Abstract: Method and apparatus which can provide continuous monitoring of the partial pressure of one or more gases in an atmosphere or feed stream, over an indefinite period of time and at a minimal cost. The method and apparatus of the present invention operates by monitoring the change in frequency of a piezoelectric element which has been coated with a film formed from manganese tertiary phosphine polymer complex. As the polymer absorbs or releases gas the frequency of the piezoelectric device will be altered.

Abstract: The present invention relates to a fractionating and observation cel of a liquid analysis device comprising a rotor, a central distribution cup or container for said liquid, and an assembly of cells on the periphery of the rotor, wherein the cells and the duct are formed by welding of two plastic pieces comprising said rotor, the liquid feed and gas evacuation duct is provided by the space existing between the two plastic pieces welded to each other by two welding seams along the edges of each duct, the opposite faces of the said pieces that constitute the duct with the said seams being left rough from molding.

Abstract: Independent reagent matrix zones are created in hydrophobic open celled natural or synthetic material by heating the open celled material along parallel lines at right angles to the length of a reagent test device so as to seal the material at predetermined intervals and thereby form separate reagent matrix areas on the same reagent test device. This technique results in a reagent test device which eliminates the runover problem which has caused cross contamination between reagent areas and resulted in the failure of reagent test devices to perform properly.

Abstract: A test composition comprising glucose oxidase, a peroxidatively active component, a chromogenic indicator system capable of providing a detectable response and a borate buffer capable of providing an initial pH above about pH 7 is particularly useful for the semiquantitative determination of high range glucose, (i.e. glucose concentrations of 1,000 mg/dL to 10,000 mg/dL). A preferred indicator system is a water soluble iodide salt and poly(vinylpyrrolidone). The use of a borate buffer capable of providing an initial pH above about pH 7 permits greatly improved resolution for the semiquantitative determination of high range glucose when the test composition is incorported onto a carrier matrix to prepare a solid state unitary test device.

Abstract: The determination of water by the Karl Fischer method is carried out using a reagent containing sulfur dioxide, iodine and a base. The determination is carried out in a liquid medium in which the sample under investigation has been dissolved. The solvents used are, above all, methanol and 2-methoxyethanol. The presence of a further solvent which enables the reaction to take place without interference is advantageous. Solvents suitable for this purpose are lower alkanols which are substituted by halogen atoms and/or phenyl radicals. These alkanols are also employed as the solvent in Karl Fischer reagents.

Abstract: Reagent test device are prepared in which reagent carrier matrices are separated from each other by hydrophobic barrier pads of identical height to the reagent carrier matrices such that liquid present in a reagent matrix material is retained therein and prevented from running over into another reagent matrix area present on the same test device.

Abstract: There is described a capillary transport device wherein the transport zone includes energy barriers such as ribs extending partway from one opposing surface to the other opposing surface of the zone, and slot means for preventing air entrapment, such means being in each energy barrier, or in every other energy barrier.There is also described a method of providing a non-mixing junction between two miscible liquids.

Abstract: A system for monitoring ambient carbon monoxide. Light from a source (14) is directed against a measuring element (10) which darkens in color as it absorbs carbon monoxide. The light reflected from the element is received by a photocell (16) which generates an electrical signal proportional to the intensity of the reflected light received thereby. The signal is sampled periodically, and stored in a microprocessor (24) which computes the rate of change of the signals. The periodic measurement of the intensity of the light can be varied in response to the rate of change of the light intensity measurement. When the rate of change reaches a level indicative of an unsafe level of ambient carbon monoxide, an alarm (34) is energized. Light from the source is simultaneously directed against a reference element (12) with the light reflected therefrom being received by a photocell (18) which generates an electrical signal proportional to the intensity of the light received thereby.

Abstract: Fecal occult blood tests of enhanced sensitivity and specificity are provided by employing (1) a developer composition comprising a solution of a hydroperoxide in a solvent comprising at least about 50% by volume of a solvent for iron protoporphyrins such as dimethyl sulfoxide and/or (2) a solid test matrix comprising a solid support impregnated with a leuco dye and a hemoprotein solubilizing agent. Test results may be further improved by incorporating plant peroxidase inhibitors, iron/copper chelating agents and buffers in the developer and/or test matrix.

Abstract: A reagent and method for in vitro determination of the eye irritating properties of individual compounds and/or mixtures is disclosed. The material to be assessed is combined with the reagent which provides a response, for example, the production of a precipitate, which is proportional to the deleterious response elicited by the material in the human eye.

