Abstract: A composition for and method of performing primary cementing operations is disclosed. The method comprises the use of a water slurry of a thixotropic cementing composition which rapidly develops sufficient static gel strength to reduce if not eliminate annular gas migration.

Abstract: Pure or substantially enriched 2,4- and 2,6-dinitrotoluene can be isolated from a mixture containing these isomers if such a mixture is distilled under a pressure of 0.5 to 20 mbar at a temperature of 80.degree. to 200.degree. C. with exclusion of reducing conditions.

Abstract: Foamed well cementing compositions and methods of performing cementing operations in salt containing subterranean environments are provided. The compositions are comprised of hydraulic cement, salt water, dispersed gas and a foaming agent selected from the group consisting of surfactants of the formula R--(OR').sub.n --OSO.sub.3.sup.- X.sup.+.

Abstract: The invention provides well working compositions containing a particulate additive to decrease the seepage loss of the fluid to fluid permeable formations contacted by the compositions.

Abstract: A polysiloxane polymer having pendant aromatic groups that is useful in increasing the viscosity of carbon dioxide. That polymer can be formed by reacting a polysiloxane containing at least one olefinic group with a phenyldialkylsilane. That polymer can be used in a method for recovering oil from an underground oil-bearing earth formation penetrated by an injection well and a producing well, in which method carbon dioxide is injected into the formation to displace oil towards the producing well from which oil is produced to the surface. The viscosity of the carbon dioxide injected into the formatin is increased at least three-fold by the presence of a sufficient amount of the polymer and a sufficient amount of a cosolvent to form a solution of the polymer in the carbon dioxide.

Abstract: Brine-in-glycol emulsions are shown for use as well working fluids. The fluids have a glycol external phase and a brine internal phase. The separate phases are emulsified to create an emulsion and weighted with traditional weighting agents. The external phase is soluble or dispersible in sea water when diluted upon discharge.

Abstract: A method for the inhibition of scale deposition on the surfaces of a well coproducing oil and scale forming brines comprising injecting into the well reservoir an acidic aqueous solution at a first pH containing dissolved therein a scale inhibitor, multivalent metal ions, and a heat sensitive pH increasing substance which decomposes at elevated temperatures liberating an alkaline compound such that the solution is inherently heated by the higher ambient reservoir temperature to a temperature at which the alkaline compound is liberated from the heat sensitive substance thus raising the pH of the solution to a point at which a sparingly soluble multivalent metal salt of the scale inhibitor is phase separated from the solution on the porous surfaces of the reservoir rock formation, providing for a slow release of inhibitor into the produced brines when the well is in its production phase.

Abstract: Methods and compositions for enhancing magnetic resonance imaging in at least a portion of a warm-blooded animal.

Abstract: A process for inhibiting corrosion in oil production fluids resides in adding to the oil production fluids an effective amount of betaine or ampholyte of the formulas 1 or 2 ##STR1## wherein R.sup.1 is C.sub.10 -C.sub.20 -alkyl or C.sub.10 -C.sub.20 -alkenyl, preferably C.sub.14 -C.sub.18 -aklyl or C.sub.14 -C.sub.18 -alkenyl and R.sup.2 and R.sup.3 are C.sub.1 -C.sub.4 -alkyl, preferably methyl.

Abstract: This invention relates to an improved aqueous based drilling fluid and specifically to a water soluble polymer that imparts desirable performance characteristics to the final drilling fluid. The invention also relates to the method for preparation of the polymer and drilling fluid. The water soluble polymer is especially useful in that it exhibits superior tolerance to divalent cations, salts, solids and elevated temperatures when added to aqueous drilling fluids. The polymer additive is characterized by increased viscosity at low shear rates and improved fluid loss control thereby exhibiting superior rheological and thixotropic properties. The polymer consists of reaction products of sulfonated monomers and monomers added to enhance the functional characteristics of the polymer.

Abstract: Radioactive high molecular weight metal-binding protein compositions and a method for therapeutic radiation treatment including the treatment of rheumatoid arthritis comprising injection of a radioactive high molecular weight metal-binding protein compositions are disclosed.

