Patents Assigned to Heraeus Quarzglas GmbH & Co., KG
  • Patent number: 11459262
    Abstract: A known method for homogenizing glass includes the following steps: providing a cylindrical blank composed of the glass, having a cylindrical outer surface which extends between a first end face and a second end face, forming a shear zone in the blank by softening a longitudinal section of the blank and subjecting it to a thermal-mechanical intermixing treatment, and moving the shear zone along the longitudinal axis of the blank. To reduce the risk of cracks and fractures during homogenizing, it is proposed that a thermal radiation dissipator is used that at least partially surrounds the shear zone, the lateral dimension of which in the direction of the longitudinal axis of the blank is greater than the shear zone and smaller than the length of the blank, the thermal radiation dissipator being moved synchronously with the shear zone along the longitudinal axis of the blank.
    Type: Grant
    Filed: October 24, 2019
    Date of Patent: October 4, 2022
    Assignee: Heraeus Quarzglas GmbH & Co. KG
    Inventors: Stephan Thomas, Jan Vydra, Martin Trommer, Michael Huenermann, Andreas Langner, Walter Lehmann, Stefan Hengster, Klaus Becker
  • Publication number: 20220306513
    Abstract: In a method of manufacturing a tube of quartz glass by molding a hollow cylinder having a wall thickness of at least 20 mm, the cylinder is continuously fed under rotation about a rotational axis into a heating zone at a relative feed rate VC, softened and radially expanded under the effect of a gas pressure. A tube strand is continuously formed and is withdrawn at a withdrawal rate VT. In order to mold thick-walled initial hollow cylinders of quartz glass into tubes with larger diameter, the gas pressure is used as an actuating variable of a diameter regulation for the tube outer diameter or for a geometrical correlated parameter thereof, and in a pressure build-up phase the gas pressure is gradually increased from a lower initial value to a higher final value, and that the following applies to the ratio of VC and VT:VT=VC±0.2·VC.
    Type: Application
    Filed: March 29, 2022
    Publication date: September 29, 2022
    Applicant: Heraeus Quarzglas GmbH & Co. KG
    Inventors: Matthias SÖHN, Boris GROMANN, Eduard VISNOW
  • Publication number: 20220267188
    Abstract: Known methods of producing a three-dimensional glass object comprise the step of shaping of a glass fiber, wherein the glass fiber provided with a protective sheath is fed continuously to a heating source, the protective sheath is removed under the influence of heat, and the glass fiber is softened. In order to facilitate the production of filigree or optically distortion-free and transparent glass objects as much as possible, and also enable the adjustment of optical and mechanical properties with high spatial resolution, in one aspect the glass fiber has a protective sheath with a layer thickness in the range of 10 nm to 10 ?m.
    Type: Application
    Filed: April 30, 2020
    Publication date: August 25, 2022
    Applicant: Heraeus Quarzglas GmbH & Co. KG
    Inventors: Miriam Sonja HÖNER, Achim HOFMANN
  • Patent number: 11390556
    Abstract: A diffuser material of synthetically produced, pore-containing quartz glass and a method for the manufacture of a molded body consisting fully or in part thereof. The diffuser material has a chemical purity of at least 99.9% SiO2, a cristobalite content of not more than 1%, and a density in the range of 2.0 to 2.18 g/cm3. Starting therefrom, to indicate a diffuser material which is improved with respect to diffuse reflectivity with Lambertian behavior over a wide wavelength range, high material homogeneity and UV radiation resistance, the quartz glass has a hydroxyl group content in the range of at least 200 wt. ppm and at least 80% of the pores have a maximum pore dimension of less than 20 ?m.
    Type: Grant
    Filed: February 13, 2017
    Date of Patent: July 19, 2022
    Assignee: HERAEUS QUARZGLAS GMBH & CO. KG
    Inventors: Gerrit Scheich, Frank Nuernberg, Andreas Goetzendorfer, Nadine Tscholitsch, Bernhard Franz, Ursula Klett, Matthew Donelon
  • Publication number: 20220204387
    Abstract: Provided is a titanium-containing quartz glass having excellent UV absorption. The quartz glass absorbs ultraviolet rays having a wavelength of 250 nm or less, ozone generation-related adverse effects on the human body, are prevented, a decrease in transmittance of the quartz glass in the range from near-ultraviolet to visible light due to being colored when irradiated with ultraviolet rays does not occur, absorption build-up or lamp burst-inducing deformation build-up, which is caused by a structural change in the quartz glass that occurs in the range of 200-300 nm when irradiated with ultraviolet rays, is suppressed, and a decrease in transmittance at intended wavelength ranges does not occur even when exposed to ultraviolet rays. The titanium-containing quartz glass having excellent UV absorption is colorless, wherein the average concentration of titanium is 10-500 ppm, the concentration of OH group is 10-350 ppm.
