Abstract: The present disclosure relates to a device and process for preparing sebacic acid through electromagnetic induction heating coupled with dry constant-temperature alkaline hydrolysis. The device includes an electromagnetic heating cylinder and a reaction kettle arranged in the electromagnetic heating cylinder, heat storage pellets fill space between the reaction kettle and the electromagnetic heating cylinder, and the heat storage pellets adhere to an inner wall of the electromagnetic heating cylinder and an outer wall of the reaction kettle. The upper end of the reaction kettle is provided with a feeding port, a gas outlet and a temperature measuring port, the reaction kettle is also provided with a stirring device, a lower portion of the reaction kettle is provided with a discharging port, and the feeding port, the gas outlet, the temperature measuring port and the discharging port all extend out of the thermal insulation cotton.

Abstract: The present disclosure belongs to the technical field of purification, and particularly relates to a method for purifying an antimony chloride solution through arsenic removal. The method includes: 1) adding copper-antimony alloy into a crude arsenic-containing antimony chloride solution to be treated in a protective atmosphere to obtain an antimony chloride solution containing low-concentration arsenic impurities after a reaction; and 2) performing distillation and concentration on the antimony chloride solution containing low-concentration arsenic impurities to obtain a high-purity antimony chloride solution.

Abstract: The present invention relates to a phosphorescent material and the use thereof, and more particularly to a cyclic tetradentate metal platinum (II) complex phosphorescent material and the use thereof. The present invention provides a cyclic tetradentate metal platinum (II) complex phosphorescent material based on 8-phenylquinoline, benzoxazole, and phenoxy groups. It is a novel tetradentate platinum (II) complex with a 6/6/6 metal fused ring structure. The phosphorescent material of the tetradentate fused ring structure system of the present invention has the characteristics of easy modulation of HOMO and LUMO orbital energy levels and strong luminescence. It has good chemical stability and thermal stability and is easy to fabricate evaporation-type OLED devices. The organic electroluminescent device fabricated using the compound of the present invention as a light-emitting layer can reduce the start-up voltage and remarkably improve the external quantum efficiency.

Abstract: Provided is a double-helix scheduling method for soundcard buffers during sound recording and reproduction, which belongs to the technical field of multimedia communication. The method includes steps as follows: step 1: preparing N frame buffers for each process of the sound recording and the sound reproduction; step 2: adding N sound recording buffers in a sound card, and starting the sound recording; and writing N sound reproduction buffers in the sound card one by one, then starting the sound playing; step 3: writing sound reproduction buffers in the sound card in a sound recording callback function; step 4: adding sound recording buffers in a sound reproduction callback function; and step 5: finishing the sound recording and the sound reproduction.

Abstract: A method for increasing the production of Erinacine A in liquid fermentation of Hericium erinaceus is provided. Through screening of exogenous factors, methyl violet and/or rotenone are selected as the exogenous factors, which ultimately greatly increases the Erinacine A content in the liquid fermentation of Hericium erinaceus, with important production and application value. The liquid fermentation method has high efficiency and can significantly increase the content of Erinacine A in the liquid fermentation process, breaking through the synthetic barrier and having the characteristics of large increase amplitude and fast effect. Compared with other current research on liquid fermentation of Hericium erinaceus to produce Erinacine A, the method for increasing the liquid fermentation production of Erinacine A from Hericium erinaceus is at the highest level, with important research significance.

Abstract: Provided are a directionally assembled flexible MOF hydrogel, a preparation method and a proton conduction application thereof. The prepared method includes: mixing a transition metal salt and L-Glu to prepare a mixed aqueous solution; putting the mixed aqueous solution into a reaction kettle to react at a constant reaction temperature in a range from 80° C. to 200° C. for a reaction period of 1-5 hours, to thereby obtain a reacted aqueous solution; cooling the reacted aqueous solution to room temperature; and washing the reacted aqueous solution after the cooling with deionized water and absolute ethanol, to thereby obtain the directionally assembled flexible MOF hydrogel, L-Glu-M (M?Zr, Fe, or Co), for sealing and storing. The preparation method is simpler and easier to operate, and the directionally assembled flexible MOF hydrogel has great prospects in the field of proton conducting technologies.

Abstract: The present invention is in the field of organic electroluminescence, and specifically relates to a fused ring carbazole tetradentate metal platinum (II) complex and use thereof. In the present invention, a tetradentate metal platinum (II) complex phosphorescent material is obtained by introducing a five-membered heterocyclic system such as benzofuran or benzothiophene at the 5, 6-positions of carbazole. Increasing the ratio of the local state (LE) in the excited triplet state of the cyclic tetradentate platinum (II) complex leads to a lower shoulder peak, which improves the luminescence color purity of the materials, which in turn increases device lifetime. The materials provided by the present invention all have good chemical stability and thermal stability and are easy to fabricate an evaporation-type OLED device.

