Patents Examined by Brandi M Doyle
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Patent number: 11708287Abstract: A method for the treatment of oil-based sludge by thermal desorption, characterized in that it comprises a step of conditioning of the sludge to be treated which includes the conditioning of the oil-based sludge with rice husk in a 1:2 ratio, before entering the TDU, increasing the technical and economic viability and cost relation of the thermal desorption for oil-based sludge treatment, showing better performance, and making possible the treatment of sludge on an industrial scale with effective rates of 28.6 m3/day, oil recovery of 54%, with a volumetric increase of 19%, compared to the original volume, and a fuel consumption adjusted to the historical data of the TDU from the economic point of view, which allows to have a high amount of rice husk, reducing the costs associated with the elimination of this agro-industrial waste.Type: GrantFiled: December 17, 2020Date of Patent: July 25, 2023Inventor: William Ariza Fontecha
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Patent number: 11697774Abstract: A modular crude oil refinery (MCOR) is designed for smaller scale deployment with a capacity to process in the range of 3,000-4,000 barrels of crude oil per day in a single production unit and with the potential to scale to over 100,000 barrels per day with linked production units. More specifically, a MCOR includes a low temperature, low pressure primary separation reactor, condensing system and recirculation systems operating in a closed loop configuration that enable the production of both heavy and light hydrocarbon products with substantially no emissions. The MCOR has the capability to receive and process crude-oil feedstocks of varying API gravity and be controlled to produce a variety of both heavy and light products including cleaner-burning bunker fuels, jet fuels, diesel fuels, gasoline fuels and asphalt binders.Type: GrantFiled: January 25, 2021Date of Patent: July 11, 2023Assignee: DESIGNER FUELS LLCInventors: George E. Snider, Darin Diorio
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Patent number: 11685868Abstract: A catalytic cracking gasoline upgrading method is provided. First, in the presence of a prehydrogenation catalyst, the full-range FCC gasoline undergoes prehydrogenation in a prehydrogenation reactor to remove diolefins, mercaptans and sulfides, and then the prehydrogenation product undergoes selective hydrodesulfurization in the presence of a hydrodesulfurization-isomerization catalyst, and straight-chain olefins are isomerized into single-branched olefins or single-branched alkanes, thus obtaining a low-olefin, ultralow-sulfur and high-octane clean gasoline product.Type: GrantFiled: December 26, 2020Date of Patent: June 27, 2023Assignee: SOUTHEAST UNIVERSITYInventors: Tinghai Wang, Yuanyuan Yue, Xiaojun Bao, Xueli Wang, Jie Liu, Pei Yuan, Haibo Zhu, Zhengshuai Bai
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Patent number: 11674091Abstract: A catalytic cracking gasoline prehydrogenation method is provided. Thiol etherification and double bond isomerization reactions are carried out on catalytic cracking gasoline through a prehydrogenation reactor. The reaction conditions are as follows: the reaction temperature is between 80° C. and 160° C., the reaction pressure is between 1 MPa and 5 MPa, the liquid-volume hourly space velocity is from 1 to 10 h?1, and the hydrogen-oil volume ratio is (3-8):1; a prehydrogenation catalyst comprises a carrier and active ingredients, the carrier contains an aluminium oxide composite carrier with a macroporous structure and one or more of ZSM-5, ZSM-11, ZSM-12, ZSM-35, mordenite, amorphous form aluminum silicon, SAPO-11, MCM-22, a Y molecular sieve and a beta molecular sieve, the surface of the carrier is loaded with one or more of the active ingredients cobalt, molybdenum, nickel and tungsten; based on oxides, the content of the active ingredients is between 0.1% and 15.5%.Type: GrantFiled: December 24, 2020Date of Patent: June 13, 2023Assignee: FUZHOU UNIVERSITYInventors: Tinghai Wang, Xiaojun Bao, Yuanyuan Yue, Xueli Wang, Jie Liu, Haibo Zhu, Pei Yuan, Zhengshuai Bai
