Abstract: A method for forming intermetallic and intermetallic-type precursor alloys for subsequent mechanical alloying applications. Elemental powders are blended in proportions approximately equal to their respective intermetallic compounds. Heating of the blend results in the formation of intermetallic compounds whereas lack of heating results in intermetallic-type powder without the intermetallic structure. The resultant powder is then blended to form a final alloy. Examples involving aluminum-titanium alloys are discussed.

Abstract: A novel nickel-base high temperature alloy body preferably containing about 22% chromium, sufficient aluminum and titanium to provide a .gamma.' precipitate structure, additional strengthing elements and oxidic yttrium in finely dispersed form. The alloy body has an elongated crystal structure and is characterized by high strength along with excellent hot corrosion and oxidation resistance.

Abstract: A system for obtaining a sample of particulate material being processed under seal from the air in a batch-type rotary grinding mill which permits sampling of material being processed without disturbing the seal. The system is comprised of a sampling member and a plug member which can be interchanged under seal while maintaining the seal in the mill.

Abstract: A process for obtaining forged low density aluminum alloys having high strength comprising control of the extrusion and forging conditions, and dispersion strengthened Al-Mg-Li alloys derived from such process.

Abstract: A consumable electrode including a core wire and a coating adapted for welding clad steel products. The resulting weld deposit overcomes the problem of iron dilution which tends to degrade the weld when available electrodes are utilized. Such clad products are often exposed to sulfur and acidified chloride environments.

Abstract: A process for producing a single crystal alloy object comprising providing a preform having coarse columnar crystals in a discard portion, isolating, by cutting, one of the columnar crystals to form a seed crystal connected to metal in a product portion of said preform, zone annealing the thus prepared preform to produce single crystal structure and discarding the discard portion of the preform.

Abstract: A pipe joint especially suited for coupling two high strength, corrosion resistant pipes. The box end is expanded by a cold working operation thereby eliminating metallurgical problems and changes associated with hot working operations. A sleeve is nested into the internal transition section of the box end to form a sealing surface between the two pipes. Moreover, the sleeve presents a smooth uninterrupted, internal flow surface.

Abstract: An improved method is provided for producing mechanically alloyed powders on a commercial scale comprising milling the components of the powder product in a gravity-dependent-type ball mill to produce a powder having a characteristic apparent density. Powder so produced will have reached an acceptable processing level and will meet one criterion for determining whether it will be suitable for further processing to the end product.

Abstract: A method for consolidating powder utilizing slurry extrusion or rolling techniques. A metallic powder, binder and boron containing activator are mixed together to form a slurry. The slurry is introduced into an active forming apparatus whereupon it is formed into an object of predetermined shape and sintered.

Abstract: A method for directly fabricating weld wire utilizing powder metallurgy techniques. Nickel containing powder, mixed into a slurry, is continuously extruded in an auger-type extrusion press into rod. The rod is consolidated to densities greater than about 91% theoretical density for subsequent rough handling.

Abstract: Aluminum-base alloys and a method of preparing aluminum-base alloys by mechanical alloying in the presence of a carbidiferous processing aid wherein a strong carbide former such as titanium is included so as to produce carbides in the final alloy more thermally stable at temperatures in excess of 100.degree. C. than Al.sub.4 C.sub.3.

Abstract: A process for producing composite materials which comprises subjecting particles of a malleable matrix material, i.e., a metal or alloy or the components of a matrix alloy and particles of a reinforcing material such as a carbide or an oxide or an intermetallic to energetic mechanical milling under circumstances to insure the pulverulent nature of the mill charge so as to enfold matrix material around each of said reinforcing particles to provide a bond between the matrix material and the surface of the reinforcing particle. The process is exemplified by the use of aluminum alloy as the matrix material and silicon carbide as the reinforcing particles. Reinforcing particles are present in an amount of about 0.2 to about 30 volume percent of total matrix and reinforcing particles. The invention is also directed to the product of the process.

Abstract: Malleability and resistance to cracking of alloys containing nickel, copper, sulfur, etc. are enhanced through the co-presence of cerium and magnesium.

Abstract: A batch-type rotary grinding mill operable under seal to the atmosphere is provided with a discharge system which permits discharge of material from the mill under seal and without disturbing the seal in the mill. The discharge system comprises at least one discharge chute which is sealably secured to the shell wall, spiraling adjacent to the shell and traversing the shell wall from one end to the other. The material is discharged from the discharge chute via a hollow trunnion which, preferably, contains a conveyor to aid in passing the material out of the mill into an environmentally protected device.

Abstract: A dispersion strengthened mechanically alloyed aluminum-base alloy system is provided by a process comprising solution treating an alloy consisting essentially of, by weight, about 0.5 up to about 4% lithium, above 1% up to about 5% magnesium, about 0.5% up to about 2% carbon, a small but effective amount of oxygen which does not exceed 1%, and the balance essentially aluminum, the dispersoid content of the alloy being up to about 8 volume %. Preferred embodiments of the alloy are in the solution treated or solution treated and underaged condition are characterized by an improved combination of strength, low density, ductility, and fracture toughness.

Abstract: A dispersion strengthened aluminum-base alloy system is provided which is prepared by mechanical alloying and is characterized by an improved continuation of properties over binary aluminum-lithium alloys. The alloy system contains, by weight, about 0.5% up to about 4% Li, about 0.05 up to about 2% carbon, about 0.1 up to about 3% oxygen, at least one of the elements magnesium or copper in an amount of up to about 5% each, provided the total amount of said magnesium and copper does not exceed about 8%, and a dispersion strengthening agent in the amount of about 2% up to about 8% by volume.

Abstract: A canless method for hot working a nickel-base gas atomized alloy powder. The powder is blended with nickel powder, consolidated and sintered to a sufficient green strength. The surface of the resultant form is sealed to create an oxygen impervious layer so as to prevent oxidation therein. The sealed surface, in a sense, acts as a can. The form is then reheated and hot worked.

Abstract: Compositions of matter are provided wherein cis-platinum (II) and cis-palladium (II) moieties having amine substituents are bonded to anionic macromolecular entities. These compositions of matter may have improved solubility in the plasma and are effective antitrypanosomal and antitumor agents in mammals. Alternatively, the compositions of matter may be insoluble in water and particularly adapted for in situ implantation into tumerous masses.

Abstract: A process for preparing hydrogen evolution cathodes comprises plasma spraying or flame spraying AB.sub.5 intermetallic compound powder alone or in association with nickel, nickel alloy or iron powder onto a steel or nickel substrate and thereafter reducing the sprayed substrate at a temperature of up to about 650.degree. C.

Abstract: A cathode for hydrogen evolution comprising a substrate stable in aqueous alkaline media having on the surface thereof a coating of particles of an AB.sub.N intermetallic, and optionally particles of a metal inert in the electrolyte, e.g., nickel, adhered to the substrate by sintered polytetrafluoroethylene or similar polymer.