Patents Examined by Anthony J Zimmer
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Patent number: 12043544Abstract: A flexible boron nitride nanoribbon aerogel has an interconnected three-dimensional porous network structure which is formed by mutually twining and contacting boron nitride nanoribbons and consists of macropores having a pore diameter of more than 50 nm, mesopores having a pore diameter of 2-50 nm and micropores having a pore diameter of less than 2 nm. The preparation method of the flexible boron nitride nanoribbon aerogel includes the following steps: performing high-temperature dissolution on boric acid and a nitrogen-containing precursor to form a transparent precursor solution, preparing the transparent precursor solution into precursor hydrogel, subsequently drying and performing high-temperature pyrolysis to obtain the flexible boron nitride nanoribbon aerogel. The boron nitride nanoribbon aerogel has excellent flexibility and resilience and can withstand different forms of loads from the outside within a wide temperature range.Type: GrantFiled: January 2, 2020Date of Patent: July 23, 2024Assignee: SUZHOU INSTITUTE OF NANO-TECH AND NANO-BIONICS (SINANO), CHINESE ACADEMY OF SCIENCESInventors: Xuetong Zhang, Guangyong Li
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Patent number: 12040463Abstract: A battery recycling process recovers lithium from nickel-rich cathode material in a recycling stream of end-of-life batteries. A dilute acid leach of a high nickel content cathode material contains a mixture of sulfuric acid based on a molar quantity of lithium in the cathode material. The highly selective leach generates a lithium rich solution with a small amount of nickel removable by nanofiltration to achieve a highly efficient recovery of the lithium contained in the recycling stream. A quantity of the leach acid based on the lithium content and a quantity of water based on a total black mass of the recycling stream results in a highly selective, near pure lithium leach when the recycling stream results from high nickel NMC batteries such as 811.Type: GrantFiled: October 12, 2022Date of Patent: July 16, 2024Assignee: Ascend Elements, Inc.Inventors: Kee-Chan Kim, Eric Gratz
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Patent number: 12017927Abstract: The present invention relates to a method for preparing nickel sulfate using low-nickel ferronickel is disclosed. The method comprises the following steps: (1) grinding ferronickel to obtain ferronickel powder, and then sintering the ferronickel powder with an oxidant to prepare ferronickel oxide powder; (2) adding sulfuric acid to the ferronickel oxide powder prepared in step (1), mixing, heating, and washing with water to prepare a sulfate salt water washing solution; (3) adding a base to the sulfate salt water washing solution prepared in step (2) to adjust the pH value, then adding a fluoride salt to form a precipitate, filtering to remove the precipitate, and drying the filtrate to obtain nickel sulfate. The method provided in the present invention can improve the efficiency of preparing nickel sulfate, reduce the loss of nickel, and prepare nickel sulfate with high purity, the content of Ni potentially reaching 19.73%-21.34%.Type: GrantFiled: May 27, 2022Date of Patent: June 25, 2024Assignees: GUANGDONG BRUNP RECYCLING TECHNOLOGY CO., LTD., HUNAN BRUNP RECYCLING TECHNOLOGY CO., LTD., HUNAN BRUNP EV RECYCLING CO., LTD.Inventors: Haijun Yu, Yingsheng Zhong, Yinghao Xie, Aixia Li, Xuemei Zhang, Changdong Li
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Patent number: 12018356Abstract: A castable, moldable, and/or extrudable structure using a metallic primary alloy. One or more additives are added to the metallic primary alloy so that in situ galvanically-active reinforcement particles are formed in the melt or on cooling from the melt. The composite contains an optimal composition and morphology to achieve a specific galvanic corrosion rate in the entire composite. The in situ formed galvanically-active particles can be used to enhance mechanical properties of the composite, such as ductility and/or tensile strength. The final casting can also be enhanced by heat treatment, as well as deformation processing such as extrusion, forging, or rolling, to further improve the strength of the final composite over the as-cast material.Type: GrantFiled: June 8, 2020Date of Patent: June 25, 2024Assignee: TERVES INC.Inventors: Brian P. Doud, Nicholas J. Farkas, Andrew J. Sherman