Abstract: The present invention provides a cyclic tetradentate metal platinum complex phosphorescent material based on pyridine heterocycle, benzoxazole, and carbazole derivatives. It is a novel tetradentate platinum (II) complex with a 6/6/6 metal fused ring phenoxy coordination structure. The phosphorescent material of the N—C—N—N tetradentate fused ring structure system of the present invention have the characteristics of easy modulation of HOMO and LUMO orbital energy levels and strong luminescence. It has good chemical stability and thermal stability, and is easy to fabricate evaporation-type OLED devices.

Abstract: The present invention discloses Stenotrophomonas maltophilia GYH and its application in degrading chlorinated hydrocarbon pollutants, and the application is carried out as follows: resting cells obtained by spreading cultivation of Stenotrophomonas maltophilia GYH are added to a pH=5-8 inorganic salt medium, and then a chlorinated hydrocarbon pollutant is added, and the cells are cultured at 20-35° C. and 140-180 rpm to degrade the pollutant. The concentration of chlorinated hydrocarbon pollutant which can be removed by Stenotrophomonas maltophilia GYH ranges from 2.9 mg/L to 8.93 mg/L. Therefore, the Stenotrophomonas maltophilia has a highly efficient degradation ability for similar industrial pollutants and is able to withstand high concentrations of these pollutants.

Abstract: A method for asymmetrically preparing L-phosphinothricin by oxidation-reduction reaction through biological multienzyme coupling, where D,L-phosphinothricin as a raw material is catalyzed by an enzyme catalysis system to obtain L-phosphinothricin, wherein the enzyme catalysis system comprises a D-amino acid oxidase mutant for catalyzing D-phosphinothricin in D,L-phosphinothricin into 2-carbonyl-4-[hydroxy(methyl)phosphono] butyric acid and a transaminase for catalytic reduction of the 2-carbonyl-4-[hydroxy(methyl)phosphono] butyric acid into L-phosphinothricin; the D-amino acid oxidase mutant is obtained by mutation of D-amino acid oxidase in wild strain Rhodotorula taiwanensis at one of the following sites: (1) M213S-N54V-F58E; (2) M213S-N54V-F58E-D207A; (3) M213S-N54V-F58E-D207A-S60T.

Abstract: An unpowered cowl with adjustable fan blades and a waste heat recovery system for cooking fumes include a cowl body, lifting mechanisms, and a pressure sensor. The cowl body includes a top cap, a bottom ring, and the fan blades disposed between the top cap and the bottom ring. The pressure sensor is disposed on an inner wall of the top cap. An upper end of each of the fan blades is disposed above the top cap and slightly exceeds an outer edge of the top cap. The lifting mechanisms are annularly disposed on the top cap. The lifting mechanisms include lifting plates, electric pushing rods, and lifting shafts. The electric pushing rods are fixed on the top cap. The lifting shafts are connected to the fan blades. The electric pushing rods and the pressure sensor are electrically connected to a control box.

Abstract: The present invention provides a metal platinum (II) and palladium (II) complex, an organic light-emitting device and a display or lighting apparatus, wherein a structure of the metal platinum (II) and palladium (II) complex is as shown in the following formula (I). A cyclometalated platinum (II) and palladium (II) complex based on a tetradentate ligand according to the present invention contains molecules having relatively strong rigidity, can effectively inhibit non-radiative transition generated by molecular vibration, and has relatively high quantum efficiency and luminous intensity. Meanwhile, a tetradentate phosphorescent metal complex of the present invention is a novel parent nucleus structure, which may be developed into a series of efficient phosphorescent metal platinum complexes. The present invention has excellent application prospects in the fields of OLED display and lighting and the like, especially in the field of light-emitting layer materials.

Abstract: A method for measuring the diameter of filament diffraction fringes by frequency domain calculation comprising: building a set of diffraction optical path measurement system and capturing diffraction fringe images; determining the starting point of the imaging range; Simulating the electromagnetic field propagation process in Fraunhofer diffraction, and determining the optimal fringe range considering the noise caused by the difference in CCD sensitivity; Finally calculating the filament diameter by Fourier transform for different lengths of fringe. The final value of the calculated filament diameter is obtained by fitting an envelope to the variation of the diameter. The invention is simple in calculation and has little dependence on the experimental device, which means the superiority of using the frequency domain for parameter measurement, and the measurement accuracy is in the sub-nanometer level.

