Patents Examined by Kumar R Bhushan
  • Patent number: 11788936
    Abstract: The invention relates to a method for treating a liquid sample, which comprises disturbing iron and at least one organic compound of interest. The, the method comprises addition of a reagent comprising an ammonium salt, alkali metal salt or earth alkali metal salt of hexacyanoferrate to the sample. Iron in the sample is allowed to interact with the reagent and to form a reaction product, the reaction product of iron is separated from the sample, and the amount of the at least one compound of interest is determined from the sample. The invention relates also to use of salt of hexacyanoferrate.
    Type: Grant
    Filed: February 17, 2017
    Date of Patent: October 17, 2023
    Assignee: Kemira Oyj
    Inventor: Tapio Honkanen
  • Patent number: 11787992
    Abstract: This invention relates to the field of techniques for treating subterranean formations with gels during an oil or gas exploration or production operation, i.e., during drilling, completion, or hydraulic fracking processes. The invention relates in particular to a system making it possible to limit or even inhibit the phenomena known as loss of fluids (wager and/or gas) in an underground formation, particularly in a zone where the temperature is high. More particularly, the invention relates to a suspension (S) comprising: an aqueous phase containing salts; and within said aqueous phase, particles (p) based on associative polymers (P).
    Type: Grant
    Filed: March 3, 2020
    Date of Patent: October 17, 2023
    Assignee: ENERGY SOLUTIONS (US) LLC
    Inventors: Arnaud Cadix, David James Wilson
  • Patent number: 11787991
    Abstract: A disintegrable rubber seal includes a rubber composite, which contains a rubber matrix including a crosslinked rubber; and an energetic filler configured to generate heat upon activation to disintegrate the rubber matrix. The energetic filler contains a metal and a metal oxide. A weight ratio of the energetic filler to the rubber matrix is about 6:1 to about 1:1.
    Type: Grant
    Filed: April 11, 2022
    Date of Patent: October 17, 2023
    Assignee: BAKER HUGHES OILFIELD OPERATIONS LLC
    Inventors: Lei Zhao, Zhiyue Xu, Zhihui Zhang, Guijun Deng
  • Patent number: 11787909
    Abstract: Acrylamide-derived hydrogels and methods of fabrication thereof from an acrylic monomer, a crosslinking agent comprising an organosilicon compound, a polymerization initiator, a solvent and a polymerization accelerator, as well as their use in controlling circulation losses. The obtained hydrogels interact with the walls of the reservoir and exhibits an increase in viscosity, either at delayed times or in response to a given stimulus, such as changes in temperature, pressure, pH, salinity, using a simple and easily scalable methodology.
    Type: Grant
    Filed: December 23, 2019
    Date of Patent: October 17, 2023
    Assignees: YPF TECNOLOGIA S.A., UNIVERSIDAD DE BUENOS AIRES, CONSEJO NACIONAL DE INVESTIGACIONES CIENTIFICAS Y TECNICAS (CONICET).
    Inventors: Joana Elisa Tasque, Pablo Alejandro Raffo, Isabel Natalia Vega, Norma Beatriz D'Accorso, Darío Alberto Contrera
  • Patent number: 11781057
    Abstract: A composition for treating a formation includes a surfactant including an amphiphilic block copolymer having a first block and a second block and an acid. The amphiphilic block copolymer is a reaction product of a first monomer and a second monomer via a reversible addition-fragmentation chain transfer polymerization (RAFT) in a two-step reaction using a chain transfer agent (CTA) and a radical initiator. The surfactant favors adsorption onto a surface of the formation such that a temporary barrier is formed, thereby attenuating a reaction rate between the acid and the formation.