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Patent number: 12006579Abstract: The embodiments of the present disclosure relate to a method, system and composition producing a magnetic carbon nanomaterial product that may comprise carbon nanotubes (CNTs) at least some of which are magnetic CNTs (mCNTs). The method and apparatus employ carbon dioxide (CO2) as a reactant in an electrolysis reaction in order to make mCNTs. In some embodiments of the present disclosure, a magnetic additive component is included as a reactant in the method and as a portion of one or more components in the system or composition to facilitate a magnetic material addition process, a carbide nucleation process or both during the electrosynthesis reaction for making magnetic carbon nanomaterials.Type: GrantFiled: November 15, 2022Date of Patent: June 11, 2024Assignee: C2CNT LLCInventor: Stuart Licht
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Patent number: 12006230Abstract: Described herein is a process for making a nickel composite hydroxide with a mean particle diameter d50 in the range from 3 to 20 ?m including combining (a) an aqueous solution of water-soluble salts of nickel and of at least one of cobalt and manganese, and, optionally, at least one of Al, Mg, B, or transition metals other than nickel, cobalt, and manganese, (b) an aqueous solution of an alkali metal hydroxide and (c) an aqueous solution of alkali metal (bi)carbonate or ammonium (bi)carbonate in the molar ratio of 0.001:1 to 0.04:1, and, optionally, (d) an aqueous solution of alkali metal aluminate, in a continuous stirred tank reactor or in a cascade of at least two continuous stirred tank reactors.Type: GrantFiled: October 30, 2019Date of Patent: June 11, 2024Assignee: BASF SEInventors: Thorsten Beierling, Daniela Pfister
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Patent number: 12006217Abstract: Processes for the production of microporous carbon material, for use in electrodes of supercapacitors and secondary batteries, in which particulate metal carbide material is fluidized with a halogen gas at a high temperature in a fluidized bed reactor, the halogen gas is desorbed at a lower temperature of 150° C. to at most 250° C. under vacuum, and then the material is passivated using hydrogen gas and then milled.Type: GrantFiled: March 16, 2022Date of Patent: June 11, 2024Assignee: SKELETON TECHNOLOGIES GMBHInventors: Markarian Ohannes Yeghia Ohannes, Markus Klose, Daniel Weingarth, Jaan Leis
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Patent number: 11999617Abstract: In a process for steam reforming of oxygenates, especially at low steam-to-carbon (S/C) ratios, a feed gas containing oxygenates, such as ethanol, is converted into syngas over a ternary carbide catalyst. Then the reformed gas is either transformed into desired chemicals or mixed into the feed stream to the reformer in a plant, such as an ammonia or methanol plant. The preferred ternary carbide is nickel zinc carbide.Type: GrantFiled: October 17, 2022Date of Patent: June 4, 2024Assignee: HALDOR TOPSØE A/SInventors: Poul Erik Højlund Nielsen, Brian Kjærgaard Olsen, Lived J. Lemus-Yegres
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Patent number: 12000013Abstract: The disclosure relates to processes for extracting lithium from an uncalcined lithium-bearing silicate and recovering a lithium salt therefrom. A slurry of the uncalcined lithium-bearing silicate and a caustic solution is heated in an autoclave to provide a Li-rich sodalite phase. The Li-rich sodalite phase is leached with a dilute acid to produce a lithium-rich pregnant liquor. Various subsequent processes to treat the lithium-rich pregnant liquor to recover a lithium salt, such as lithium phosphate, lithium carbonate, lithium sulphate or lithium hydroxide, are described.Type: GrantFiled: July 24, 2019Date of Patent: June 4, 2024Assignees: Australian Nuclear Science And Technology Organisation, Lithium Australia LimitedInventors: Andrew Napier, Christopher Griffith
