Patents Assigned to UT-Battelle, LLC
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Patent number: 11984243Abstract: Permanent magnet materials are provided. The permanent magnet materials are cerium based materials including zirconium and iron in combination with cobalt. The permanent magnet materials may have the formula Ce2ZrFe15?xCox wherein 6?x?15. In some embodiments, the permanent magnet materials have the formula Ce2+yZr1?yFe(15?x)(2?z)/2)CoxCu((15?x)z/2) wherein 6?x?15, 0?y?0.4, and z=0 or 1. In other embodiments, the permanent magnet materials have the formula Ce2Zrx(Fe1?yCoy)17?2x, where 0<x?1 and 0.4?y?1. Permanent magnets including the permanent magnet materials are also provided.Type: GrantFiled: March 3, 2022Date of Patent: May 14, 2024Assignees: UT-BATTELLE, LLC, Iowa State University Research Foundation, Inc.Inventors: David S. Parker, Tribhuwan Pandey, Cajetan Ikenna Nlebedim, Xubo Liu
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Patent number: 11980939Abstract: An electromagnet alignment system for in-situ alignment of a magnetic particulate material is provided. The magnetic particulate material is dispensed through an orifice of a dispensing nozzle used for 3D printing. The system has an electromagnet assembly having a coil. The coil is configured to generate a pulsed magnetic field having a target magnetic flux intensity upon energization of the coil when the magnetic particulate material is being heated and moved through the dispensing nozzle. As a result, the magnetic particulate material is at least partially aligned with respect to a direction by the pulsed magnetic field. The system further includes a power source for implementing the energization of the coil.Type: GrantFiled: April 15, 2021Date of Patent: May 14, 2024Assignee: UT-BATTELLE, LLCInventors: Mariappan Parans Paranthaman, Brian K. Post, Brian C. Sales
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Patent number: 11982684Abstract: Systems, methods and programs are provided for automated science experiments which use a model with learnt model parameters to define points for physical-characteristic measurements once the model is trained. The systems, methods and programs use active learning which enables describing a relationship between local features of sample-surface structure shown in image patches and determined representations of physical-characteristic measurements.Type: GrantFiled: May 26, 2023Date of Patent: May 14, 2024Assignee: UT-Battelle, LLCInventors: Maxim A. Ziatdinov, Kevin Roccapriore, Yongtao Liu, Kyle P. Kelley, Rama K. Vasudevan, Jacob D. Hinkle, Sergei V. Kalinin
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Method of solvent-free manufacturing of composite electrodes incorporating radiation curable binders
Patent number: 11984577Abstract: A method of making an electrode includes the step of mixing active material particles, radiation curable resin precursors, and electrically conductive particles to create an electrode precursor mixture. The electrode precursor mixture is electrostatically sprayed onto a current collector to provide an electrode preform. The electrode preform is heated and calendered to melt the resin precursor such that the resin precursor surrounds the active particles and electrically conductive particles. Radiation is applied to the electrode preform sufficient to cure the radiation curable resin precursors into resin.Type: GrantFiled: March 29, 2022Date of Patent: May 14, 2024Assignee: UT-BATTELLE, LLCInventors: Zhijia Du, Christopher James Janke, Jianlin Li, David L. Wood, III, Claus Daniel -
Patent number: 11975491Abstract: A system for predicting one or more analytes based on outputs from thin film gas sensors is provided. The system may comprise an electronic nose (e-nose). The e-nose may comprise the gas sensors and a first processor. The system may further comprise a second processor. The second processor may be configured to receive the output from each of the gas sensors, evaluate a prediction accuracy using an evaluation parameter of each of a plurality of models which are trained and tested and select a model from among the plurality of models to deploy based on a comparison of the evaluation parameter for each of the plurality of models and use the same. The second processor may also receive, an output of each of the gas sensors caused by unknown one or more analytes; and predict, using the deployed model, the one or more analytes that causes the output.Type: GrantFiled: September 23, 2021Date of Patent: May 7, 2024Assignee: UT-BATTELLE, LLCInventors: Ilia N. Ivanov, Eric S. Muckley, Nicholas West
