Abstract: In various embodiments, a fluid is treated by flowing the fluid through a flow cell having (i) a fluid entry, (ii) a fluid exit, (iii) a treatment region disposed between the fluid entry and exit, and (iv) an interior surface reflective to ultraviolet (UV) light, and diffusively reflecting UV light emitted from one or more UV light sources to illuminate the treatment region substantially uniformly, thereby treating the fluid.
Type:
Grant
Filed:
March 24, 2016
Date of Patent:
August 29, 2017
Assignee:
CRYSTAL IS, INC.
Inventors:
Jianfeng Chen, Rajul V. Randive, Craig Moe
Abstract: In various embodiments, light-emitting devices incorporate graded layers with compositional offsets at one or both end points of the graded layer to promote formation of two-dimensional carrier gases and polarization doping, thereby enhancing device performance.
Type:
Grant
Filed:
September 16, 2016
Date of Patent:
June 13, 2017
Assignee:
CRYSTAL IS, INC.
Inventors:
Craig Moe, James R. Grandusky, Shawn R. Gibb, Leo J. Schowalter, Kosuke Sato, Tomohiro Morishita
Abstract: Bulk single crystal of aluminum nitride (AlN) having an areal planar defect density ?100 cm?2. Methods for growing single crystal aluminum nitride include melting an aluminum foil to uniformly wet a foundation with a layer of aluminum, the foundation forming a portion of an AlN seed holder, for an AlN seed to be used for the AlN growth. The holder may consist essentially of a substantially impervious backing plate.
Type:
Grant
Filed:
August 13, 2014
Date of Patent:
June 6, 2017
Assignee:
CRYSTAL IS, INC.
Inventors:
Robert T. Bondokov, Kenneth E. Morgan, Leo J. Schowalter, Glen A. Slack
Abstract: Bulk single crystal of aluminum nitride (AlN) having an areal planar defect density?100 cm?2. Methods for growing single crystal aluminum nitride include melting an aluminum foil to uniformly wet a foundation with a layer of aluminum, the foundation forming a portion of an AlN seed holder, for an AlN seed to be used for the AlN growth. The holder may consist essentially of a substantially impervious backing plate.
Type:
Grant
Filed:
August 13, 2014
Date of Patent:
April 18, 2017
Assignee:
CRYSTAL IS, INC.
Inventors:
Robert T. Bondokov, Kenneth E. Morgan, Leo J. Schowalter, Glen A. Stack
Abstract: In various embodiments, light-emitting devices incorporate smooth contact layers and polarization doping (i.e., underlying layers substantially free of dopant impurities) and exhibit high photon extraction efficiencies.
Type:
Grant
Filed:
February 18, 2016
Date of Patent:
April 11, 2017
Assignee:
CRYSTAL IS, INC.
Inventors:
James R. Grandusky, Leo J. Schowalter, Muhammad Jamil, Mark C. Mendrick, Shawn R. Gibb
Abstract: Reducing the microvoid (MV) density in AlN ameliorates numerous problems related to cracking during crystal growth, etch pit generation during the polishing, reduction of the optical transparency in an AlN wafer, and, possibly, growth pit formation during epitaxial growth of AlN and/or AlGaN. This facilitates practical crystal production strategies and the formation of large, bulk AlN crystals with low defect densities—e.g., a dislocation density below 104 cm?2 and an inclusion density below 104 cm?3 and/or a MV density below 104 cm?3.
Type:
Grant
Filed:
March 25, 2016
Date of Patent:
March 21, 2017
Assignee:
CRYSTAL IS, INC.
Inventors:
Robert Bondokov, Kenneth E. Morgan, Glen A. Slack, Leo J. Schowalter
Abstract: In various embodiments, non-zero thermal gradients are formed within a growth chamber both substantially parallel and substantially perpendicular to the growth direction during formation of semiconductor crystals, where the ratio of the two thermal gradients (parallel to perpendicular) is less than 10, by, e.g., arrangement of thermal shields outside of the growth chamber.
Type:
Grant
Filed:
April 15, 2015
Date of Patent:
February 28, 2017
Assignee:
CRYSTAL IS, INC.
Inventors:
Robert T. Bondokov, Shailaja P. Rao, Shawn R. Gibb, Leo J. Schowalter
Abstract: In various embodiments, an illumination device features an ultraviolet (UV) light-emitting device at least partially surrounded by an encapsulant and having a rigid lens. Downward forces is applied while the encapsulant is at least partially cured to substantially prevent partial or full detachment of the rigid lens from the light-emitting device, and/or substantially suppress formation of bubbles between the light-emitting device and the rigid lens.