    Type: Application
    Filed: January 17, 2020
    Publication date: June 30, 2022
    Applicants: Shin-Etsu Quartz Products Co., Ltd., Heraeus Quarzglas Gmbh & Co. KG
    Inventors: Atsushi SHIMADA, Katsuhide ORIKASA, Makoto TANAKA, Tomoichi KUMATA, Hiromi TARUKAWA
  • Publication number: 20220185720
    Abstract: Described is a process for the production of synthetic fused silica in which the deposition surface is located for a period of at least 50% of the build-up time of the soot body at a burner distance in which the horizontally integrated luminous intensity of the flame of the burner used in the targetless state is still at least ? of the maximum horizontally integrated luminous intensity of the flame.
    Type: Application
    Filed: December 16, 2021
    Publication date: June 16, 2022
    Applicant: Heraeus Quarzglas GmbH & Co. KG
    Inventors: Martin THÜRER, Walter LEHMANN, Martin TROMMER
  • Publication number: 20220185716
    Abstract: Described is a process for the production of synthetic fused silica in which the feedstock vapor is reacted from an organosilicon starting compound and any combustible burner auxiliary gases at an air number in the burner of less than or equal to 1.00. Furthermore, one embodiment relates to a corresponding apparatus.
    Type: Application
    Filed: December 16, 2021
    Publication date: June 16, 2022
    Applicant: Heraeus Quarzglas GmbH & Co. KG
    Inventors: Martin THÜRER, Walter LEHMANN, Martin TROMMER
  • Publication number: 20220185715
    Abstract: Described is a method of producing synthetic fused silica in which the synthetic flame used in the method has a ratio of the Full Width at Half Maximum (FWHMvert) vertical luminous intensity to the Full Width at Half Maximum (FWHMhori) horizontal luminous intensity greater than 10 in a targetless state, the luminous intensities being measured in candela/mm2.
    Type: Application
    Filed: December 16, 2021
    Publication date: June 16, 2022
    Applicant: Heraeus Quarzglas GmbH & Co. KG
    Inventors: Martin THÜRER, Walter LEHMANN, Martin TROMMER
  • Patent number: 11339076
    Abstract: One aspect relates to a process for the preparation of a quartz glass body. The process includes providing a silicon dioxide granulate I prepared from a pyrogenically produced silicon dioxide powder, treating the silicon dioxide granulate I with a reactant at a temperature in a range from 1000 to 1300° C., and making a glass melt out of the silicon dioxide granulate. A quartz glass body is made out of at least a part of the glass melt. Furthermore, one aspect relates to a quartz glass body obtainable by this process. Furthermore, one aspect relates to a light guide, an illuminant, and a formed body, each of which is obtainable by further processing of the quartz glass body. One aspect additionally relates to a process for the preparation of a silicon dioxide granulate II.
    Type: Grant
    Filed: December 16, 2016
    Date of Patent: May 24, 2022
    Assignee: Heraeus Quarzglas GmbH & Co. KG
    Inventors: Matthias Otter, Thomas Kayser, Mirko Wittrin
  • Publication number: 20220153626
    Abstract: Doped quartz glass components for use in a plasma-assisted manufacturing process contain at least one dopant which is capable of reacting with fluorine to form a fluoride compound, and the fluoride compound has a boiling point higher than that of SiF4. The doped quartz glass component has high dry-etch resistance and low particle formation, and has uniform etch removal when used in a plasma-assisted manufacturing process. The doped quartz glass has a microhomogeneity defined by (a) a surface roughness with an Ra value of less than 20 nm after the surface has been subjected to a dry-etching procedure as specified in the description, or (b) a dopant distribution with a lateral concentration profile in which maxima of the dopant concentration are at an average distance apart of less than 30 ?m.
