Abstract: The invention concerns a method for producing a population of particles of a polymer, wherein the polymer is poly-butylene terephthalate (=PBT) or polyethylene terephthalate (=PET) or a copolymer comprising polybutylene terephthalate and/or polyethylene terephthalate, wherein the polymer is dissolved in an organic solvent which solvent is selected such that it completely solubilizes the polymer only at a temperature of the solvent above 100° C., wherein the method comprises heating the solvent and the solid polymer immersed in the solvent at least to a first temperature, at which first temperature the polymer completely dissolves, cooling the solution until a second temperature is reached at which second temperature clouding of the solution starts, further cooling the solution at a rate in a range of 0.05 ° C./min to 5° C./min or keeping the solution at the second temperature or at a temperature up to 3° C.
Type:
Grant
Filed:
March 26, 2019
Date of Patent:
March 26, 2024
Assignee:
Evonik Operations GmbH
Inventors:
Maximilian Alexander Dechet, Stephanie Kloos, Jochen Schmidt, Wolfgang Peukert
Abstract: A process for the epoxidation of propene involves reacting propene with hydrogen peroxide, in the presence of a methanol solvent and a shaped titanium zeolite epoxidation catalyst in a fixed bed reactor. The process then involves recovering methanol from the reaction mixture, treatment of the recovered methanol by passing it through a bed of an acidic ion exchange resin, and recycling the treated methanol to the epoxidation reaction; as well as regeneration of the acidic ion exchange resin. Catalyst breakage can be reduced or avoided by washing the regenerated bed of an acidic ion exchange resin with methanol until the methanol exiting the resin bed has an apparent pH higher than 1.8, before methanol treated with the acidic ion exchange resin is recycled to the epoxidation reaction.
Abstract: Hydroxy-substituted sphingolipids are useful as constituents in cosmetic formulations. A method for preparing the sphingolipids involves reacting a lysosphingolipid with a hydroxycarboxylic acid or an intramolecular cyclic ester of a hydroxycarboxylic acid. The sphingolipids can be used for therapy or prophylaxis of cell damage, including skin cell damage and cell damage induced by UV radiation.
Type:
Application
Filed:
January 5, 2022
Publication date:
March 21, 2024
Applicant:
Evonik Operations GmbH
Inventors:
Xin LU, Jennifer Schild, Sandra Nattland, Marita Regina Baetsen, Ursula Maczkiewitz, Hans Henning Wenk, Monica Desiree van Logchem, Lisa Maus
Abstract: An apparatus and corresponding process can be used for producing nanocarriers and or nanoformulations and corresponding process products. The apparatus is characterized by a vertical orientation of the feed conduits leading to active element. The feed conduits are nested within one another and are axially movable in terms of their orientation to one another. The process provides for the mixing of at least two liquid phases with different acidities. The volume flow of the first phase is greater than that of the second phase.
Type:
Application
Filed:
March 8, 2022
Publication date:
March 21, 2024
Applicant:
Evonik Operations GmbH
Inventors:
Mario GOMEZ, Jürgen Erwin Lang, Marcel Arndt
Abstract: The use of long-chain citric acid esters as additives in aqueous polymer dispersions for production of porous polymer coatings, preferably for production of porous polyurethane coatings, is described.
Type:
Grant
Filed:
May 26, 2021
Date of Patent:
March 19, 2024
Assignee:
Evonik Operations GmbH
Inventors:
Michael Klostermann, Kai-Oliver Feldmann, Jan Marian von Hof, Marvin Jansen, Sina Arnold
Abstract: A polymeric blend contains a polyether block amide and a thermoplastic polymer, where the polyether block amide is based on a subunit 1 and a subunit 2. Subunit 1 is composed of at least one linear aliphatic diamine containing 5 to 15 carbon atoms and at least one linear aliphatic dicarboxylic acid containing 6 to 16 carbon atoms. Subunit 2 is composed of at least one polyether diol containing at least 3 carbon atoms per ether oxygen and primary OH groups at the chain ends. The sum total of the carbon atoms from diamine and dicarboxylic acid is an odd number and is 19 or 21 carbon atoms. The number-average molar mass of the subunit 2 is 200 to 900 g/mol. The thermoplastic polymer is selected from an ethylene/vinylene acetate, a thermoplastic polyester elastomer, a polyolefin elastomer, thermoplastic polyurethane, or any mixture thereof.