    Type: Grant
    Filed: October 29, 2021
    Date of Patent: October 10, 2023
    Assignee: SAUDI ARABIAN OIL COMPANY
    Inventors: Sivaprakash Shanmugam, Amy J. Cairns, Mohammed Sayed
  • Patent number: 11781062
    Abstract: The present invention relates to a bionics-based efficiently transported and packed proppant and preparation method thereof, comprising enhanced fracturing fluid and biomimetic dandelion proppant; the mass ratio of the enhanced fracturing fluid and the biomimetic dandelion is: 1-2:100-400; the 100 pbw of enhanced fracturing fluid includes 0.1-1 pbw of drag reducing agent, 0.01-0.1 pbw of cleanup additive, 0.2-0.8 pbw of clay stabilizer, 0.01-0.05 pbw of bactericide, 0.01-0.2 pbw of nanoparticle enhancer, and water; the biomimetic dandelion proppant consists of modified proppant and modified fiber, and the mass ratio between the modified proppant and the modified fiber is 99-99.9:0.1-1.
    Type: Grant
    Filed: June 21, 2022
    Date of Patent: October 10, 2023
    Assignee: Southwest Petroleum University
    Inventors: Pingli Liu, Jun Li, Jian Yang, Jianfa Wu, Shang Gao, Xingwu Guo, Jian Zou, Xitang Lan, Liping Zhang, Zhifeng Luo, Lan Ren, Changlong Liu, Juan Du, Xiang Chen, Nianyin Li, Peng Wang
  • Patent number: 11773311
    Abstract: A method for preparing PAM with the aluminum-based crosslinker is provided. The method includes diluting the PAM with deionized water; adding the crosslinker gradually while stirring at room temperature; sonicating in a water bath; adding HCl and KOH to adjust pH; and testing compatibility with salts.
    Type: Grant
    Filed: June 16, 2021
    Date of Patent: October 3, 2023
    Assignees: QATAR FOUNDATION FOR EDUCATION, SCIENCE AND COMMUNITY DEVELOPMENT, QATAR UNIVERSITY
    Inventors: Mohamed Shamlooh, Ibnelwaleed Ali Hussein, Mustafa Nasser, Musaab Magzoub, Saeed Salehi
  • Patent number: 11767596
    Abstract: Disclosed are molybdenum-containing complexes used in compositions and methods for inhibiting or reducing high temperature corrosion in petroleum refineries.
    Type: Grant
    Filed: July 29, 2020
    Date of Patent: September 26, 2023
    Assignee: ECOLAB USA INC.
    Inventors: Oussama Zenasni, Janelle Pennington, Ramon Colorado, Jr., Philip Andrew Thornthwaite
  • Patent number: 11767271
    Abstract: A porous material including a composite oxide body containing calcium oxide, iron oxide, and silica, and a plurality of inter-connecting microchannel structures is provided. A preparing method of porous material is further provided. With the inter-connecting microchannel structures of the porous material and the advantages of high porosity and large specific surface area, the porous material has a bright prospect in the fields of catalysts, filters, adsorption materials, and fuel carriers.
    Type: Grant
    Filed: September 21, 2020
    Date of Patent: September 26, 2023
    Assignee: INDUSTRIAL TECHNOLOGY RESEARCH INSTITUTE
    Inventors: Ming-Hui Chang, Sheng-Min Yu, Hsiu-Hsia Lee, Chien-Chung Hsu
  • Patent number: 11760916
    Abstract: A low dosage hydrate inhibitor blend comprising a cationic surfactant and a co-surfactant. The cationic surfactant has the structural formula: wherein: R1 is an alkyl group or alkenyl group having from 5 to 22 carbon atoms, R2 and R3 are alkyl groups having from 1 to 6 carbon atoms, R4 is a hydrogen atom or an alkyl group having from 1 to 6 carbon atoms, and X— is selected from the group of a carboxylate, an acrylate, a methacrylate, a halide, a phosphonate, a sulfate, a sulfonate, a hydroxide, a carbonate, or any combination thereof; and The co-surfactant is present in the inhibitor blend in an amount of no greater than about 10 percent by weight based on the total weight of the blend.
    Type: Grant
    Filed: January 31, 2019
    Date of Patent: September 19, 2023
    Assignee: Halliburton Energy Services, Inc.