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Patent number: 11648488Abstract: Method for revamping a refining section of a methanol distillation plant comprising a medium pressure (MP) column a low pressure (LP) column, wherein both said columns comprise at least one bottom boiler, a gaseous stream of distilled methanol withdrawn from the MP column is fed to at least one bottom boiler of the LP column and a liquid solution containing methanol withdrawn from the MP column is fed to the LP column, the method of revamping comprising the installation of a high pressure (HP) column; the installation of a line feeding a gaseous stream of distilled methanol from the HP column to at least one bottom boiler of the MP column and the installation of a bottom line for exporting from the HP column a liquid stream consisting essentially of water.Type: GrantFiled: April 10, 2019Date of Patent: May 16, 2023Assignee: Casale SAInventor: Raffaele Ostuni
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Patent number: 11629297Abstract: Disclosed herein are methods, systems, and compositions for providing catalysts for tail gas clean up in sulfur recovery operations. Aspects of the disclosure involve obtaining catalyst that was used in a first process, which is not a tailgas treating process and then using the so-obtained catalyst in a tailgas treating process. For example, the catalyst may originally be a hydroprocessing catalyst. A beneficial aspect of the disclosed methods and systems is that the re-use of spent hydroprocessing catalyst reduces hazardous waste generation by operators from spent catalyst disposal. Ultimately, this helps reduce the environmental impact of the catalyst life cycle. The disclosed methods and systems also provide an economically attractive source of high-performance catalyst for tailgas treatment, which benefits the spent catalyst generator, the catalyst provider, and the catalyst consumer.Type: GrantFiled: October 4, 2021Date of Patent: April 18, 2023Assignee: Evonik Operations GmbHInventors: Terence McHugh, James Seamans, Brian Visioli, Pettus Kincannon, John Wesley Thompson, Alexander Enderlin
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Patent number: 11603498Abstract: In an aspect, a method of decontaminating a hydrocarbon fluid comprises applying an ultrasonic wave to the hydrocarbon fluid in a storage tank to maintain or reduce an amount of a microorganism in the storage tank; wherein a source of the ultrasonic wave is located within the storage tank and the storage tank has at least one of an inner volume of greater than or equal to 20 meters cubed and/or that is capable of storing 55 to 160,000 liters of the hydrocarbon fluid. In another aspect, a method of decontaminating a hydrocarbon fluid comprises applying an ultrasonic wave to the hydrocarbon fluid to disrupt a cell membrane of a microorganism to form a disrupted microorganism and to reduce a particle size of the disrupted microorganism to be less than or equal to 1.5 micrometers thereby forming a clean hydrocarbon fluid suitable for injecting through an injection nozzle.Type: GrantFiled: March 15, 2021Date of Patent: March 14, 2023Assignee: PHOENIX ENVIRONMENTAL, INC.Inventors: Davis Smith, Casey Joe Smith
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Patent number: 11590469Abstract: A method for producing an electrically-conductive pellet includes reducing a size of a first material. The method also includes wetting the first material to produce a first slurry. The method also includes introducing the first slurry into a fluidizer to produce a first pellet. The method also includes reducing a size of a second material. The second material is an electrically-conductive material. The method also includes wetting the second material to produce a second slurry. The method also includes applying the second slurry to the first pellet.Type: GrantFiled: November 15, 2021Date of Patent: February 28, 2023Assignee: CARBO CERAMICS INC.Inventors: Minjung Cho, Todd Roper, Thu Lieng
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Patent number: 11572515Abstract: A hydrocracking process is disclosed. The hydrocracking process comprises hydrocracking a hydrocarbon feed stream in a hydrocracking reactor in the presence of a hydrogen stream and a hydrocracking catalyst to produce a hydrocracked effluent stream. The hydrocracked effluent stream is separated in a separator to provide a vapor hydrocracked stream and a liquid hydrocracked stream. The liquid hydrocracked stream is fractionated to provide a naphtha stream, a kerosene stream having a T90 temperature of about 204° C. (399° F.) to about 238° C. (460° F.), a diesel stream having a T90 temperature of about 360° C. (680° F.) to about 383° C. (721° F.) and an unconverted oil stream. The kerosene stream, the unconverted oil stream, and a portion of the diesel stream is recycled to the hydrocracking reactor for hydrocracking.Type: GrantFiled: December 31, 2020Date of Patent: February 7, 2023Assignee: UOP LLCInventors: Massimo Sangalli, John A. Petri, Magaly Estremera, Yoga R Ayar