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Patent number: 11979036Abstract: A system and method for sensorless coil detection that exploits a dead-time effect in a WPT inverter as an indicator of presence of a receiver. In one embodiment, a system described herein may be configured to detect arrival of a moving receiver prior to alignment of the moving receiver with the transmitter for power transmission.Type: GrantFiled: December 28, 2021Date of Patent: May 7, 2024Assignee: UT-Battelle, LLCInventors: Utkarsh D. Kavimandan, Veda P. Galigekere, Burak Ozpineci
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Patent number: 11970764Abstract: A method for producing a structure containing an array of MWCNTs on a metal substrate, comprising: (i) subjecting a metal substrate to a surface oxidation process at a first elevated temperature in an oxygen-containing atmosphere and under a first reduced pressure; (ii) subjecting the metal substrate to a surface reduction process at a second elevated temperature in a reducing atmosphere and under a second reduced pressure of at least 0.01 atm and less than 1 atm to result in reduction of the surface of said metal substrate, wherein the reducing atmosphere contains hydrogen gas; (iii) subjecting the metal substrate to a third reduced pressure of no more than 0.1 atm; and (iv) contacting the metal substrate, while at the third reduced pressure and under an inert or reducing atmosphere, with an organic substance at a third elevated temperature for suitable time to produce the MWCNTs on the metal substrate.Type: GrantFiled: November 5, 2020Date of Patent: April 30, 2024Assignee: UT-Battelle, LLCInventors: Chanaka Kapila Kumara Ihala Gamaralalage, Jun Qu, Paul A. Menchhofer
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Patent number: 11964918Abstract: An improved method for embedding one or more sensors in SiC is provided. The method includes depositing a binder onto successive layers of a SiC powder feedstock to produce a dimensionally stable green body have a true-sized cavity. A sensor component is then press-fit into the true-sized cavity. Alternatively, the green body is printed around the sensor component. The assembly (the green body and the sensor component) is heated within a chemical vapor infiltration (CVI) chamber for debinding, and a precursor gas is introduced for densifying the SiC matrix material. During infiltration, the sensor component becomes bonded to the densified SiC matrix, the sensor component being selected to be thermodynamically compatible with CVI byproducts at elevated temperatures, including temperatures in excess of 1000° C.Type: GrantFiled: January 6, 2021Date of Patent: April 23, 2024Assignee: UT-BATTELLE, LLCInventors: Christian M. Petrie, Brian C. Jolly, Kurt A. Terrani, Michael P. Trammell
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Patent number: 11958251Abstract: An additive manufacturing system comprising at least one electronic nose (e-nose) is provided. The e-nose may comprise a housing and gas sensors. The housing may have an air channel. The active sensor portion of the sensors are positioned in the air channel. The housing may be mounted to an extruder head of an additive manufacturing device. The system may also comprise a processor. The processor may determine whether there is an abnormality in an additive manufacturing process based on one or more combinations of outputs from the gas sensors received during the additive manufacturing process input into a deployed machine learning model; and generate a report for the additive manufacturing process containing the determination.Type: GrantFiled: September 23, 2021Date of Patent: April 16, 2024Assignees: UT-BATTELLE, LLC, UNIVERSITY OF TENNESSEE RESEARCH FOUNDATIONInventors: Ilia N. Ivanov, Eric S. Muckley
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Patent number: 11953432Abstract: A system comprising a nonlinear medium (NLM), an optical transduction module, a dual homodyne detector and a processor is provided. The NLM receives at least a pump beam and issues the pump, probe and conjugate beams, where the beams are linearly polarized. Optics route the probe, the conjugate or both beams to the sample. The sample imparts polarization rotation to light that interacts therewith. The optical transduction module imparts to the interacted light an optical phase shift that is a 1:1 transduction of the polarization rotation, where at least one of the probe light or the conjugate light carries the imparted optical phase shift. The processor obtains the optical-phase shift based on respective detection signals from the dual homodyne detector and determines, based on the obtained optical-phase shift, at least one of a Faraday polarization rotation, a Kerr polarization rotation or a spin noise spectrum.Type: GrantFiled: July 29, 2022Date of Patent: April 9, 2024Assignee: UT-BATTELLE, LLCInventors: Benjamin J. Lawrie, Yun-Yi Pai, Chengyun Hua, Raphael C. Pooser, Claire E. Marvinney
