Abstract: The object of the present invention is to provide a method of producing low oxygen-containing potassium fluorotantalate crystals or low oxygen-containing potassium fluoroniobate crystals, the crystals obtained by the production method, and a method of analyzing oxygen contained in these crystals. The method of producing low oxygen-containing potassium fluorotantalate crystals comprises generating recrystallized potassium fluorotantalate crystals by controlled cooling of a saturated solution of potassium fluorotantalate containing hydrofluoric acid as an essential component, collecting the generated recrystallized crystals through filtration, and drying the collected recrystallized crystals in a drying apparatus so as to obtain the crystals, and the production method is characterized in that the saturated solution of potassium fluorotantalate containing hydrofluoric acid as an essential component contains hydrofluoric acid in a concentration of 0.5 mol/l to 10 mol/l.

Abstract: A polyurethane resin having a total concentration of the urethane group and the urea group of not less than 15% by weight is prepared by reacting a diisocyanate component (e.g., an aromatic diisocyanate) with a diol component (e.g., a C2–8alkylene glycol). The repeating unit of the polyurethane resin may contain a constitutive unit of an aromatic or alicyclic compound. The polyurethane resin may be shaped into a film for use as a gas barrier film. The film may be a gas barrier composite film composed of a base film layer and a resin layer at least comprising the polyurethane resin. The present invention provides a polyurethane resin excellent in gas barrier properties against water vapor, oxygen, aromatics, and others, and a film containing the same.

Abstract: The present invention herein provides a gel for electrophoresis which comprises a gel prepared from single-stranded glucan which has ?-1,3-glucoside bonds as a main chain and ?-1,6-glucoside bonds on side chains, or a mixture of the glucan with a second polysaccharide, or acrylamide and/or derivative thereof; and a method for the preparation of a gel for electrophoresis comprising the steps of dissolving a glucan, which has ?-1,3-glucoside bonds as a main chain and ?-1,6-glucoside bonds on side chains, in a first solvent which can dissociate the helical structure of the glucan to thus form single-stranded glucan; removing the first solvent; dissolving the single-stranded glucan in a second solvent capable of dissolving the same; and then heat-treating the resulting solution.

Abstract: The present invention relates to a process for producing optically active ?-nitroalcohols wherein nitroaldol reactions of aldehydes and nitroalkanes are carried out in the presence of a base and an optically active metal complex catalyst represented by the following formula (c): (where R4, R5, and R6 represent a hydrogen atom, an alkyl group, an alkenyl group, an aryl group, an acyl group, an alkoxycarbonyl group, or an aryloxycarbonyl group, and R5 and R6 may be linked together to form a ring; X* represents a hydrocarbon group having an asymmetric carbon atom or axial asymmetry; M represents a cobalt ion or a chromium ion; and Y represents an anion capable of forming a salt when the valence of M is larger than that of a ligand).

Abstract: Measurements are obtained by a computing unit based on an output Vh from an indirectly-heated constant-temperature controlling flow rate measuring section (16) and an output Vout from a two-constant-point temperature difference detecting flow rate measuring sections (18a, 18b). In the flow rate measuring section (16), a heating element (163) is feedback-controlled based on a detected temperature by a heat sensing element (162) to obtain an output Vh based on the feedback-controlled condition. An output Vout is obtained from flow rate measuring sections (18a, 18b) based on the detected temperature difference between a heat sensing element (182) disposed on the liquid-flow-direction upstream side of the flow rate measuring section (16) and a temperature sensing element disposed on the downstream side.

Abstract: The present invention relates to a novel production method of 4,6-diaminoresorcin, and to 2-sulfonic acid-4,6-dinitroresorcin as its intermediate and salts thereof.

Abstract: A glycoside in which at least two phenolic hydroxyl groups of a compound having at least two phenolic hydroxyl groups in its molecule are glycosidically linked to anomeric carbon atoms of at least two sugar molecules can be prepared with high yield by a method including the step of allowing phenolic hydroxyl groups of a compound having at least two phenolic hydroxyl groups in its molecule to react with sugar molecules each having an acetylated hydroxyl group attached to an anomeric carbon atom in the presence of an organic solvent and an acid catalyst while removing acetic acid formed during the reaction from the reaction system.