    Type: Application
    Filed: February 27, 2020
    Publication date: May 19, 2022
    Applicant: Heraeus Quarzglas GmbH & Co. KG
    Inventors: Mark STAMMINGER, Mario SUCH
  • Patent number: 11299417
    Abstract: The invention relates to a process for preparing a quartz glass body comprising the process steps i.) Providing a silicon dioxide granulate, ii.) Making a glass melt from the silicon dioxide granulate in a melting crucible, and iii.) Making a quartz glass body from at least a part of the glass melt, wherein the melting crucible is comprised in an oven and is made of at least one material comprising tungsten or molybdenum or a combination thereof. The invention further relates to a quartz glass body which can be obtained by this process. Further, the invention relates to a light guide, an illuminant and a formed body, each of which can be obtained by processing the quartz glass body further.
    Type: Grant
    Filed: December 16, 2016
    Date of Patent: April 12, 2022
    Assignee: Heraeus Quarzglas GmbH & Co. KG
    Inventors: Matthias Otter, Walter Lehmann, Michael Hünermann, Nils Christian Nielsen, Nigel Robert Whippey, Boris Gromann, Abdoul-Gafar Kpebane
  • Patent number: 11267745
    Abstract: A method for the production of synthetic quartz glass using a special cleaning device is provided. The method includes (a) evaporating a production material containing a polymerizable polyalkylsiloxane compound while forming a production material vapor, (b) passing the production material vapor resulting from step (a) through a cleaning device to purify the production material vapor, (c) supplying the purified production material vapor resulting from step (b) to a reaction zone in which the purified production material vapor is converted to SiO2 particles through oxidation and/or through hydrolysis, (d) depositing the SiO2 particles resulting from step (c) on a deposition surface, and optionally drying and vitrifying the deposited SiO2 particles resulting from step (d) to form synthetic quartz glass. The cleaning device includes a bulk of porous silica particles which have a BET specific surface area of at least 2 m2/g. A device for carrying out the method is also provided.
    Type: Grant
    Filed: December 15, 2015
    Date of Patent: March 8, 2022
    Assignee: HERAEUS QUARZGLAS GMBH & CO. KG
    Inventors: Hilmar Laudahn, Klaus-Uwe Badeke, Martin Trommer
  • Publication number: 20220041488
    Abstract: A process for the production of a fluorinated quartz glass including the steps of generating SiO2 particles in a synthesis burner; depositing the resulting SiO2 particles into a body; and vitrifying the resulting body, wherein a fluorinating agent having a boiling point greater than or equal to ?10° C. is supplied to the synthesis burner.
    Type: Application
    Filed: August 6, 2021
    Publication date: February 10, 2022
    Applicant: Heraeus Quarzglas GmbH & Co. KG
    Inventors: Stefan OCHS, Thomas KAYSER, Martin TROMMER, Andreas LANGNER, Sascha PIHAN, Kay SCHUSTER, Michael Hünermann
  • Publication number: 20220041489
    Abstract: A process for producing a fluorinated quartz glass is described, including providing an SiO2 soot body; reacting the SiO2 soot body with a fluorinating agent having a boiling point of greater than or equal to ?10° C. to obtain a fluorinated SiO2 soot body; and vitrifying the fluorinated SiO2 soot body.
    Type: Application
    Filed: August 6, 2021
    Publication date: February 10, 2022
    Applicant: Heraeus Quarzglas GmbH & Co. KG
    Inventors: Stefan OCHS, Martin TROMMER, Thomas KAYSER
  • Patent number: 11236002
    Abstract: One aspect relates to a process for the preparation of a quartz glass body. The process includes providing a silicon dioxide granulate from a pyrogenically produced silicon dioxide powder, making a glass melt out of silicon dioxide granulate, and making a quartz glass body out of at least part of the glass melt. The size of the quartz glass body is reduced to obtain a quartz glass grain. The quartz glass body is processed to make a preform and an opaque quartz glass body is made from the preform. One aspect further relates to an opaque quartz glass body which is obtainable by this process. One aspect further relates to a reactor and an arrangement, which are each obtainable by further processing of the opaque quartz glass body.
