Patents Assigned to Sandia
  • Patent number: 6290868
    Abstract: The present application is directed to a new class of composite materials, called field-structured composite (FSC) materials, which comprise a oriented aggregate structure made of magnetic particles suspended in a nonmagnetic medium, and to a new class of processes for their manufacture. FSC materials have much potential for application, including use in chemical, optical, environmental, and mechanical sensors.
    Type: Grant
    Filed: May 27, 1999
    Date of Patent: September 18, 2001
    Assignee: Sandia Corporation
    Inventors: James E. Martin, Robert C. Hughes, Robert A. Anderson
  • Patent number: 6290859
    Abstract: A process is disclosed whereby a 5-50-nanometer-thick conformal tungsten coating can be formed over exposed semiconductor surfaces (e.g. silicon, germanium or silicon carbide) within a microelectromechanical (MEM) device for improved wear resistance and reliability. The tungsten coating is formed after cleaning the semiconductor surfaces to remove any organic material and oxide film from the surface. A final in situ cleaning step is performed by heating a substrate containing the MEM device to a temperature in the range of 200-600 ° C. in the presence of gaseous nitrogen trifluoride (NF3). The tungsten coating can then be formed by a chemical reaction between the semiconductor surfaces and tungsten hexafluoride (WF6) at an elevated temperature, preferably about 450° C. The tungsten deposition process is self-limiting and covers all exposed semiconductor surfaces including surfaces in close contact.
    Type: Grant
    Filed: November 12, 1999
    Date of Patent: September 18, 2001
    Assignee: Sandia Corporation
    Inventors: James G. Fleming, Seethambal S. Mani, Jeffry J. Sniegowski, Robert S. Blewer
  • Patent number: 6290909
    Abstract: Apparatus and method for driving a sample, having a well-defined volume, under pressure into a chromatography column. A conventional high pressure sampling valve is replaced by a sample injector composed of a pair of injector components connected in series to a common junction. The injector components are containers of porous dielectric material constructed so as to provide for electroosmotic flow of a sample into the junction. At an appropriate time, a pressure pulse from a high pressure source, that can be an electrokinetic pump, connected to the common junction, drives a portion of the sample, whose size is determined by the dead volume of the common junction, into the chromatographic column for subsequent separation and analysis. The apparatus can be fabricated on a substrate for microanalytical applications.
    Type: Grant
    Filed: April 13, 2000
    Date of Patent: September 18, 2001
    Assignee: Sandia Corporation
    Inventors: Phillip H. Paul, Don W. Arnold, David W. Neyer
  • Patent number: 6288473
    Abstract: A piezoelectric motor has peak performance at a specific frequency f1 that may vary over a range of frequencies. A drive system is disclosed for operating such a motor at peak performance without feedback. The drive system consists of the motor and an ac source connected to power the motor, the ac source repeatedly generating a frequency over a range from f1−&Dgr;x to f1+&Dgr;y.
    Type: Grant
    Filed: March 31, 2000
    Date of Patent: September 11, 2001
    Assignee: Sandia Corporation
    Inventor: Anthony Mittas
  • Patent number: 6287440
    Abstract: A method for eliminating gas bubble blockage of current flow during operation of an electrokinetic pump. By making use of the ability to modify the surface charge on the porous dielectric medium used in electrokinetic pumps, it becomes possible to place electrodes away from the pressurized region of the electrokinetic pump. While gas is still generated at the electrodes they are situated such that the generated gas can escape into a larger buffer reservoir and not into the high pressure region of the pump where the gas bubbles can interrupt current flow. Various combinations of porous dielectric materials and ionic conductors can be used to create pumps that have desirable electrical, material handling, and flow attributes.
    Type: Grant
    Filed: June 18, 1999
    Date of Patent: September 11, 2001
    Assignee: Sandia Corporation
    Inventors: Don W. Arnold, Phillip H. Paul, Joseph S. Schoeniger
  • Patent number: 6286386
    Abstract: An apparatus that can return a payload to a known orientation after unknown motion, without requiring external power or complex mechanical systems. The apparatus comprises a faceted cage that causes the system to rest in a stable position and orientation after arbitrary motion. A gimbal is mounted with the faceted cage and holds the payload, allowing the payload to move relative to the stable faceted cage. The payload is thereby placed in a known orientation by the interaction of gravity with the geometry of the faceted cage, the mass of the system, and the motion of the payload and gimbal. No additional energy, control, or mechanical actuation is required. The apparatus is suitable for use in applications requiring positioning of a payload to a known orientation after arbitrary or uncontrolled motion, including remote sensing and mobile robot applications.
