Abstract: A a process for making a lubricious composition useful for preventing seizing of threaded fasteners in application to the threaded surface(s) thereof, comprising: (a) forming metal wire by drawing of metal source material through a wire drawing die; (b) lubricating the wire drawing die with an oil lubricant in forming the metal wire, to produce as a by-product thereof a metal flake/oil mixture; (c) separating the metal flake/oil mixture to recover a metal flake/oil suspension; and (d) formulating the metal flake/oil suspension in a metal flake-containing lubricant composition. The invention in another aspect relates to a product of such process. In a specific compositional aspect, the invention relates to a composition comprising an oil-based vehicle, 15%-35% by weight particulate metal (e.g., microscopic flake aluminum), based on the total weight of the composition, and 10%-30% by weight graphite, based on the total weight of the composition.

Abstract: A radiation surface-curable RTV silicone composition which subsequent to radiation surface curing thereof, is interiorly moisture-curable in character. Such radiation surface-curable, interiorly moisture-curable RTV silicone composition comprises: a silanol-containing silicone; a silane cross-linker for the silicone, such cross-linker having joined directly to a silicon atom thereof an ethylenically unsaturated functional group and at least two hydrolyzable functional groups; and a photoinitiator effective for radiation surface curing of the silicone composition. Also disclosed is a "liquid potting system" formulation, which is irradiated subsequent to dispensing thereof at the potting locus, so that the radiation surface-cured skin layer overlies and contains (cooperatively with the associated bounding surface(s) of the potting locus) the uncured liquid, so that the potted structure or material is encapsulated in a liquid (damping) medium.

Abstract: The invention relates to a dispensing process particularly for a sealing/adhesive product which comprises at least one step of pumping the sealing/adhesive product to allow a step of distribution thereof onto at least one part to be sealed, such as for example a motor vehicle mechanical component; an intermediate step of deaeration of the sealing/adhesive product, so as to optimize its distribution on the part to be sealed, is provided between the pumping step and the distribution step. The apparatus for dispensing the sealing/adhesive product (14) comprises elements (2) for feeding the sealing/adhesive product to elements (4) for distributing it onto at least one part (5) to be sealed and sealing/adhesive product deaeration means (3) which cooperate with the pumping and distribution elements for the uniform deposition of the sealant/adhesive on the part.

Abstract: A curable thiol-ene composition specially adapted for use as a primary coating on optical fibers comprises a polythiol and a compound having a plurality of norbornene groups thereon, are characterized in that one of either the compound having the plurality of norbornene groups or the polythiol has a backbone of a poly(tetramethylene oxide), or is an oligomer thereof, and the poly(tetramethylene oxide) has a molecular weight of between 250 and 5,000. The formulations are relatively low viscosity liquids at practical application temperatures and cure substantially completely with very low irradiation fluence. The formulations cure in ambient air. There is no need to exclude oxygen or to control humidity. The formulations of the invention can be cured using low intensity UV lamps which do not generate significant amounts of heat. The cured products have excellent low temperature flexibility, good humidity and water absorbtion resistance and good thermal oxidative stability.

Abstract: Stable thiol-ene compositions are provided which comprise a polythiol, a polyene and a stabilizer system comprising an alkenyl substituted phenolic compound having a formula: ##STR1## wherein R.sup.1, R.sup.2 and R.sup.3 are independently selected from the group consisting of H, OR, a C.sub.1 -C.sub.8 alkyl, substituted alkyl, alkenyl or substituted alkenyl, a C.sub.6 -C.sub.20 aryl or substituted aryl, or a cyano group; R.sup.4 is H, R, OR, halogen, COR, COOR, or SR; R.sup.5 is OH, OR, OCOR, OCOOR, OCONHR, or OTMS; R is a C.sub.1 -C.sub.6 alkyl, a cycloalkyl, or a C.sub.6 -C.sub.20 caryl or substituted aryl; x and y are 1, 2, or 3; z is 0, 1, or 2; and x+y+z=2, 3, or 4; or a formula: ##STR2## where x, y, z, w, R.sup.1 R.sup.2 R.sup.3, R.sup.4 and R.sup.5 are defined as above, except that x+y+z=2-6, and R.sup.6 is CH.sub.2, C(CH.sub.3).sub.2, O, S, or SO.sub.

Abstract: Vibration dampening hydrosilation cured silicone formulations which cure at room temperature and, after a subsequent heat cure cycle, provide good primerless adhesion to aluminum and titanium substrates and improved adhesion to polymeric composite materials such as polyimide/glass fiber composite materials. The composition includes (a) a polyorganosiloxane having plural alkenyl groups thereon; (b) a polyorganosiloxane having plural silicon hydride groups thereon; (c) a hydrosilation catalyst, and (d) a combination of adhesion promoter compounds including at least one silane adhesion promoter compound; triallyl isocyanurate; and diallyl maleate. Still further improvements to polyimide substrates are provided when a primer is employed or the substrate is treated by a very brief exposure to a flame or to UV irradiation.

Abstract: A process for treating waste washing water, which is only slightly affected by temperature, can dispense with any chemical, and wherein the quality of treated water is not affected by a change in the waste water concentration. The process comprises conducting impregnation with an impregnant having a composition comprising triethylene glycol dimethacrylate, 2-hydroxyethyl methacrylate, lauryl methacrylate, nonionic surfactant and azobisisobutyronitrile; separating the impregnant thereafter; washing the surface of the impregnated article with water; and treating the waste water by filtering the liquid having the above composition though a filter having a retained particle diameter of at most 20 .mu.m.