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Patent number: 11999620Abstract: Methods of using sorbents to enhance the production of hydrogen from fuel, and related systems, are generally described. In some embodiments, the production of hydrogen from the fuel involves a reforming reaction and/or a gasification reaction combined with a water-gas shift reaction.Type: GrantFiled: November 5, 2020Date of Patent: June 4, 2024Assignee: Massachusetts Institute of TechnologyInventors: Trevor Alan Hatton, Takuya Harada, Cameron G. Halliday
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Patent number: 12000333Abstract: The present disclosure provides systems and methods for processing ammonia. The system may comprise one or more reactor modules configured to generate hydrogen from a source material comprising ammonia. The hydrogen generated by the one or more reactor modules may be used to provide additional heating of the reactor modules (e.g., via combustion of the hydrogen), or may be provided to one or more fuel cells for the generation of electrical energy.Type: GrantFiled: August 16, 2022Date of Patent: June 4, 2024Assignee: AMOGY, INC.Inventors: Young Suk Jo, Hyunho Kim, Gregory Robert Johnson, Matthew Jacob Montgomery
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Patent number: 11999616Abstract: A capacitive element and a dielectric thin film having a small dielectric loss and a large relative permittivity, particularly at low frequencies. [Solution] This dielectric thin film includes an A-B—O—N oxynitride. When the A-B—O—N oxynitride is represented by the compositional formula AaBbOoNn, (o+n)/a<3.00 is satisfied.Type: GrantFiled: August 27, 2019Date of Patent: June 4, 2024Assignee: TDK CORPORATIONInventors: Kumiko Yamazaki, Wakiko Sato, Junichi Yamazaki
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Patent number: 12000015Abstract: This disclosure provides a method of improving gold recovery in a cyanide leaching circuit comprising a gold ore slurry. The method includes the step of providing a gold recovery additive chosen from polyacrylic acid, copolymers of acrylic acid and a sulfonated co-monomer, and combinations thereof, wherein the additive has a weight average molecular weight of from about 500 to about 10,000 g/mol. The method also includes the step of combining the gold recovery additive with the gold ore slurry in the cyanide leaching circuit, wherein the gold recovery additive is present in an amount of from about 10 to about 1000 g per ton of dry gold ore to improve the recovery of gold from the gold ore slurry.Type: GrantFiled: March 30, 2021Date of Patent: June 4, 2024Assignee: Solenis Technologies, L.P.Inventor: Kirill N. Bakeev
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Patent number: 11993514Abstract: Methods comprising: evaporating a catalyst source to produce a catalyst gas; condensing the catalyst gas to produce a catalyst vapor comprising catalyst droplets suspended in a gas phase; and contacting the catalyst vapor with a hydrocarbon gas to catalyze a decomposition reaction of the hydrocarbon gas into hydrogen gas and carbon. And, systems comprising: a catalyst source evaporator that provides a first stream to a reactor; a hydrocarbon source that provides a second stream to the reactor; a cooling column coupled to the reactor via a third stream comprising hydrogen, catalyst liquid, solid carbon, optionally catalyst gas, and optionally unreacted hydrocarbon gas such that the cooling column receives the third stream from the reactor; and wherein the cooling column has effluent streams that include (a) a fourth stream that comprises hydrogen and optionally catalyst gas and (b) a fifth stream that comprises catalyst liquid.Type: GrantFiled: September 16, 2020Date of Patent: May 28, 2024Assignee: Palo Alto Research Center IncorporatedInventors: Jessica Louis Baker Rivest, Divyaraj Desai, Dane Andrew Boysen, Ashish V. Pattekar