    Type: Grant
    Filed: May 6, 1999
    Date of Patent: September 11, 2001
    Assignee: Sandia Corporation
    Inventors: Barry L. Spletzer, Gary J. Fischer, Michael A. Martinez
  • Patent number: 6283499
    Abstract: The present invention relates to an inflatable occupant restraint device having an inflator, an outer bag disposed around the inflator to allow the outer bag to be filled with gas produced by the inflator, an inner bag, disposed in between the outer bag and the inflator, wherein the inner bag is made of a flexible material having at least one flow outlet in the flexible material altering the flow of gas produced by the inflator. The inner bag protects the outer bag from hot gases and particles emanating from the inflator. The inner bag may also have a pattern of stitched seams forming gas flow outlets to impart a desired flow pattern to the inflating gases.
    Type: Grant
    Filed: February 18, 1998
    Date of Patent: September 4, 2001
    Assignee: Sandia Corporation
    Inventors: James M. Nelsen, Kenneth W. Gwinn
  • Patent number: 6284908
    Abstract: A method for disproportionation of an oligohydridosiloxane to produce a polysilsesquioxane compound and an organohydridosilane compound when contacted with a basic catalyst. The basic catalyst can be a tetraalkylammonium hydroxide, an alkali metal hydroxide, and an alkali earth hydroxide. These basic catalysts are generally dissolved in an organic solvent for delivery. The hydroxide catalysts are attractive because many readily decompose by heating above 150° C., thus being easily removed from the final materials. The oligohydridosiloxane is contacted with the basic catalyst under conditions effective to catalytically convert the oligohydridosiloxane into a polysilsesquioxane compound and an organohydridosilane compound. The reaction can occur in either an inert or oxidative atmosphere and can occur without heating, at room temperature. Both polysilsesquioxane foams and gels of the formula (RSiO1.5)n can be produced.
    Type: Grant
    Filed: September 25, 2000
    Date of Patent: September 4, 2001
    Assignee: Sandia Corporation
    Inventors: Douglas A. Loy, Kamyar Rahimian
  • Patent number: 6285904
    Abstract: A method and apparatus for determining characteristics of tissue is disclosed. The method comprises supplying optical energy to a tissue and detecting at a plurality of locations consequent energy scattered by the tissue. Analysis of the scattered energy as taught herein provides information concerning the properties of the tissue, specifically information related to the fat and lean content and thickness of the tissue. The apparatus comprises a light source adapted to deliver optical energy to a tissue. A plurality of detectors can be mounted at different positions relative to the source to detect energy scattered by the tissue. A signal processor as taught herein can determine characteristics of the tissue from the signals from the detectors and locations of the detectors, specifically information related to the fat and lean content and thickness of the tissue.
    Type: Grant
    Filed: March 27, 2000
    Date of Patent: September 4, 2001
    Assignee: Sandia Corporation
    Inventors: Thomas M. Weber, Barry L. Spletzer, Jon R. Bryan, Fred M. Dickey, Richard N. Shagam, Luc Gooris
  • Patent number: 6281488
    Abstract: A displacement sensor includes a first optical fiber for radiating light to a target, and a second optical fiber for receiving light from the target. The end of the first fiber is adjacent and not axially aligned with the second fiber end. A lens focuses light from the first fiber onto the target and light from the target onto the second fiber.
    Type: Grant
    Filed: December 9, 1998
    Date of Patent: August 28, 2001
    Assignee: Sandia Corporation
    Inventor: Kevin J. Fleming
  • Patent number: 6277257
    Abstract: An electrokinetic high pressure hydraulic pump for manipulating fluids in capillary-based systems. The pump uses electro-osmotic flow to provide a high pressure hydraulic system, having no moving mechanical parts, for pumping and/or compressing fluids, for providing valve means and means for opening and closing valves, for controlling fluid flow rate, and manipulating fluid flow generally and in capillary-based systems (Microsystems), in particular. The compact nature of the inventive high pressure hydraulic pump provides the ability to construct a micro-scale or capillary-based HPLC system that fulfills the desire for small sample quantity, low solvent consumption, improved efficiency, the ability to run samples in parallel, and field portability. Control of pressure and solvent flow rate is achieved by controlling the voltage applied to an electrokinetic pump.