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Patent number: 11542446Abstract: Methods are provided for using a molecular sieve catalyst for dewaxing formed using a synthesis mixture comprising a morphology modifier. The catalyst may be used, for example, for production of a lubricant base stock. For example, ZSM-48 crystals formed using the morphology modifier (and/or formulated catalysts made using such crystals) can have an increased activity and/or can provide an improved yield during catalytic dewaxing of lubricant base stocks.Type: GrantFiled: August 14, 2019Date of Patent: January 3, 2023Assignee: Exxon Mobil Technology and Engineering CompanyInventors: Preeti Kamakoti, Scott J. Weigel, Stephen J. McCarthy, Shifang L. Luo, Sina Sartipi, Martine Dictus, Marc H. Anthonis, Helge Jaensch
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Patent number: 11518947Abstract: The present disclosure generally relates to dispersions useful for scavenging hydrogen sulfide. The dispersions may be anhydrous and contain a solvent and a hydrogen sulfide scavenging compound. The hydrogen sulfide scavenging compound may be hexamine, for example. The solvent may be a C2-8 polyol, such as glycerin.Type: GrantFiled: March 26, 2018Date of Patent: December 6, 2022Assignee: ECOLAB USA Inc.Inventor: Kim R. Solomon
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Patent number: 11504699Abstract: A method of making a hydrodesulfurization catalyst having nickel and molybdenum sulfides deposited on a support material containing mesoporous silica that is optionally modified with zirconium. The method of making the hydrodesulfurization catalyst involves a single-step calcination and reduction procedure. The utilization of the hydrodesulfurization catalyst in treating a hydrocarbon feedstock containing sulfur compounds (e.g. dibenzothiophene, 4,6-dimethyldibenzothiophene) to produce a desulfurized hydrocarbon stream is also provided.Type: GrantFiled: June 27, 2019Date of Patent: November 22, 2022Assignee: King Fahd University of Petroleum and MineralsInventors: Khalid R. Alhooshani, Saheed Adewale Ganiyu
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Patent number: 11499108Abstract: Disclosed herein are scavenging and antifouling compositions useful in applications relating to the production, transportation, storage, and separation of crude oil and natural gas. Also disclosed herein are methods of using the compositions as scavengers and antifoulants, particularly in applications relating to the production, transportation, storage, and separation of crude oil and natural gas.Type: GrantFiled: January 21, 2020Date of Patent: November 15, 2022Assignee: ChampionX USA Inc.Inventors: Lawrence J. Karas, Matthew Aaron Trevino, Kellen Harkness, Jeffrey Robert Eveland
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Patent number: 11492258Abstract: An object of the present invention is to provide a method for producing a bis(fluorosulfonyl)amide alkali metal salt powder having high purity while suppressing reduction in yield due to thermal decomposition, etc. The method for producing a bis(fluorosulfonyl)amide alkali metal salt powder according to the present invention comprises precipitating a bis(fluorosulfonyl)amide alkali metal salt by conducting distillation using a thin-film evaporator while adding a poor solvent for the bis(fluorosulfonyl)amide alkali metal salt such as an aromatic hydrocarbon solvent and a linear or branched aliphatic hydrocarbon solvent to a solution formed by dissolving the bis(fluorosulfonyl)amide alkali metal salt in a good solvent for the bis(fluorosulfonyl)amide alkali metal salt such as an ester solvent and nitrile solvent.Type: GrantFiled: February 26, 2019Date of Patent: November 8, 2022Assignee: NIPPON SODA CO., LTD.Inventors: Kenichi Hayashi, Hiroyuki Nishijima, Masahiro Hori, Toshiaki Nishizawa, Asami Kohori