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Patent number: 11994062Abstract: The present disclosure provides systems and methods for processing ammonia. The system may comprise one or more reactor modules configured to generate hydrogen from a source material comprising ammonia. The hydrogen generated by the one or more reactor modules may be used to provide additional heating of the reactor modules (e.g., via combustion of the hydrogen), or may be provided to one or more fuel cells for the generation of electrical energy.Type: GrantFiled: August 23, 2023Date of Patent: May 28, 2024Assignee: AMOGY, Inc.Inventors: Young Suk Jo, Hyunho Kim, Gregory Robert Johnson, Matthew Jacob Montgomery
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Patent number: 11993520Abstract: A method for recovering NiSO4.6H2O crystals from a nickel rich organic phase is provided. The method includes contacting a nickel rich organic phase with an aqueous strip solution of sufficient H2SO4 concentration to extract nickel from the organic phase and of sufficient Ni2+ concentration to precipitate NiSO4.6H2O crystals and form a nickel lean organic phase. Also provided are methods for recovering NiSO4.6H2O crystals that include preceding processing steps, including low temperature pressure oxidation (LTPOX) autoclaving of a nickel sulphide concentrate to afford a pregnant leach solution (PLS).Type: GrantFiled: September 26, 2019Date of Patent: May 28, 2024Assignee: IGO LimitedInventors: Karel John Osten, Rossano Antonio Grassi, Arturo Gutierrez Clausdorff, Ryan Colin Harrison
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Patent number: 11994061Abstract: The present disclosure provides systems and methods for processing ammonia. The system may comprise one or more reactor modules configured to generate hydrogen from a source material comprising ammonia. The hydrogen generated by the one or more reactor modules may be used to provide additional heating of the reactor modules (e.g., via combustion of the hydrogen), or may be provided to one or more fuel cells for the generation of electrical energy.Type: GrantFiled: August 16, 2022Date of Patent: May 28, 2024Assignee: AMOGY INC.Inventors: Young Suk Jo, Hyunho Kim, Gregory Robert Johnson, Matthew Jacob Montgomery
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Patent number: 11987496Abstract: A method for producing a bis(fluorosulfonyl)imide lithium salt is disclosed. The method includes the steps of: (a) reacting bis(chlorosulfonyl)imide with NH4F(HF)n (n=0-10) to prepare ammonium bis(fluorosulfonyl)imide; and (b) reacting the ammonium bis(fluorosulfonyl)imide with a lithium base, wherein in at least one of steps (a) and (b), after the reaction, a process of adding an alkoxy trialkyl silane to the reaction solution to remove a fluorine anion is performed.Type: GrantFiled: September 4, 2019Date of Patent: May 21, 2024Assignee: DAEGU CATHOLIC UNIVERSITY INDUSTRY ACADEMIC COOPERATION FOUNDATIONInventors: Sang Ryul Lee, Kyoung Chol Kim, Ja Young Park, Ji Hyeong Kim, Jeong In Kim, Seok Ju Lee, Jongyun Jang, Seongjeong Lee, Mingi Chu, Dong Wook Kang
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Patent number: 11981580Abstract: A method for producing a halide includes heat-treating a mixed material in an inert gas atmosphere, the mixed material being a mixture of M2O3, NH4X, and LiZ. The M includes at least one element selected from the group consisting of Y, a lanthanoid, and Sc. The X is at least one element selected from the group consisting of CI, Br, I, and F. The Z is at least one element selected from the group consisting of CI, Br, I, and F.Type: GrantFiled: May 16, 2021Date of Patent: May 14, 2024Assignee: PANASONIC INTELLECTUAL PROPERTY MANAGEMENT CO., LTD.Inventors: Takashi Kubo, Yusuke Nishio, Akihiro Sakai, Akinobu Miyazaki
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Patent number: 11975979Abstract: A method for growing bulk boron arsenide (BA) crystals, the method comprising utilizing a seeded chemical vapor transport (CVT) growth mechanism to produce single BAs crystals which are used for further CVT growth, wherein a sparsity of nucleation centers is controlled during the further CVT growth. Also disclosed are bulk BAs crystals produced via the method.Type: GrantFiled: June 20, 2019Date of Patent: May 7, 2024Assignee: UNIVERSITY OF HOUSTON SYSTEMInventors: Zhifeng Ren, Fei Tian, Gang Chen, Bai Song, Ke Chen, Li Shi, Xi Chen, Sean Sullivan, David Broido, Navaneetha Krishnan Ravichandran