    Type: Grant
    Filed: March 18, 1999
    Date of Patent: August 21, 2001
    Assignee: Sandia Corporation
    Inventors: Phillip H. Paul, David J. Rakestraw, Don W. Arnold, Kenneth R. Hencken, Joseph S. Schoeniger, David W. Neyer
  • Patent number: 6275740
    Abstract: The invention generally relates to various aspects of a plasma process, and more specifically the monitoring of such plasma processes. One aspect relates in at least some manner to calibrating or initializing a plasma monitoring assembly. This type of calibration may be used to address wavelength shifts, intensity shifts, or both associated with optical emissions data obtained on a plasma process. A calibration light may be directed at a window through which optical emissions data is being obtained to determine the effect, if any, that the inner surface of the window is having on the optical emissions data being obtained therethrough, the operation of the optical emissions data gathering device, or both. Another aspect relates in at least some manner to various types of evaluations which may be undertaken of a plasma process which was run, and more typically one which is currently being run, within the processing chamber.
    Type: Grant
    Filed: April 23, 1998
    Date of Patent: August 14, 2001
    Assignee: Sandia Corporation
    Inventors: Michael Lane Smith, Jr., Joel O'Don Stevenson, Pamela Peardon Denise Ward
  • Patent number: 6270641
    Abstract: The performance of microchannel devices is improved by providing turns, wyes, tees, and other junctions that produce little dispersions of a sample as it traverses the turn or junction. The reduced dispersion results from contraction and expansion regions that reduce the cross-sectional area over some portion of the turn or junction. By carefully designing the geometries of these regions, sample dispersion in turns and junctions is reduced to levels comparable to the effects of ordinary diffusion. A numerical algorithm was employed to evolve low-dispersion geometries by computing the electric or pressure field within candidate configurations, sample transport through the turn or junction, and the overall effective dispersion. These devices should greatly increase flexibility in the design of microchannel devices by permitting the use of turns and junctions that do not induce large sample dispersion.
    Type: Grant
    Filed: April 26, 1999
    Date of Patent: August 7, 2001
    Assignee: Sandia Corporation
    Inventors: Stewart K. Griffiths, Robert H. Nilson
  • Patent number: 6271335
    Abstract: A method of making a thermally-removable encapsulant by heating a mixture of at least one bis(maleimide) compound and at least one monomeric tris(furan) or tetrakis(furan) compound at temperatures from above room temperature to less than approximately 90° C. to form a gel and cooling the gel to form the thermally-removable encapsulant. The encapsulant can be easily removed within approximately an hour by heating to temperatures greater than approximately 90° C., preferably in a polar solvent. The encapsulant can be used in protecting electronic components that may require subsequent removal of the encapsulant for component repair, modification or quality control.
    Type: Grant
    Filed: January 18, 2000
    Date of Patent: August 7, 2001
    Assignee: Sandia Corporation
    Inventors: James H. Small, Douglas A. Loy, David R. Wheeler, James R. McElhanon, Randall S. Saunders
  • Patent number: 6270846
    Abstract: An evaporation-induced self-assembly method to prepare a surfactant-templated thin film by mixing a silica sol, a surfactant, and a hydrophobic polymer and then evaporating a portion of the solvent during coating onto a substrate and then heating to form a liquid-phase, thin film material with a porosity greater than approximately 50 percent. The high porosity thin films can have dielectric constants less than 2 to be suitable for applications requiring low-dielectric constants. An interstitial compound can be added to the mixture, with the interstitial compound either covalently bonded to the pores or physically entrapped within the porous structure. The selection of the interstitial compound provides a means for developing thin films for applications including membranes, sensors, low dielectric constant films, photonic materials and optical hosts.
    Type: Grant
    Filed: March 2, 2000
    Date of Patent: August 7, 2001
    Assignee: Sandia Corporation
    Inventors: C. Jeffrey Brinker, Yunfeng Lu, Hongyou Fan
  • Patent number: 6271670
    Abstract: A method and tool using a continuous electromagnetic wave from a transverse magnetic-dipole source with a coaxial electric-dipole receiver is described for the detection of external sidewall cracks and other anomalies in boiler tubes and other enclosures. The invention utilizes the concept of radar backscatter rather than eddy-currents or ultrasound, which are sometimes used in prior art crack-detection methods. A numerical study of the distribution of the fields shows that the direct transmission from the source to the receiver is reduced from that in free space. Further, if the diameter of the receiver dipole is made sufficiently small, it should be possible to detect cracks with a scattering loss of up to −40 dB in thin-walled boiler tubes.