Abstract: A cyanoacrylate monomer adhesive formulation which has improved thermal properties resulting from the inclusion in the formulation of an effective amount for enhancing the thermal resistance of the cured polymer of a naphthosultone compound having at least one strong electron withdrawing group thereon, suitably a nitro group.

Abstract: A method for illuminating explosive, flammable, and other hazardous environments. The method employs electroluminescent lights heaving controlled dielectric strength and capacitance, which when matched with the low current and voltage from an intrinsically safe power supply, and the controlled capacitance of each lighting circuit, produces an emergency lighting system which is both safe and effective.

Abstract: A matable connector assembly, suitable for use in fluid dispensing apparatus, comprising (1) a male connector comprising a housing defining an outer male coupling distal portion and having an axial bore containing therewithin an inner male coupling element which is axially bidirectionally slidable in the axial bore, the outer male coupling distal portion comprising transversely protruding tang element(s) thereon, and a manually securable locking member, and (2) a female connector comprising a housing defining a cavity therein, wherein the cavity contains an enclosing wall member defining a first cavity compartment therewithin, and a second cavity compartment exterior to the enclosing wall member within the cavity. The first cavity compartment is of a size and shape to couplingly receive the inner male coupling element therein.

Abstract: A process for sealing or adhering two surfaces having gaps of more than 100 micrometers between the surfaces which comprises:(A) applying to at least one of said surfaces an anaerobic composition comprising:(i) a room temperature polymerizable (meth)acrylic monomer,(ii) a peroxy free radical initiator, and(iii) an amount effective as an accelerator of a combination of saccharin and at least one onium salt (other than an iodide); and(B) placing said surfaces in an abutting relationship until the composition has cured through the gaps.Exemplified onium salts are phosphonium salts of the formula IV and quaternary ammonium salts of the formula II: ##STR1## wherein R.sup.1, R.sup.2, R.sup.3 and R.sup.4 which may be the same or different, are hydrocarbyl, hydrocarbylaryl, aryl or a substituted derivative thereof;X is Cl, Br or F, or a soft anion.

Abstract: Xanthate, dithiocarbamate and dithiophosphate salts of transition metals, together with a coinitiator selected from organic halogen and tertiary amine compounds provide light activated initiator systems for radically polymerizable ethylenically unsaturated compounds such as (meth)acrylate esters.

Abstract: A treatment method for polyene resins used in thiol-ene formulations, especially norbornene resins, significantly stabilizes thiol-ene compositions made from batches of polyene resin which otherwise give compositions with poor dark stability. The treatment comprises contacting the polyene with an amphoteric treating agent selected from the group consisting of silicated magnesium oxide, basic aluminum oxide, silica gel, magnesium oxide, magnesium hydroxide, calcium oxide, calcium hydroxide, barium oxide, and barium hydroxide, and then separating the resin from the treating agent prior to mixture with a polythiol to form a thiol-ene composition. The treatment method significantly reduces ionic content in polyene resins, particularly chloride ion but also sodium and potassium ions. Consequently, treatment is also beneficial with polyene resins which do not produce substantial dark stability problems.

Abstract: Anionically polymerizable di-.alpha.-cyanopentadienoate disiloxane compounds of the formula:[CH.sub.2 .dbd.CH--CH.dbd.C(CN)--C(.dbd.O)--O--CH.sub.2 --R--Si(R").sub.2 ].sub.2 --Owhere R is --CH.dbd.CH-- or --C(.dbd.CH.sub.2)-- and the R" groups are the same or different hydrocarbon or halo substituted hydrocarbon groups are prepared by hydrolysis of a cyanoacetoxypropenylsilane having a hydrolyzable group attached to the silicon atom and then condensing the resulting disiloxane compound with acrolein. The di-.alpha.-cyanopentadienoate disiloxane compounds are useful as instant adhesives and as co-monomers in cyanoacrylate or cyanopentadienoate instant adhesives, providing the adhesive polymers or copolymers with improved thermal resistance.

Abstract: A package, with a nozzle, a chamber, a cap which fits over the nozzle, and a pin attached to the interior of the cap which fits into the opening of the nozzle, for storing and dispensing a liquid, having an improved closure mechanism comprising at least one rectangular stopping member and at least one rectangular band in the interior of the cap and at least one guide flange on the nozzle. The package also has a plurality of guide ribs located around the nozzle to aid in the proper placement of the cap. The package is designed to be leak proof, nonclogging, able to dispense the liquid precisely, and can be easily opened even when the pin has bonded to the opening of the nozzle without breaking or shearing the pin.

Abstract: In a method for manufacturing ophthalmic, telescopic, microscopic, etc. lenses, the use of a radiation (e.g., UV or visible light) curable adhesive formulation containing a predominant amount of an acrylic capped organic prepolymer; a lesser amount of an ethylenically unsaturated diluent monomer; a minor amount of a non-reactive releasing agent and a suitable photoinitiator for blocking (bonding) and deblocking (debonding) a lens blank to a support member.

Abstract: An adhesive composition capable of post-cure expansion comprising a multifunctional (meth)acrylate and a maleimide capable of effectuating expansion upon post-cure. A homogeneous mixture of a monomer and maleimide are subjected to a first cure heat stage wherein a rigid partially-cured plastic is formed and a post-cure heart stage to effectuate permanent expansion of the cured adhesive composition.

Abstract: (Meth)acrylic ester formulations employing peroxy initiators have accelerated cure rates when the substrates to which they are applied, or the compositions themselves, include nitrite, borate, silicate or carbonate salts. The compositions should be free of acids having a PKa of 6 or less unless the composition also includes a transition metal compound.