which is dissolved in a solvent, comprising a conduit (4) for transporting the dissolved measuring substance from a feed means (3) to a measuring location (12), wherein the feed means (3) is designed to optionally feed a solvent or dissolved measuring substance into the conduit (4), is characterized in that the conduit (4) is designed, at least partially, as a polycapillary area (9) which has N parallel connected capillaries (21a, 21b, 21c; 62a, 62b), such that the individual capillaries (21a, 21b, 21c; 62a, 62b) have identical flow times from the feed means (3) to the measuring location (12) and wherein N?2. The apparatus improves the signal-to-noise ratio of the analysis.

Abstract: A magnetic resonance apparatus comprising a superconducting magnet coil which is disposed in a cryostat, and a refrigerator for cooling the magnet coil, which comprises a compressor for compressing a working gas, and a high-pressure line and a low-pressure line between the compressor and a control valve, which periodically connects the high-pressure line and the low-pressure line to a connecting line from the control valve to a cold head of the refrigerator, thereby generating pressure pulses via the connected working gas, wherein the control valve is mechanically rigidly connected to the cryostat, is characterized in that one pressure reservoir is provided in the high-pressure line and/or in the low pressure line, which is mechanically rigidly connected to the cryostat and which is connected to the compressor via a mechanically flexible line section.

Abstract: A probe head for nuclear magnetic resonance measurements in an area of a surface of a measuring object is disclosed. The probe head comprises first means for generating a static magnetic field extending at least partially parallel to the surface, second means for generating a radio frequency magnetic field having components extending perpendicular to the surface, and third means for amplifying a radio frequency magnetic field effective within the measuring object. The third means are configured as an aperture and are located between the second means and the surface.

Abstract: A method for applying a sample film to a sample carrier for subsequent spectroscopic analysis is described, comprising providing a quantity of sample in liquid state, providing a sample carrier having at least one sample position, applying the quantity of sample in liquid state on the at least one sample position in a plurality of partial quantities of the quantity of sample in such a manner that the partial quantities on the at least one sample position are not in contact with one another before being dried, drying the quantity of sample to form the sample film.

Abstract: A method for introducing a liquid sample into an NMR spectrometer to measure an NMR spectrum of the liquid sample, wherein the liquid sample is injected into a supply line and wherein further liquids are supplied into the supply line following the liquid sample, which are separated from each other and from the liquid sample by gas bubbles is characterized in that the liquid sample is supplied via an injection inlet to a valve configuration whose output side can be connected to the supply line and the further liquids and gas are supplied to the valve configuration via supply lines, wherein a desired sequence of sample segments, gas bubbles and further liquid segments is generated through temporally matched switching of the valve configuration in the supply line and is supplied to the NMR spectrometer. The inventive method realizes supply of a liquid sample into an NMR spectrometer with rapid sample transfer while thereby preventing mixing and dilution of the individual segments.

Abstract: The invention concerns an NMR apparatus (1) comprising an NMR spectrometer (2) for sequential investigation of several samples in sample containers (6) of substantially identical geometrical design, at a measuring position (10) in the NMR spectrometer (2) comprising a supply line (8) for pneumatic supply of the sample containers (6) from a magazine (3) to the measuring position (10). The apparatus is characterized in that the magazine (3) is disposed within a temperature-controlled cabinet, in particular, a cold chamber (4) and the supply line (8) can be heated. This substantially increases the throughput of samples of the NMR apparatus (1) with simple technical means.

Abstract: A method for driving a power supply (84) of a magnetic field coil (85) for generating a predetermined magnetic field profile B(r,t) in the volume under investigation of a nuclear magnetic resonance (=NMR) apparatus (81), wherein for compensation of distortions caused by the apparatus, an input signal i(t) is predistorted, that predetermines the time behavior of the magnetic field profile, wherein the power supply (84) is driven by the predistorted signal o(t), is characterized in that the predistortion is performed using a transfer function of the form G ? ( s ) = O ? ( s ) I ? ( s ) = ? n = 0 N ? s n ? b n ? n = 0 N ? s n ? a n , with s=?+j?, s?C, and with N?2, wherein O(s) is the Laplace transform of o(t), and I(s) is the Laplace transform of i(t). This inventive method improves compensation of distortions of one or more gradient fields including their correlations during rapid switching.

Abstract: A magnet system of a magnetic resonance apparatus for generating a magnetic field which is homogeneous and temporally highly stable within a volume under investigation and which extends along a z-axis, with a superconducting magnet coil (3) which is disposed in a cryostat (1) and with a periodically operated refrigerator (2) having a magnetic regenerator material which is disposed in a regenerator housing (5) within the cryostat (1) in the stray field of the magnet coil (3), and which is provided with a device (4) for shielding or compensating a magnetic disturbing field in the volume under investigation generated by the periodic operation of the refrigerator (2) due to regenerator magnetization changes is characterized in that the regenerator housing (5) is surrounded by a compensation coil arrangement (4) which can be superconductingly short-circuited and which is made from a plurality of conductor loops (6, 7a, 7b) which are separately short-circuited during measurement to keep a plurality of magnetic flux

Abstract: An electrode rod (1;21) for a pH meter, comprising a measuring end (2; 22) for immersion into a liquid test sample (31), wherein the measuring end (2; 22) has a pH measuring element, and wherein electrical feed lines (5) in the electrode rod (1;21) extend towards the pH measuring element, is characterized in that at least one capillary (8, 9, 10; 23) for feeding a liquid into the test sample (31) extends in the electrode rod (1; 21), and the at least one capillary (8, 9, 10; 23) has an outlet opening (11, 12, 13; 24) in the area of the measuring end (2; 22). The inventive electrode rod facilitates and accelerates preparation of liquid test samples, in particular, adjustment of a pH value for small amounts of test samples or narrow sample containers.

Abstract: A superconducting magnet system with a superconducting magnet coil system, which is disposed in a cryogenic fluid tank (2) of a cryostat (1), and an exchangeable refrigerator (5; 31) which is operated in a vacuum container (8) and is provided to re-liquify the cryogenic fluid flowing through a tubular conduit (4; 21) is characterized in that the tubular conduit (4; 21) is rigidly installed in the cryostat (1). The refrigerator reaches its optimum performance during operation in a vacuum, and can be easily exchanged in case of a defect.