Abstract: A polyimide metal laminate comprising a stainless steel layer/a resin layer/a thermoplastic polyimide resin layer/a metal thin film layer, wherein a thickness of the metal layer is in the range of 0.001 to 1.0 ?m, a method for producing the same and a hard disk suspension comprising these polyimide metal laminate are provided. The hard disk suspension can be capable of fine pitch processing such that wiring pitch is not more than 50 ?m.

Abstract: A copper foil which is substantially free of generation of voids even if fusing treatment is conducted on a tin-plated layer and which is excellent in etching properties is provided. To achieve this object, a pure copper-coated copper foil in which a pure-copper plated layer is formed at least on a gloss surface of a base copper foil is employed. The pure copper-plated layer preferably has a thickness of not less than 0.3 ?m. A method of producing a pure copper-coated copper foil, in which electrolysis is conducted using, as an electrolyte, an aqueous sulfuric acid-copper sulfate solution having a Cl? ion concentration of not more than 0.5 mg/l with a base copper foil serving as a cathode, thereby forming a pure copper-plated layer at least on a gloss surface of the base copper foil. The aqueous sulfuric acid-copper sulfate solution preferably has a Cu2+ ion concentration of 40 g/l to 120 g/l and a free SO42? ion concentration of 100 g/l to 200 g/l.

Abstract: Adhesive composition and a flexible packaging composite film that can produce a reduced amount of low-molecular-weight compounds eluted into contents of a composite film to prevent spoilage of inherent properties or performances of the contents, can produce improved oil resistance to prevent significant reduction in strength even when used for oily contents, and can develop favorable flexibility of the composite film to prevent reduction in peel strength. Polyester polyamide polyol and/or polyurethane polyester polyamide polyol including an amide bond produced by reaction between a dimer acid and polyamine is prepared as a polyol component and also concentration of a cyclic compound formed by the amide bond and/or an ester bond in extracted water which is extracted from a composite film adhesively bonded by the adhesive composition by water of 0.5 mL/cm2 per unit area of the composite film is set to be 0.

Abstract: An optical recording medium having a recording layer which contains at least one compound selected from the group consisting of mono-, di-, and triazaporphyrin compounds optionally in the form of a metal complex; or an optical recording medium comprising a substrate and formed thereon at least a recording layer containing an organic dye as a main component, characterized in that the organic dye has a first maximum value of absorption at a wavelength ?1 of 400 nm or less in the absorption spectrum and has a second maximum value of absorption at a longer-wavelength side than the ?1, and a wavelength band wherein the refractive index (n) and the absorption coefficient (k) of the above organic dye satisfy n?1.90 and 0.03?k?0.30.

Abstract: The invention provides a surface-treated copper foil which can sufficiently ensure adhesive strength with a low-dielectric substrate used in forming a printed wiring board for high-frequency applications and can minimize transmission losses. There is provided a surface-treated copper foil for a low-dielectric substrate which is used in bonded relationship to a low-dielectric substrate, which is characterized in that a nodular-treated layer constituted by bump-like copper particles is formed on a surface of the copper foil and that ultrafine copper particles are caused to precipitate on the whole surface of the nodular-treated layer and adhere thereto and the roughness value Rz of the surface is 1.0 to 6.5 ?m. The surface color of the surface-treated copper foil has L* of not more than 50, a* of not more than 20 and b* of not more than 15.

Abstract: By providing a composition in which refractive index can be controlled, and scratch resistivity and adhesion (especially adhesion to a resin having a thiourethane bond or epithiosulfide bond) are excellent when the composition is coated on a base material such as a resin and then cured, the composition comprises (a) a thio(meth)acrylate compound represented by the general formula (1) and (b) ultrafine inorganic particles: wherein a linking(or connecting) group R represents an aliphatic residue, an aromatic residue, an alicyclic residue or a heterocyclic residue or an aliphatic residue having an oxygen atom, a sulfur atom, an aromatic ring, an aliphatic ring, or a heterocycle in the chain; Rm represents each independently a hydrogen atom or a methyl group; and n is an integer of 1 to 4.

Abstract: A jig for calcining an electronic component including a substrate and a zirconia surface layer formed on the substrate, wherein one of the skewness, the kurtosis, the central surface average roughness the wear resistance and the thermal shock resistance of the zirconia surface layer is specified to a certain range. Consequently, the jig for calcining the electronic component can efficiently conduct the calcination without deteriorating the properties of the electronic component to be calcined.