Type:
Application
Filed:
December 23, 2021
Publication date:
March 14, 2024
Applicant:
Evonik Operations GmbH
Inventors:
Chenyu Ye, Kathrin Salwiczek, Dominik Vogel, Beiyuan Zhu, Michael Gerhard Hagemann
Abstract: The invention relates in particular to a process for the preparation of DL/LD-methionine diketopiperazine (I) characterized in that a DD/LL-methionylmethionine-containing aqueous solution or suspension, which has a pH of 3 to 7, measured using a pH electrode at 20° C., is reacted at a temperature of 150 to 220° C., preferably at 170 to 210° C., until an aqueous solution or suspension has formed containing at least a proportion of 30 mol %, preferably 50 mol %, especially 60 mol % of DL/LD-methionine diketopiperazine, based on the total content of DL/LD- and DD/LL-methionine diketopiperazine in the reaction mixture. This process forms part of an overall process for the preparation of DL/LD-methionylmethionine, which is obtained by hydrolysis from the DL/LD-methionine diketopiperazine (I) produced initially.
Type:
Application
Filed:
December 23, 2021
Publication date:
March 14, 2024
Applicant:
Evonik Operations GmbH
Inventors:
Sascha BRAUNE, Geert VAN EESTER, Hans-Joachim HASSELBACH, Claudia DYBALLA
Abstract: Brushware contains the constituents of monofilaments or bristles, and at least one head, handle, and/or neck. The constituents contain or are made of polymers from the same polymer class selected from among polymers and/or copolymers, and wherein the polymer class is selected from polyamides or polyesters.
Abstract: A composition contains glycolipids and triethyl citrate (TEC). The TEC can assist in stabilizing a foam of a corresponding aqueous composition. A method can be used for preparing a corresponding formulation, preferably a cosmetical or pharmaceutical formulation, by providing the composition and diluting the composition. The pH of the composition may be adjusted during the dilution by adding an organic or inorganic base.
Type:
Grant
Filed:
March 8, 2021
Date of Patent:
March 5, 2024
Assignees:
Evonik Operations GmbH, Evonik Dr. Straelmans GmbH
Inventors:
Kathrin Daniela Brandt, Stefan Julian Liebig, Hans Henning Wenk, Manuela Salmina-Petersen, Christoph Tölle, Alina Muss
Abstract: The invention provides a process for regenerating a catalyst used for the hydrogenation of an aromatic species, consisting of several steps. First the system is purged with nitrogen, then air is metered in stepwise, and the addition of nitrogen is subsequently ended until only air is present.
Type:
Grant
Filed:
December 10, 2021
Date of Patent:
March 5, 2024
Assignee:
Evonik Operations GmbH
Inventors:
Johan Anton, Michael Grass, Johannes Kraft, Thomas Schneider, Grzegorz Ziomek
Abstract: A polymer composition can be used for selective absorbing sintering, SAS, or selective inhibition sintering, SIS. The polymer has open mesopores and the cumulative pore volume distribution of the mesopores, measured to DIN 66134, is at least 0.01 cm3/g.