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Patent number: 11485918Abstract: Processes herein may be used to thermally crack various hydrocarbon feeds, and may eliminate the refinery altogether while making the crude to chemicals process very flexible in terms of crude. In embodiments herein, crude is progressively separated into light and heavy fractions utilizing convection heat from heaters used in steam cracking. Depending on the quality of the light and heavy fractions, these are routed to one of three upgrading operations, including a fixed bed hydroconversion unit, a fluidized catalytic conversion unit, or a residue hydrocracking unit that may utilize either an ebullated bed reactor with extrudate catalysts or a slurry hydrocracking reactor using a homogeneous catalyst system, such as a molybdenum based catalysts which may optionally be promoted with nickel. Products from the upgrading operations can be finished olefins and/or aromatics, or, for heavier products from the upgrading operations, may be used as feed to the steam cracker.Type: GrantFiled: March 16, 2020Date of Patent: November 1, 2022Assignee: LUMMUS TECHNOLOGY LLCInventors: Ujjal K. Mukherjee, Kandasamy Sundaram
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Patent number: 11479729Abstract: A method of upgrading a petroleum feedstock, the method comprising the steps of introducing a disulfide oil, a water feed, and a petroleum feedstock to a supercritical water upgrading unit, and operating the supercritical water upgrading unit to produce a product gas stream, a product oil stream, and a used water stream.Type: GrantFiled: March 24, 2021Date of Patent: October 25, 2022Assignee: Saudi Arabian Oil CompanyInventors: Ki-Hyouk Choi, Emad N. Shafei, Mohammed Zuhair Albahar, Abdulaziz A. Ghabbani
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Patent number: 11466220Abstract: Described is a novel process for fractionating biomass pyrolysis oil quantitatively into energy dense hydrophobic aromatic fraction and water-soluble organics in an economical and energy efficient manner. Using the concepts of solvents and anti-solvent behaviours to separate the pyrolysis oil, which is an emulsion, a method utilising minimal quantities of solvents and water is proposed, By comparison with the existing methods to isolate the hydrophobic aromatic fraction, there is a volume reduction of greater than 50:1. Additionally, there is a significant time saving over the 24 hours for the accepted method as a solvent, and the anti-solvent system is spontaneous.Type: GrantFiled: June 21, 2017Date of Patent: October 11, 2022Assignee: ALDER ENERGY, LLCInventors: Sanjeev Gajjela, Ralph Phillips Overend, Javier Gonzalez Catalan, Zhiheng Wu, Patricia Lapuente, Jose Antonio Medrano Catalan
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Patent number: 11459514Abstract: In the hydrocracking process in accordance with the invention, which comprises a hydrocracking section, a high pressure hot separator and a fractionation section, upstream of the fractionation section, a stripper or reboiler column type separation column is added which treats at least a portion of the heavy effluent obtained from the high pressure hot separator. All or a portion of the bottom fraction from said column, which is rich in polynuclear aromatic compounds, is purged. At least a portion of the bottom fraction obtained from the fractionation section, which is constituted by unconverted products, is recycled to the reaction section.Type: GrantFiled: December 21, 2017Date of Patent: October 4, 2022Assignee: AXENSInventor: Nicolas Pupat
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Patent number: 11446586Abstract: According to an example aspect of the present invention, there is provided a method for separating and purifying furan carboxylates from a crude reaction mixture comprising furans, by utilizing high vacuum distillation in a total heating environment.Type: GrantFiled: February 11, 2019Date of Patent: September 20, 2022Assignee: TEKNOLOGIAN TUTKIMUSKESKUS VTT OYInventors: David Thomas, Juha Linnekoski
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Patent number: 11407950Abstract: A process for steam cracking a whole crude including a volatilization step performed to maintain a relatively large hydrocarbon droplet size. The process may include contacting a whole crude with steam to volatilize a portion of the hydrocarbons, wherein the contacting of the hydrocarbon feedstock and steam is conducted at an initial relative velocity of less than 30 m/s, for example. The resulting vapor phase, including volatilized hydrocarbons and steam may then be separated from a liquid phase comprising unvaporized hydrocarbons. The hydrocarbons in the vapor phase may then be forwarded to a steam pyrolysis reactor for steam cracking of the hydrocarbons in the vapor phase.Type: GrantFiled: March 16, 2020Date of Patent: August 9, 2022Assignees: Lummus Technology LLC, Saudi Aramco Technologies CompanyInventors: Dennis Maloney, Kandasamy Sundaram, Raghu Narayan, Abdul Rahman Zafer Akhras