Abstract: In analysis of a liquid sample by adding a reagent to a liquid sample, thereby initiating reaction, and measuring a rate of the reaction, thereby quantitatively determining an analytical item being contained in the sample and taking part in the reaction, the analysis is carried out by measuring a physical quantity of the liquid sample, setting an effective limit level for the sample, then adding a reagent to the sample, measuring a physical quantity of the resulting liquid mixture, and computing the analysis value of the desired analytical value of the sample from the physical quantities so far measured before the effective limit level is reached. An exact effective limit level can be automatically set for the individual sample, and thus an analysis value can be obtained with high exactness.

Abstract: A method for quantitative determination of bilirubin is disclosed. The method comprises bringing a bilirubin-containing aqueous liquid sample into contact with a hydrophobic bilirubin extracting composition containing a hydrophobic amine capable of extracting bilirubin. The amine extracts the bilirubin in said aqueous liquid sample. Photometry is then used to determine the concentration of bilirubin extracted with the bilirubin extracting composition. A device for use in this method is also disclosed. The device has a layer containing a hydrophobic bilirubin extracting composition containing a hydrophobic amine capable of extracting bilirubin.

Abstract: A method of analyzing molecular layers of amino-functional group coupling agents on inorganic substrates is disclosed. A saturated solution of 1-dimethylaminonaphthalene-5-sulfonyl chloride is added to a sample to be tested, and sufficient time is allowed, with or without heating, for the reaction of the 1-dimethylaminonaphthalene-5-sulfonyl chloride with any amino functional group coupling agent which might be present. The color intensity of the reaction product is compared under ultraviolet light in an otherwise substantially dark room with the color intensity of standards representative of known thicknesses of coupling agent to determine the existence and thickness of the coupling agent on the particles being analyzed.

Abstract: Method and apparatus system for quickly determining on site if chemicals which are to be mixed can be done so safely without having a run-away exothermal reaction take place and without exposing personnel to the chemicals. The invention is particularly useful in dumping quantities of waste chemicals into a waste chemical reservoir containing a very complex mixture of many other waste chemicals.

Abstract: Conversion flask for use is an apparatus for the sequential performance of chemical processes on a sample of chemical material. The flask includes at least three capillary tubes and a large bore tube extending into the interior thereof for the introduction and withdrawal of various fluids. The capillary tubes are constructed to introduce a plurality of fine bubbles into a liquid within the flask to agitate the liquid and accelerate drying, to impinge chemicals on the walls of the flask, and to produce a spray onto the interior walls of the flask in proximity to its upper end to wash down the interior walls of the flask.

Abstract: A method for measuring binder characteristics in a mat of binder coated mineral fibers, the binder having a first cure indicator constituent, the amount of which changes at a first rate as the binder is cured, and a second cure indicator constituent, the amount of which changes at a second rate, different from the first rate, as the binder is cured, comprising radiating the mat and binder with first, second, third and fourth wavelengths of electromagnetic radiation, the first wavelength being absorbed by the binder including the first cure indicator constituent, the second wavelength being a reference for the first wavelength and being not absorbed by the binder or the cure indicator constituents, the third wavelength being absorbed by the binder including the second cure indicator constituent, and the fourth wavelength being a reference for the third wavelength and being not absorbed by the binder or the cure indicator constituents, and further sensing the amount of energy of the first, second, third and fou

Abstract: An improved distillation apparatus is disclosed containing expansion means and vapor draw means surrounded by heating means to provide vapor/liquid phase separation entirely within the heating bath. The apparatus is especially useful for determining phenol content in refinery waste streams.

Abstract: Gas sensor which is constructed of an electrically insulating base, electrodes formed on said base, and a gas sensitive film formed on the surface of said base at a portion where it detects a gas to be sensed, e.g., an oxygen gas. The gas sensor of the present invention is characterized in that the gas sensitive film is a thermal-sprayed film which is made of an oxide having a perovskite structure. The thermal-sprayed film has its surface formed with fine cracks to have its effective surface area increased so that the response is speeded up. Moreover, the thermal spraying process is so effected during the formation of the oxide film that an impurity to adversely affect the reliability may be avoided from being mixed.The gas sensor may have said gas sensitive film coated with a ceramic material so that is performance may be further improved while protecting the gas sensitive film. Furthermore, it is also effective to add another sensor with the electrically insulating base being commonly used.

Abstract: An exploration method is disclosed for mapping subsurface migration of crude petroleum by measuring electron spin resonance signals from materials within samples of the subsurface formations and identifying the samples that contain petroleum crude by detecting enhancement and/or suppression of the electron resonance signals due to the addition of a chemical material. Electron spin resonance signals from crude oil are enhanced by the presence of iodine and suppressed by the presence of ferric chloride.

Abstract: Disclosed is a method for measuring aggregation in sponge cells using a clinical aggregometer. In addition, using the marine sponge cell as an in vitro model for neutrophil aggregation, a method to determine the relative anti-inflammatory properties of non-steroidal anti-inflammatory pharmaceutical agents by clinical aggregometry is also disclosed.