Abstract: A clutch mechanism of the power device includes a movable gear member which is rotated integrally with a wheel and engaged with a stationary gear member when moved in a first direction and disengaged from the stationary gear member when moved in a second direction opposite to the first direction, an armature for pushing out the movable gear member in the first direction when rotated relatively to the movable gear member, and an electromagnetic coil for applying brake resistance to the armature by attracting the armature by the magnetic force to restrict a co-rotating state of the armature and the movable gear member. The armature has a clutch holding surface for maintaining a clutch-engaged state where the movable gear member and the stationary gear member is engaged with other even when the electromagnetic coil is turned off in the clutch-engaged state.

Abstract: The display filter is constituted by laminating a transparent adhesive layer (C) 31 containing dye, a polymer film (B) 20, a transparent electrically conductive layer (D) 10, a transparent adhesive layer (E) 40, and a functional transparent layer (A) 60 having an anti-reflection property, a hard coat property, a gas barrier property, an antistatic property and an anti-fouling property sequentially in this order, adhered on a display area 00; on this occasion, the transparent electrically conductive layer (D) 10 is grounded to a ground terminal of the display via an electrode 50 and an electrically conductive copper foil adhesive tape 80.

Abstract: A two-component sealant composition for a plastic liquid crystal display cell of the invention contains the following components (1) to (6): (1) a liquid epoxy resin having from 1.7 to 6 in weight average of epoxy groups in one molecule and an ionic conductivity of an aqueous solution obtained by extraction separation by contact mixing with 10 times by weight of pure water at from 40 to 80° C. of 2 mS/m or less, (2) a curing agent containing one or a mixture of two or more selected from a tetrafunctional mercapto compound, a modified polymercapto derivative, a micro-encapsulated imidazole compound, or a methyl methacrylate adduct of an alicyclic diamine, having an ionic conductivity of an aqueous solution obtained by extraction separation by contact mixing with 10 times by weight of pure water at from 40 to 80° C. of 0.6 mS/m or less, (3) a curing accelerator,(4) an inorganic filler,(5) a silane coupling agent, and (6) rubbery polymer fine particles having a softening temperature of 0° C.

Abstract: An olefin polymerization catalyst having a high polymerization activity at high temperatures and a process for olefin polymerization using the catalyst are disclosed. The olefin polymerization catalyst comprises a transition metal compound which is represented by the following formula (I) and in which the net charge parameter of the central metal is not more than 2.00: wherein M is a transition metal atom of Group 4 to Group 5 of the periodic table, m is an integer of 1 to 5, Q is —N? or —C(R2)?, A is —O—, —S—, —Se— or —N(R5)—, R1 is an aliphatic hydrocarbon group or an alicyclic hydrocarbon group, R2 to R5 are each a hydrogen atom, a hydrocarbon group, an oxygen-containing group or the like, n is a number satisfying a valence of M, and X is a hydrogen atom, a halogen atom, a hydrocarbon group or the like.

Abstract: A hoisting device can be small-sized and energy can be saved. A hoisting device 10 according to the present invention has a hoist 30 and a control unit 32. The hoist 30 rotates a drum 12 having a wire 14 wound thereon by an oil pressure motor 42 rotatable in normal and reverse directions. To the oil pressure motor 42, operating oil is supplied from an oil pressure pump 44. The oil pressure pump 44 is a two-way discharge fixed capacity type, and rotated by a servomotor 46. An acceleration/displacement transducer 34 in the control unit 32 finds a moving direction and a moving speed of a wire hanging point in the vertical direction from an output signal of an acceleration sensor 24.

Abstract: The present invention is to provide a surface protecting film for a semiconductor wafer which can prevent breakage of the semiconductor wafer even when the semiconductor wafer is thinned to not more than 200 ?m, and a method of protecting the semiconductor wafer using the protecting film. The present invention relates to a surface protecting adhesive film for a semiconductor wafer comprising a base film having an adhesive layer formed on one surface thereof, wherein the base film comprises a layer (A) having a storage elastic modulus of from 1×107 Pa to 1×109 Pa at a temperature range of from 20° C. to 180° C.