Type:
Grant
Filed:
October 26, 2021
Date of Patent:
March 5, 2024
Assignee:
Evonik Operations GmbH
Inventors:
Wolfgang Diekmann, Maik Grebe, Franz-Erich Baumann, Wolfgang Christoph, Sylvia Monsheimer, Beatrice Küting
Abstract: The present invention relates to a computer-implemented method for identifying an incorrectly or non-calibrated infrared spectrometer, comprising the steps of a) recording an infrared spectrum of a sample with a first infrared spectrometer to provide a sample infrared spectrum, b) recording an infrared spectrum of the same sample as in step a) with a second infrared spectrometer to provide a reference infrared spectrum, wherein said second spectrometer is a correctly calibrated infrared spectrometer, or b?) providing a reference spectrum of the same sample as in step a), wherein said reference spectrum was recorded on a second infrared spectrometer, which is a correctly calibrated spectrometer, c) determining a difference between the wavelength of each extreme point in the sample of step a) and the wavelength of each extreme point in the reference spectrum of step b) or b?), and d) indicating the infrared spectrometer of step a) as incorrectly calibrated or non-calibrated, when at least one difference was det
Type:
Grant
Filed:
December 13, 2019
Date of Patent:
February 27, 2024
Assignee:
Evonik Operations GmbH
Inventors:
Ingolf Reimann, Joachim Reising, Christoph Mueller
Abstract: In a cyclic anthraquinone process for producing hydrogen peroxide, which comprises a distillation unit with vapor compression for concentrating hydrogen peroxide, aqueous condensate from the distillation unit is passed over a bed of a cation exchange resin in its protonated from to provide a purified condensate, and the purified condensate is used as extractant for extracting hydrogen peroxide in the anthraquinone process, as column reflux for the distillation unit or as a diluent for diluting an aqueous hydrogen peroxide solution.
Type:
Grant
Filed:
May 26, 2021
Date of Patent:
February 27, 2024
Assignee:
Evonik Operations GmbH
Inventors:
Nils Henning Seidel, Johannes Kamp, Jürgen Glenneberg, Christian Panz, Eduardo Federico Arévalo Saade, Hari Prasad Mangalapally
Abstract: A process for removing butenes from C4-hydrocarbon streams containing butanes and butenes involves extractive distillation with a suitable solvent. The process also involves heat integration, which allows utilization of the heat of the solvent for heating and/or at least partly evaporating various streams.
Type:
Application
Filed:
January 21, 2022
Publication date:
February 22, 2024
Applicant:
Evonik Operations GmbH
Inventors:
Philip Lutze, Stephan Peitz, Armin Matthias Rix, Tanita Valèrie Six, Moritz Schröder, Niklas Paul
Abstract: A process for removing butenes from C4-hydrocarbon streams containing butanes and butenes involves extractive distillation with a suitable solvent. The process also involves heat integration, which allows utilization of the heat of the solvent for heating and/or at least partly evaporating various streams.
Type:
Application
Filed:
January 21, 2022
Publication date:
February 22, 2024
Applicant:
Evonik Operations GmbH
Inventors:
Tanita Valèrie SIX, Armin Matthias Rix, Moritz Schröder, Stephan Peitz, Niklas Paul, Philip Lutze, Andreas Oldenkott, Franz-Josef Stock, Marius Tiesbohnenkamp
Abstract: A production process can produce foam materials from polymer compositions. This process involves preheating in the foaming of polymers containing blowing agents and subsequent foaming by a thermal process assisted by microwaves.
Type:
Grant
Filed:
December 19, 2019
Date of Patent:
February 20, 2024
Assignee:
Evonik Operations GmbH
Inventors:
Thomas Richter, Andreas Liebe, Christian Traßl, Florian Becker, Vincent Ma Junyong
Abstract: A capsule shell contains 40 to 99% by weight of a core-shell polymer and 1 to 60% by weight of a cellulose. The core-shell polymer contains 50 to 90% by weight of a core, containing polymerized units of 65 to 75% by weight of ethyl acrylate and 25 to 35% by weight of methyl methacrylate; and 10 to 50% by weight of a shell, containing polymerized units of 45 to 55% by weight of ethyl acrylate and 45 to 55% by weight of methacrylic acid.
Abstract: The production of SiOC-bonded, linear polydimethylsiloxane-polyoxyalkylene block copolymers comprising repeating (AB) units by reaction of polyether diols with trifluoromethanesulfonic acid-acidified, equilibrated ?,?-diacetoxypolydimethylsiloxanes is described, wherein the reaction is undertaken by adding a solid, liquid or gaseous base, optionally using inert solvents.