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Patent number: 11945947Abstract: A crosslinked polymeric composition comprising A, B, C, D, and E units having the following structures, respectively: and wherein dashed bonds represent optional bonds; the asterisks (*) in C units represent covalent bond connection points with asterisks in A units and E units; the asterisks (*) in D units represent covalent bond connection points with asterisks in B units and E units; wherein a portion of E units are bound to C units, a portion of E units are bound to D units, and a portion of E units are bound to both C and D units; and the composition contains a multiplicity of A, B, C, D, and E units. Also described is a method for producing the crosslinked polymeric composition by reacting epoxy-containing molecules (A molecules), isocyanate-containing molecules (B molecules), and disulfide-containing molecules (C molecules).Type: GrantFiled: April 24, 2023Date of Patent: April 2, 2024Assignee: UT-Battelle, LLCInventors: Tomonori Saito, Zhengping Zhou, Md Anisur Rahman
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Patent number: 11945764Abstract: A method for producing a diglycolamide molecule having the formula: wherein R1 and R2 are independently selected from alkyl groups (R) and acyl groups (C(O)R) in which the alkyl groups (R) contain 1-30 carbon atoms and optionally contain an ether or thioether linkage between carbon atoms, and R5 and R6 are independently selected from hydrogen atom and alkyl groups containing 1-3 carbon atoms; and one or both pairs of R1 and R2 are optionally interconnected to form a ring; the method comprising: combining a diglycolic acid molecule (A) and a secondary amine (B) to form a salt intermediate (C), and heating the salt intermediate (C) to a temperature of 100° C. to 300° C.Type: GrantFiled: June 8, 2022Date of Patent: April 2, 2024Assignee: UT-Battelle, LLCInventors: Santa Jansone-Popova, Ilja Popovs
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Patent number: 11936199Abstract: Polyphase wireless power transfer systems are provided. The transfer system may be used for charging hybrid and electric vehicles. The systems are capable of transferring over 50 KW over an air gap of 15 cm. The systems use a rotating magnetic field to transfer power. The system may comprise transmitter coil assembly. The coil assembly may be one or more layers. The system may employ either unipolar or bipolar coils. The transmitter also comprises compensating capacitance connected in series with at least one coil for each phase. A value of the compensating capacitance for each phase is determined such that the transmitter has at least two independently excitable resonant modes at a resonant frequency. The transmitter is compatible with a plurality of different receivers including three-phase, single phase with a circular coil and single phase with DD coils.Type: GrantFiled: January 2, 2020Date of Patent: March 19, 2024Assignee: UT-BATTELLE, LLCInventors: Jason L. Pries, Veda Prakash Galigekere, Gui-Jia Su
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Patent number: 11919245Abstract: A method for additively manufacturing a microstructure from a caloric material includes providing a geometry of the microstructure to a processor of an additive manufacturing device, the geometry defining a plurality of microfeatures of the microstructure. The method also includes generating, via the processor, a three-dimensional (3D) model representative of the geometry of the microstructure, wherein one or more of the plurality of microfeatures are represented in the 3D model by a non-arcuate profile. Further, the method includes printing, via the additive manufacturing device, the microstructure from the caloric material according to the 3D model. As such, the non-arcuate profile reduces a file size of the 3D model as compared to an arcuate profile.Type: GrantFiled: August 18, 2020Date of Patent: March 5, 2024Assignees: Haier US Appliance Solutions, Inc., UT-Battelle, LLCInventors: Michael Goodman Schroeder, Amelia McDow Elliott, Ayyoub Mehdizadeh Momen
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Patent number: 11919815Abstract: A method for the manufacture of a three-dimensional object using a refractory matrix material is provided. The method includes the additive manufacture of a green body from a powder-based refractory matrix material followed by densification via chemical vapor infiltration (CVI). The refractory matrix material can be a refractory ceramic (e.g., silicon carbide, zirconium carbide, or graphite) or a refractory metal (e.g., molybdenum or tungsten). In one embodiment, the matrix material is deposited according to a binder-jet printing process to produce a green body having a complex geometry. The CVI process increases its density, provides a hermetic seal, and yields an object with mechanical integrity. The residual binder content dissociates and is removed from the green body prior to the start of the CVI process as temperatures increase in the CVI reactor. The CVI process selective deposits a fully dense coating on all internal and external surfaces of the finished object.Type: GrantFiled: March 24, 2022Date of Patent: March 5, 2024Assignee: UT-BATTELLE, LLCInventors: Kurt A. Terrani, Michael P. Trammell, Brian C Jolly