Abstract: Fabrication of doped AlN crystals and/or AlGaN epitaxial layers with high conductivity and mobility is accomplished by, for example, forming mixed crystals including a plurality of impurity species and electrically activating at least a portion of the crystal.
Abstract: Bulk single crystals of AlN having a diameter greater than about 25 mm and dislocation densities of about 10,000 cm?2 or less and high-quality AlN substrates having surfaces of any desired crystallographic orientation fabricated from these bulk crystals.
Type:
Grant
Filed:
October 22, 2014
Date of Patent:
September 20, 2016
Assignee:
Crystal IS, Inc.
Inventors:
Leo Schowalter, Glen A. Slack, Juan Carlos Rojo, Robert T. Bondokov, Kenneth E. Morgan, Joseph A. Smart
Abstract: In various embodiments, methods of forming single-crystal AlN include providing a substantially undoped polycrystalline AlN ceramic having an oxygen concentration less than approximately 100 ppm, forming a single-crystal bulk AlN crystal by a sublimation-recondensation process at a temperature greater than approximately 2000° C., and cooling the bulk AlN crystal to a first temperature between approximately 1500° C. and approximately 1800° C. at a first rate less than approximately 250° C./hour.
Type:
Grant
Filed:
April 16, 2015
Date of Patent:
September 20, 2016
Assignee:
Crystal IS, Inc.
Inventors:
Sandra B. Schujman, Shailaja P. Rao, Robert T. Bondokov, Kenneth E. Morgan, Glen A. Slack, Leo J. Schowalter
Abstract: In various embodiments, a fluid is treated by flowing the fluid through a flow cell having (i) a fluid entry, (ii) a fluid exit, (iii) a treatment region disposed between the fluid entry and exit, and (iv) an interior surface reflective to ultraviolet (UV) light, and diffusively reflecting UV light emitted from one or more UV light sources to illuminate the treatment region substantially uniformly, thereby treating the fluid.
Type:
Grant
Filed:
August 29, 2014
Date of Patent:
April 26, 2016
Assignee:
CRYSTAL IS, INC.
Inventors:
Jianfeng Chen, Rajul V. Randive, Craig Moe
Abstract: In various embodiments, light-emitting devices incorporate smooth contact layers and polarization doping (i.e., underlying layers substantially free of dopant impurities) and exhibit high photon extraction efficiencies.
Type:
Grant
Filed:
March 13, 2014
Date of Patent:
March 29, 2016
Assignee:
Crystal IS, Inc.
Inventors:
James R. Grandusky, Leo J. Schowalter, Muhammad Jamil, Mark C. Mendrick, Shawn R. Gibb
Abstract: In various embodiments, an illumination device features an ultraviolet (UV) light-emitting device at least partially surrounded by an encapsulant. A barrier layer is disposed between the light-emitting device and the encapsulant and is configured to substantially prevent UV light emitted by the light-emitting device from entering the encapsulant.
Abstract: In various embodiments, methods of forming single-crystal AlN include providing a substantially undoped polycrystalline AlN ceramic having an oxygen concentration less than approximately 100 ppm, forming a single-crystal bulk AlN crystal by a sublimation-recondensation process at a temperature greater than approximately 2000° C., and cooling the bulk AlN crystal to a first temperature between approximately 1500° C. and approximately 1800° C. at a first rate less than approximately 250° C./hour.
Type:
Grant
Filed:
June 30, 2010
Date of Patent:
May 19, 2015
Assignee:
CRYSTAL IS, INC.
Inventors:
Sandra B. Schujman, Shailaja P. Rao, Robert T. Bondokov, Kenneth E. Morgan, Glen A. Slack, Leo J. Schowalter
Abstract: In various embodiments, non-zero thermal gradients are formed within a growth chamber both substantially parallel and substantially perpendicular to the growth direction during formation of semiconductor crystals, where the ratio of the two thermal gradients (parallel to perpendicular) is less than 10, by, e.g., arrangement of thermal shields outside of the growth chamber.
Type:
Grant
Filed:
June 30, 2011
Date of Patent:
May 12, 2015
Assignee:
Crystal IS, Inc.
Inventors:
Robert T. Bondokov, Shailaja P. Rao, Shawn Robert Gibb, Leo J. Schowalter
Abstract: In various embodiments, a rigid lens is attached to a light-emitting semiconductor die via a layer of encapsulant having a thickness insufficient to prevent propagation of thermal expansion mismatch-induced strain between the rigid lens and the semiconductor die.
Type:
Grant
Filed:
July 19, 2012
Date of Patent:
February 24, 2015
Assignee:
Crystal IS, Inc.
Inventors:
Leo J. Schowalter, Jianfeng Chen, James R. Grandusky