    Type: Grant
    Filed: December 16, 2016
    Date of Patent: February 1, 2022
    Assignee: Heraeus Quarzglas GmbH & Co. KG
    Inventors: Matthias Otter, Michael Hünermann, Nils Christian Nielsen, Frank Wessely, Andreas Schreiber, Björn Roos, Gerrit Scheich
  • Patent number: 11214505
    Abstract: One aspect is a process to producing a synthetic quartz glass, including an annealing treatment that includes: putting a synthetic quartz glass as a parent material into a heat treatment furnace; elevating a temperature in the heat treatment furnace to a prescribed keeping temperature that is equal to or higher than the annealing point; keeping the keeping temperature; annealing the synthetic quartz glass; and taking the synthetic quartz glass out of the heat treatment furnace. The process includes determining an annealing rate v [° C./h] of the annealing step based on a value of S/V [mm2/mm3], wherein S [mm2] is the surface area of the synthetic quartz glass as a parent material and V [mm3] is the volume thereof and a target birefringence Re [nm/cm] for the synthetic quartz glass after the annealing, and the annealing step is performed at the determined annealing rate v.
    Type: Grant
    Filed: April 23, 2018
    Date of Patent: January 4, 2022
    Assignees: Shin-Etsu Quartz Products Co., Ltd., Heraeus Quarzglas GmbH & Co. KG
    Inventor: Manabu Utsumi
  • Publication number: 20210371321
    Abstract: One aspect is a method for producing a multilayered silica glass body. The method involves producing a multilayered silica glass body in which a transparent silica glass layer is provided on the surface of a siliceous substrate made of a siliceous material. The method includes preparing the siliceous substrate, preparing a silica slurry in which silica particles are dispersed in a liquid, applying the silica slurry to the surface of the siliceous substrate, leveling the silica slurry applied to the surface of the siliceous substrate by applying vibration to the siliceous substrate, drying the leveled silica slurry, and vitrifying the dried silica slurry by heating to form a transparent silica glass layer. As a result, a transparent silica glass layer of uniform thickness is obtained at excellent yield, and a method for producing a multilayered silica glass body easily in a short time is provided.
    Type: Application
    Filed: September 3, 2019
    Publication date: December 2, 2021
    Applicants: HERAEUS QUARZGLAS GMBH & CO. KG, SHIN-ETSU Quartz Products Co., Ltd.
    Inventors: Tatsuya MORI, Akihiko SUGAMA
  • Patent number: 11053126
    Abstract: One aspect is a production process including feeding a feed material composition into a reaction zone at a feeding position, wherein the feed material composition is liquid or gaseous or both; reacting the feed material composition in the reaction zone into a first plurality of particles by a chemical reaction; depositing the first plurality of particles onto a substrate surface of a substrate, thereby obtaining a porous silicon dioxide material, having a pore structure, in the form of up to 20 layers superimposing the substrate surface; at least partially removing the porous silicon dioxide material from the substrate surface; and modifying the pore structure of the porous silicon dioxide material, thereby obtaining the porous silicon dioxide material having a further pore structure.
    Type: Grant
    Filed: October 26, 2018
    Date of Patent: July 6, 2021
    Assignee: Heraeus Quarzglas GmbH & Co. KG
    Inventors: Sascha Pihan, Jörg Becker, Christian Neumann
  • Patent number: 11053152
    Abstract: One aspect relates to a process for the preparation of a quartz glass body. The process includes providing a silicon dioxide granulate, making a glass melt out of the silicon dioxide granulate, and making a quartz glass body out of at least a part of the glass melt. In one aspect, providing a silicon dioxide granulate includes providing of a silicon dioxide powder and processing of the powder to obtain a silicon dioxide granulate including the spray drying of a silicon dioxide slurry using a nozzle. The nozzle has a contact surface to the slurry made of glass, plastic or a combination thereof. Furthermore, one aspect relates to a quartz glass body obtainable by this process. Furthermore, one aspect relates to the preparation of a silicon dioxide granulate. One aspect also relates to a light guide, an illuminant, and a formed body, made from processing of the quartz glass body.
    Type: Grant
    Filed: December 16, 2016
    Date of Patent: July 6, 2021
    Assignee: Heraeus Quarzglas GmbH & Co. KG
    Inventors: Matthias Otter, Mirko Wittrin, Markus Wilde
  • Publication number: 20210163336
    Abstract: Known heating burners for producing a welded joint between components of quartz glass include a burner head in which at least one burner nozzle is formed, a burner-head cooling system for the temperature control of the burner head and a supply line connected to the burner nozzle for a fuel gas. Starting from this, to modify a heating burner in such a way that impurities in the weld seam between quartz-glass components to be connected are largely avoided, it is suggested that the burner head should include a base body of silver or of a silver-based alloy.
    Type: Application
    Filed: February 16, 2021
    Publication date: June 3, 2021
    Applicant: Heraeus Quarzglas GmbH & Co. KG
    Inventor: Oliver GANZ