    Inventors: Deepak S. Monteiro, Qiang Lan, Loan Vo, Philippe Prince
  • Patent number: 11753576
    Abstract: This invention relates to a method for inhibiting the agglomeration of gas hydrates, comprising the injection of an anti-agglomerant comprising a N,N-dialkyl-ammoniumalkyl fatty acid amide represented by the formula (I) wherein R1 is an alkyl or alkenyl group having from 7 to 21 carbon atoms, R2 and R3 are each independently an alkyl group containing 1 to 10 carbon atoms, or together form an optionally substituted ring having 5 to 10 ring atoms, wherein the ring may carry up to 3 substituents, R4 is hydrogen or an alkyl group having 1 to 6 carbon atoms, R5 is hydrogen or an optionally substituted hydrocarbyl group having 1 to 17 carbon atoms and A is an alkylene group having two or three carbon atoms, into a fluid comprising gas, water and oil under conditions prone to the formation of gas hydrates, wherein the N,N-dialkyl-ammoniumalkyl fatty acid amide represented by the formula (I) is produced by the condensation reaction of a fatty acid with an N,N-dialkylamino alkyl amine and subsequent neutralization
    Type: Grant
    Filed: May 28, 2019
    Date of Patent: September 12, 2023
    Assignee: Clariant International Ltd.
    Inventors: Scot Bodnar, Dan Smith, Felix Hoevelmann, Corinna Krüger, Matthias Krull, Jonathan James Wylde, Lisa Greaney Tejada
  • Patent number: 11753492
    Abstract: A corrosion inhibiting polymer is provided.
    Type: Grant
    Filed: May 20, 2022
    Date of Patent: September 12, 2023
    Assignee: Saudi Arabian Oil Company
    Inventors: Imran Ul-Haq, Abdullah Al-Malki, Manal Al-Eid, Hassan Ali Al-Ajwad
  • Patent number: 11753577
    Abstract: This invention relates to a method for inhibiting the agglomeration of gas hydrates, comprising the injection of an anti-agglomerant comprising a N,N-dialkyl-ammoniumalkyl fatty acid amide represented by the formula (I) wherein R1 is an alkyl or alkenyl group having from 7 to 21 carbon atoms, R2 and R3 are each independently an alkyl group containing 1 to 10 carbon atoms, or together form an optionally substituted ring having 5 to 10 ring atoms, wherein the ring may carry up to 3 substituents, R4 is hydrogen or an alkyl group having 1 to 6 carbon atoms, R5 is hydrogen or an optionally substituted hydrocarbyl group having 1 to 22 carbon atoms and A is an alkylene group having two or three carbon atoms, into a fluid comprising gas, water and oil under conditions prone to the formation of gas hydrates, wherein the N,N-dialkyl-ammoniumalkyl fatty acid amide represented by formula (I) is produced by the aminolysis of an ester of a fatty acid and a C1- to C4-alcohol with an N,N-dialkylamino alkyl amine and s
    Type: Grant
    Filed: May 28, 2019
    Date of Patent: September 12, 2023
    Assignee: Clariant International Ltd.
    Inventors: Scot Bodnar, Dan Smith, Felix Hoevelmann, Corinna Krüger, Matthias Krull, Jonathan James Wylde, Lisa Greaney Tejada
  • Patent number: 11753580
    Abstract: An inverse emulsion composition comprising: one or more hydrophobic liquids having a boiling point at least about 100° C.; up to about 38% by weight of one or more acrylamide-(co)polymers; one or more emulsifier surfactants; and one or more inverting surfactants; wherein, when the composition is inverted in an aqueous solution, it provides an inverted solution having a filter ratio using a 1.2 micron filter (FR1.2) of about 1.5 or less.
    Type: Grant
    Filed: April 17, 2019
    Date of Patent: September 12, 2023
    Assignee: KEMIRA OYJ
    Inventors: Logan Jackson, Thomas J. Lynch, Ronald Robinson, Frances Fournier, Hong Yang, Sukhjit Aujla, Do Hoon Kim, Dennis Arun Alexis
  • Patent number: 11753578
    Abstract: Methods for treating paraffins, iron sulfide, hydrogen sulfide, and/or bacteria in subterranean operations and operations involving the production and/or transportation of oil and gas are provided. In one or more embodiments, the methods include contacting a surface comprising at least one paraffin deposit and at least one iron sulfide deposit with a treatment fluid comprising a paraffin dissolver and acrolein; and allowing the treatment fluid to at least partially dissolve or degrade the paraffin deposit and the iron sulfide deposit.