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Patent number: 11916206Abstract: A method of recycling lithium-ion batteries is disclosed. The method includes isolating a composite electrode that comprises an electrode material adhered to a current collector with a polyvinylidene difluoride (PVDF) binder from a spent lithium-ion battery. The method also includes contacting the composite electrode in a polyol fluid capable of releasing the PVDF binder from the current collector without substantially altering either component. The composite electrode may be a cathode or an anode. The method also includes rapidly delaminating the electrode material from the current collector to give a free electrode material and a free current collector, and recovering each of the free electrode material and the free current collector from the mixture. The free electrode material may be reused to prepare another composite electrode, as well as a lithium-ion battery comprising the same, which are also disclosed.Type: GrantFiled: February 16, 2021Date of Patent: February 27, 2024Assignee: UT-BATTELLE, LLCInventors: Ilias Belharouak, Yaocai Bai, Jianlin Li, Rachid Essehli
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Patent number: 11916404Abstract: A wireless power supply power supply including first tuning circuitry coupled directly to a transmitter, the first tuning circuitry including an LCC configuration. The wireless power supply may include second tuning circuitry coupled directly to switching circuitry (e.g., an inverter) of the power supply, where the second tuning circuitry may be operable to direct power from the switching circuitry to the first tuning circuitry for supply to the transmitter, and where the second tuning circuitry includes a reactance operable to establish inductive operation of the switching circuitry at the switching frequency of the switching circuitry.Type: GrantFiled: May 12, 2022Date of Patent: February 27, 2024Assignee: UT-Battelle, LLCInventors: Jason L. Pries, Omer C. Onar, Gui-Jia Su, Veda Galigekere, Mostak Mohammad
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Patent number: 11898226Abstract: A method for additive manufacturing of a composite object containing a bonded network of boron carbide particles and aluminum occupying spaces between boron carbide particles, the method comprising: (i) producing a porous preform constructed of boron carbide by an additive manufacturing process in which particles of boron carbide are bonded together; and (ii) infiltrating molten aluminum, at a temperature of 1000-1400° C., into pores of said porous preform to produce said composite object constructed of boron carbide particles within an aluminum matrix, wherein the boron carbide is present in the composite object in an amount of 30-70 wt. %. The resulting composite material is also herein described.Type: GrantFiled: February 25, 2020Date of Patent: February 13, 2024Assignee: UT-Battelle, LLCInventors: Corson L. Cramer, James O. Kiggans, Jr., Amelia M. Elliott, David C. Anderson
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Patent number: 11892383Abstract: A system and method for sampling a sample material includes a device for directing sample into a capture probe. The device for supplying sample material to the probe can be a device for radiating energy to the sample material to eject sample from the sample material. A probe includes an outer probe housing having an open end. A liquid supply conduit has an outlet positioned to deliver liquid to the open end. An exhaust conduit removes liquid from the open end of the housing. The liquid supply conduit can be connectable to a liquid supply for delivering liquid at a first volumetric flow rate to the open end of the housing. A liquid exhaust system can be in fluid connection with the liquid exhaust conduit for removing liquid from the liquid exhaust conduit at a second volumetric flow rate such that gas with sample is withdrawn with the liquid.Type: GrantFiled: July 18, 2022Date of Patent: February 6, 2024Assignee: UT-BATTELLE, LLCInventors: Vilmos Kertesz, Gary J. Van Berkel
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Patent number: D1021401Type: GrantFiled: July 19, 2022Date of Patent: April 9, 2024Assignee: UT-Battelle, LLCInventor: Mariano M. Ruiz-Rodriquez