Abstract: A BMOFs nanosheet based on a ZIF/MIL topology, and a preparation method and an application thereof are provided. The preparation method includes dispersing a MOF material of a ZIFs series in an organic phase, then adding an aqueous phase to obtain a mixture; and adding a MOF material of a MILs series into the mixture, sealing, standing for 1-5 days, filtering, performing centrifugal washing, drying, and performing acetone ultrasonic exfoliation to obtain the BMOFs nanosheet based on the ZIF/MIL topology. The preparation method is simple to operate and moderate in conditions, and the prepared ZIF/MIL BMOFs nanosheet has good electrocatalytic activity and stability in an OER.

Abstract: Disclosed in the present invention is a health state assessment method for equipment based on a knowledge graph attention network, includes: steps: 1) constructing a graph data model which can comprehensively reflect change of a health state of the equipment by deeply integrating association relationships of equipment components, monitoring data dependence relationships and priori information, etc. by means of a knowledge graph and by combining with domain priori knowledge; 2) extracting feature information of the health state knowledge graph by using a graph attention network, and obtaining a target node vector representation which accurately reflects the health state of the equipment by means of learning; and 3) making a health state representation vector of the equipment pass through a fully connected layer to obtain a health state classification prediction probability, and performing training to reducing a loss value relative to a true label, thereby obtaining a health state assessment result.

Abstract: The present application belongs to the field of organic electroluminescence and specifically relates to a fluorinated tetradentate platinum (II) complex, an electronic device, an equipment and application of the fluorinated tetradentate platinum (II) complex. The present application provides a fluorinated tetradentate platinum (II) complex, which has a structure as shown in Formula (I) or Formula (II): In Formula (I) or Formula (II), F1 represents one or more F substitutions on the benzene ring where it is (they are) located, where n is a positive integer from 1 to 5; R1, R2, R3, and R4 are each independently selected from the group consisting of hydrogen, N, a C1-C30 alkyl, a C1-C30 cycloalkyl, and a C6-C60 aryl. The compound has good chemical stability, which can improve and balance the transport of holes and electrons, making energy transfer between the host and guest more efficient.

Abstract: Disclosed are a phosphinothricin dehydrogenase mutant, a recombinant bacterium and a one-pot multi-enzyme synchronous directed evolution method. The phosphinothricin dehydrogenase mutant, with an amino acid sequence as shown in SEQ ID No.1, is obtained by mutating alanine at position 164 to glycine, arginine at position 205 to lysine, and threonine at position 332 to alanine in a phosphinothricin dehydrogenase derived from Pseudomonas fluorescens. The recombinant bacterium is obtained by introducing a gene encoding the phosphinothricin dehydrogenase mutant into a host cell. The host cell can also incorporate a gene encoding a glucose dehydrogenase or a gene encoding a formate dehydrogenase to undergo synchronous directed evolution to achieve double gene overexpression. The one-pot multi-enzyme synchronous directed evolution method of the present invention can screen recombinant bacteria with greatly improved activity.

Abstract: The present invention provides a metal platinum complex, an organic optoelectronic device, and a display or lighting apparatus. A new 6/5/7 metal fused-ring structure is developed by using 8-phenylquinoline structure and a derivative thereof, and benzo five-membered heterocycles and a phenoxy oxygen tetradentate ligand, to obtain a new class of tetradentate cyclometalated platinum complex phosphor material.

Abstract: Disclosed in the present disclosure are a catalytic combustion type hydrogen sensor and a manufacturing method therefor. The catalytic combustion type hydrogen sensor includes a catalytic combustion element and a compensation element, where both the catalytic combustion element and the compensation element are planar film structures taking mica sheets as substrates, and platinum resistors and aluminum oxide film carriers are sequentially adhered on surfaces of the mica sheets. A layer of palladium nanoparticles are further adhered to a surface of the aluminum oxide film carrier of the catalytic combustion element as a catalyst.

Abstract: An electric boiler device based on utilization of residual energy of an elevator includes a heat storage module, an electric heating module and a control module. A heat storage water tank of the heat storage module is replenished with water from a tap water pipe network, and a preheating unit of the heat storage module converts the residual energy of the elevator into heat energy of the heat storage water tank by using an energy consumption resistor. The control module replenishes a heating water tank with water by delivering preheated water to the electric heating module according to a water level of the heating water tank, and controls a heating unit of the electric heat module to heat the heating water tank according to a user-set temperature, and heated hot water is provided through a user water supply pipe network.