    Type: Grant
    Filed: April 26, 2021
    Date of Patent: September 12, 2023
    Assignee: Halliburton Energy Services, Inc.
    Inventors: Yulia Mosina, Kiran Gawas, Chandrashekhar Khandekar
  • Patent number: 11746275
    Abstract: A wellbore fluid includes an aqueous fluid, a viscosifer, a stabilizer agent, and a lubricant. The aqueous fluid is an inhibitive divalent fluid. A method of preparing the divalent wellbore fluid includes are provided or formulated, methods produce the divalent wellbore fluids, and methods inject or circulate the inhibitive divalent wellbore fluids into a wellbore or borehole provided in a formation and/or into a reservoir of the formation.
    Type: Grant
    Filed: May 25, 2020
    Date of Patent: September 5, 2023
    Assignee: SCHLUMBERGER TECHNOLOGY CORPORATION
    Inventor: Justin Linscombe
  • Patent number: 11739167
    Abstract: Process for producing aqueous polyacrylamide solutions by polymerizing an aqueous solution comprising at least acrylamide thereby obtaining an aqueous polyacrylamide gel and dissolving said aqueous polyacrylamide gel in water, wherein the manufacturing steps are allocated to two different locations A and B and the process comprises the step of transporting an aqueous polyacrylamide gel from a location A to a location B. Modular, relocatable plant for manufacturing aqueous polyacrylamide solutions wherein the units of the plant are located at two different locations A and B.
    Type: Grant
    Filed: October 18, 2018
    Date of Patent: August 29, 2023
    Assignee: BASF SE
    Inventors: Faissal-Ali El-Toufaili, Joerg Unger
  • Patent number: 11739246
    Abstract: A method of recycling a direct emulsion wellbore fluid may include disrupting a direct emulsion comprising an aqueous external phase and an oleaginous internal phase, wherein the direct emulsion is stabilized by a surfactant composition; and separating the aqueous phase and the oleaginous phase.
    Type: Grant
    Filed: July 1, 2019
    Date of Patent: August 29, 2023
    Assignee: SCHLUMBERGER TECHNOLOGY CORPORATION
    Inventors: Hui Zhang, Jeremy Smith, Xia Wei, Weiqing Huang, Steven Philip Young
  • Patent number: 11732184
    Abstract: A sintered rod-shaped proppant and anti-flowback agent possesses high strength and high conductivity. The sintered rods comprise between about 0.2% by weight and about 4% by weight aluminum titanate. In some embodiments, the sintered rods are made by mixing bauxitic and non-bauxitic sources of alumina that may also contain several so-called impurities (such as TiO2), extruding the mixture, and sintering it. The starting material may optionally be milled to achieve better compacity and crush resistance in the final sintered rod. A fracturing fluid may comprise the sintered rods alone or in combination with a proppant, preferably a proppant of a different shape.
    Type: Grant
    Filed: June 7, 2019
    Date of Patent: August 22, 2023
    Assignee: U.S. Ceramics LLC
    Inventors: Jean Andre Alary, Thomas Parias
  • Patent number: 11725102
    Abstract: Process of providing polyacrylamides to a site-of-use comprising at least the steps of mixing a polyacrylamide powder at a manufacturing site with an aqueous liquid, thereby obtaining a homogeneous aqueous polyacrylamide concentrate, transporting said concentrate in a transport unit from the manufacturing site to the site-of-use, and removing the homogeneous aqueous concentrate from the transport unit at the site-of-use. Process of treating subterranean, oil and/or gas bearing formations by injecting an aqueous treatment fluid into at least one wellbore, wherein the aqueous treatment fluid is manufactured by mixing at least an aqueous base fluid with said homogeneous aqueous polyacrylamide concentrate at the site-of-use.
    Type: Grant
    Filed: October 17, 2019
    Date of Patent: August 15, 2023
    Assignee: BASF SE
    Inventors: Faissal-Ali El-Toufaili, Dennis Loesch, Anna-Corina Schmidt, Tobias Joachim Zimmermann, Markus Ostermayr, Jack F. Tinsley, Brent Busby, Daniel Barrera-Medrano