    Type: Grant
    Filed: February 8, 1999
    Date of Patent: August 7, 2001
    Assignee: Sandia Corporation
    Inventor: Thurlow W. H. Caffey
  • Patent number: 6269725
    Abstract: An apparatus and method for disarming improvised bombs are disclosed. The apparatus comprises a fluid-filled bottle or container made of plastic or another soft material which contains a fixed or adjustable, preferably sheet explosive. The charge is fired centrally at its apex and can be adjusted to propel a fluid projectile that is broad or narrow, depending upon how it is set up. In one embodiment, the sheet explosive is adjustable so as to correlate the performance of the fluid projectile to the disarming needs for the improvised explosive device (IED). Common materials such as plastic water bottles or larger containers can be used, with the sheet explosive or other explosive material configured in a general chevron-shape to target the projectile toward the target. In another embodiment, a thin disk of metal is conformably mounted with the exterior of the container and radially aligned with the direction of fire of the fluid projectile.
    Type: Grant
    Filed: August 2, 1999
    Date of Patent: August 7, 2001
    Assignee: Sandia Corporation
    Inventor: Christopher R. Cherry
  • Patent number: 6268630
    Abstract: A silicon-on-insulator (SOI) field-effect transistor (FET) and a method for making the same are disclosed. The SOI FET is characterized by a source which extends only partially (e.g. about half-way) through the active layer wherein the transistor is formed. Additionally, a minimal-area body tie contact is provided with a short-circuit electrical connection to the source for reducing floating body effects. The body tie contact improves the electrical characteristics of the transistor and also provides an improved single-event-upset (SEU) radiation hardness of the device for terrestrial and space applications. The SOI FET also provides an improvement in total-dose radiation hardness as compared to conventional SOI transistors fabricated without a specially prepared hardened buried oxide layer. Complementary n-channel and p-channel SOI FETs can be fabricated according to the present invention to form integrated circuits (ICs) for commercial and military applications.
    Type: Grant
    Filed: March 16, 1999
    Date of Patent: July 31, 2001
    Assignee: Sandia Corporation
    Inventors: James R. Schwank, Marty R. Shaneyfelt, Bruce L. Draper, Paul E. Dodd
  • Patent number: 6269278
    Abstract: The invention generally relates to various aspects of a plasma process, and more specifically the monitoring of such plasma processes. One aspect relates in at least some manner to calibrating or initializing a plasma monitoring assembly. This type of calibration may be used to address wavelength shifts, intensity shifts, or both associated with optical emissions data obtained on a plasma process. A calibration light may be directed at a window through which optical emissions data is being obtained to determine the effect, if any, that the inner surface of the window is having on the optical emissions data being obtained therethrough, the operation of the optical emissions data gathering device, or both. Another aspect relates in at least some manner to various types of evaluations which may be undertaken of a plasma process which was run, and more typically one which is currently being run, within the processing chamber.
    Type: Grant
    Filed: April 23, 1998
    Date of Patent: July 31, 2001
    Assignee: Sandia Corporation
    Inventors: Michael Lane Smith, Jr., Joel O'Don Stevenson, Pamela Peardon Denise Ward
  • Patent number: 6266437
    Abstract: A system for detecting defects on a moving web having a sequential series of identical frames uses an imaging device to form a real-time camera image of a frame and a comparitor to comparing elements of the camera image with corresponding elements of an image of an exemplar frame. The comparitor provides an acceptable indication if the pair of elements are determined to be statistically identical; and a defective indication if the pair of elements are determined to be statistically not identical. If the pair of elements is neither acceptable nor defective, the comparitor recursively compares the element of said exemplar frame with corresponding elements of other frames on said web until one of the acceptable or defective indications occur.
    Type: Grant
    Filed: September 4, 1998
    Date of Patent: July 24, 2001
    Assignee: Sandia Corporation
    Inventors: Paul H. Eichel, Gerard E. Sleefe, K. Terry Stalker, Amy A. Yee