Abstract: Macrocyclic derivatives of 1,4,7,10-tetraazacyclododecane of general formula (I) hereinbelow, wherein A is a group of formula (II) hereinbelow, in which R is H or alkyl or optionally substituted benzyl or a H(OCH.sub.2 CH.sub.2).sub.1-4-, Me(OCH.sub.2 CH.sub.2).sub.1-4-, or Et(OCH.sub.2 CH.sub.2).sub.1-4- group, X or O--R.sub.1, in which R.sub.1 is H or alkyl, hydroxyalkyl, alkoxyalkyl, alkoxyhydroxyalkyl or a polyoxaalkyl group or X is --NR.sub.2 R.sub.3, in which R.sub.2 and R.sub.3 are H or alkyl, hydroxyalkyl, alkoxyalkyl or alkoxyhydroxyalkyl, and B.sub.1, B.sub.2 and B.sub.3 have the same meanings as A or are H or a group of formula (III) hereinbelow, in which R.sub.4 is H or alkyl, Y is a O--R.sub.5 group, wherein R.sub.5 is H or alkyl, hydroxyalkyl, alkoxyalkyl, alkoxyhydroxyalkyl or a polyoxaalkyl group, or Y is a --NR.sub.6 R.sub.7 group, wherein R.sub.6 and R.sub.

Abstract: A corrosion inhibitor for an acid well treating composition includes first metal ions including Sb, Cu, and Bi complexed with a quaternary ammonium compound and second metal ions complexed with a quaternary ammonium compound. The complexed compounds may be prepared and introduced into the acid or the first metal ions may be introduced directly into the acid system.

Abstract: A precipitation control composition comprises an iron sequestering agent and a ketone-type compound as sulfide modifier. The precipitation control composition is useful to retard undesirable precipitation of iron and sulfur species from an acid solution of increasing pH. In combination with an acid solution, the precipitate control composition comprises an acidizing composition which is particularly useful in the acidizing of sour hydrocarbon wells. Also disclosed is the method of retarding undesirable precipitation of iron and sulfur species from an acid solution of increasing pH.

Abstract: An improvement when 1,3,5,7-tetranitro-1,3,5,7-tetraazacyclooctane is preed by nitrolysis of 1,3,5,7-tetraacyl-1,3,5,7-tetraazaceyloctane with a solution of nitric acid and nitrogen pentoxide or phosphorous pentoxide. This improved process herein before set forth produces 99% yield and purity of product.

Abstract: The present invention relates to drilling fluid additives, more particularly to superior drilling fluid thinners or polyfunctional drilling fluid conditioners, and methods of their preparation. The thinners comprise chelates and complexes prepared by reaction of sulfonitrohumic acid and sulfolignin with compounds of elements of Groups IVB and VIII of the periodic table, and especially titanium zirconium iron sulfolignin sulfonitrohumates, as well as mixture formed in the reaction. These chelates are stable, and are readily binded with clay and have a good heat resistance. The thinners of the present invention can remarkably reduce viscosity, yield point, gel strength and water loss of well-drilling fluids, and have a high salts and calcium resistivity, and can be widely used in extracting and exploiting petroleum, natural gas, geothermal fluids and underground water.

Abstract: 1-(n)-acetyl-3,5,7-trinitrocyclotetramethylenetetramine is prepared by nilysis of 1,3,5,7-tetracyl-1,3,5,7-tetraazacyclooctane with a solution of nitric acid and nitrogen pentoxide or phosphorous pentoxide.

Abstract: A water-based drilling fluid additive composition comprising a water soluble polyoxyalkylene compound selected from polyoxyalkylene glycols, monoalkylethers of polyoxyalkylene glycols, and mixtures thereof, which have a cloud point in the range from about 60.degree. F. to about 180.degree. F., in combination with a water dispersible particulate asphalt having an ASTM D-36 softening point of at least 290.degree. F., an ASTM D-5 penetration depth not exceeding about 10 mm, and a particulate size not exceeding more than about 10 percent retained on a 40 mesh U.S. screen.

Abstract: Fluoroalkyl derivatives which are novel compounds represented by the following general formula (I) or (II) of: ##STR1## orR.sub.1 --CH.dbd.CR.sub.2 (CF.sub.2).sub.n F (II)(wherein R.sub.1 stands for ##STR2## (where X stands for a hydrogen atom, a chlorine atom, a bromine atom, a fluorine atom, an iodine atom, a methyl group, an ethyl group, a methoxy group, an ethoxy group or a nitro group), an aroyloxy group, or an alkyl or alkoxycarbonyl group having 1 to 20 carbon atoms, and R.sub.2 stands for a hydrogen atom or a methyl group; and n stands for an integer of from 1 to 20.) A process for the preparation of the derivative is a process comprising reacting an olefin compound and a fluoroalkanesulfonyl chloride in the presence of a metal catalyst, or a process comprising an additional alkali treatment step which follows the aforementioned process.

Abstract: A method of preparing 2-bromo-4,6-dinitromesitylene having only small amounts of impurities, by first mixing fuming sulfuric acid with bromomesitylene, and then adding concentrated nitric acid.