Patents Examined by Michael J. DiVerdi
  • Patent number: 6171993
    Abstract: The present invention provides an ethylene copolymer resin that has unique melt elastic properties not observed in ethylene copolymers heretofore known. Specifically, the ethylene copolymer resin of the present invention when in pelletized form has a reduction in melt elasticity (ER) of 10% or more to a final value of 1.0 or less upon rheometric low shear modification or solution dissolution. Moreover, the resin of the present invention when in reactor-made form exhibits at least a partially reversible increase of 10% or more in ER when pelletizing the same. An ethylene polymerization catalyst, a process of preparing the ethylene copolymer resin and a high-impact film are also provided herein.
    Type: Grant
    Filed: December 4, 1998
    Date of Patent: January 9, 2001
    Assignee: Equistar Chemicals, LP
    Inventors: Harilaos Mavridis, Mark K. Reinking, Ramesh N. Shroff, Joel A. Mutchler, Charles S. Holland, Keta M. Lindstrom, Kiran M. Gupte, Michael H. Treptau, Francis M. Mirabella
  • Patent number: 6156115
    Abstract: Multilayer interference pigment consisting of a central layer of a transparent or semitransparent material of low refractive index and alternating layers of a metal or of a material of high refractive index and of a material of low refractive index either side of the central layer, the material of low refractive index preferably being magnesium fluoride or acrylate and the metal preferably being aluminium or chromium.
    Type: Grant
    Filed: October 26, 1998
    Date of Patent: December 5, 2000
    Assignee: Merck Patent Gesellschaft mit beschrankter Haftung
    Inventors: Gerhard Pfaff, Gerd Bauer, Martin Friz, Matthias Kuntz, Christina Schank
  • Patent number: 6156690
    Abstract: The present invention provides a solid catalyst component for polymerization of olefins obtained by allowing a solid component and an alcohol to come in contact with each other, wherein the solid component is prepared by allowing a magnesium compound, a titanium compound and an electron donor compound to come in contact with each other, and also provides a catalyst for polymerization of olefins made of the solid catalyst component, an organic aluminum compound represented by the general formula R.sup.1.sub.p AlQ.sub.3-p and an organic silicon compound represented by the general formula R.sup.2.sub.q Si(OR.sup.3).sub.4-q. By using the catalysts in a polymerization of olefins, polyolefins excellent in stereoregularity can be obtained in high yield.
    Type: Grant
    Filed: February 25, 1999
    Date of Patent: December 5, 2000
    Assignee: Toho Titanium Co., Ltd.
    Inventor: Motoki Hosaka
  • Patent number: 6156117
    Abstract: A method of preparing a polymer structured pigment slurry which comprises providing an anionic, aqueous slurry including a plurality of solid mineral particles, adding a low molecular weight, cationic polymer in an amount of less than about 0.20% by weight to the slurry and then adding a small amount of an inorganic dispersant to the polymer treated pigment slurry. The Malvern median particle size of the mineral particles treated with the polycationic polymer is less than about 20% larger than the Malvern median particle size of the untreated mineral particles.
    Type: Grant
    Filed: September 1, 1998
    Date of Patent: December 5, 2000
    Assignee: J. M. Huber Corporation
    Inventors: Gary M. Freeman, Sung-Tsuen Liu
  • Patent number: 6150295
    Abstract: Novel catalyst systems which comprise pyridine-2-carboxaldimine nickel complexes can be used with methylaluminoxane in slurry polymerization processes to polymerize mono-1-olefins and, optionally a higher alpha-olefin comonomer, to produce low molecular weight polymers.
    Type: Grant
    Filed: March 30, 1998
    Date of Patent: November 21, 2000
    Assignee: Phillips Petroleum Company
    Inventor: Nancy W. Eilerts
  • Patent number: 6146455
    Abstract: The invention relates to a novel crystal modification (.delta.-modification) of C.I. Pigment Red 53:2 of the formula (1) ##STR1## having the following characteristic reflections in the X-ray powder diffraction pattern:______________________________________ 2.THETA. d relative intensity (in %) ______________________________________ 3.3 26.6 32 4.7 18.7 100 7.5 11.9 14 9.4 9.3 19 10.5 8.4 13 13.8 6.4 10 14.2 6.2 9 14.9 5.9 10 16.7 5.3 11 17.6 5.0 9 18.1 4.9 16 18.9 4.7 10 20.4 4.3 7 21.1 4.2 9 22.1 4.0 9 22.7 3.9 12 23.1 3.8 9 23.6 3.8 13 24.1 3.7 9 24.9 3.6 10 25.5 3.5 23 26.3 3.4 9 27.7 3.2 9 28.1 3.2 6 28.9 3.1 6 30.4 2.
    Type: Grant
    Filed: June 21, 1999
    Date of Patent: November 14, 2000
    Assignee: Clariant GmbH
    Inventors: Martin Ulrich Schmidt, Hans Joachim Metz
  • Patent number: 6147024
    Abstract: The present invention provides a catalyst for the polymerization of olefin that exhibits improved selectivity and broader molecular weight distribution in the polymer product. The catalyst is a conventional supported Ziegler-Natta catalyst in combination with a mixture of at least two electron donors, both having the general formula SiR.sub.m (OR').sub.4-m where R is selected from the group consisting of an alkyl group, a cycloalkyl group, an aryl group and a vinyl group; R' is an alkyl group; and m is 0-3, wherein when R is an alkyl group, R may be identical with R'; when m is 0, 1 or 2, the R' groups may be identical or different; and when m is 1, 2 or 3, the R groups may be identical or different. This catalyst produces polypropylene having xylene solubles of 1-7 to 5.1 wt % and a molecular weight distribution of about 10.
    Type: Grant
    Filed: July 12, 1999
    Date of Patent: November 14, 2000
    Assignee: Fina Technology, Inc
    Inventors: Edwar S. Shamshoum, David John Rauscher, Douglas Alan Burmaster
  • Patent number: 6139618
    Abstract: A fine yellow composite iron oxide hydroxide pigment of the present invention has an average major axial diameter of not less than 0.005 .mu.m and less than 0.1 .mu.m, which comprises:fine goethite particles as core particles, containing aluminum inside thereof in an amount of 0.05 to 50% by weight, calculated as Al, based on the weight of said core particles; anda composite oxide hydroxide of Fe and Al, coated on the surface of each core particle. Such fine yellow composite iron oxide hydroxide pigment are excellent in transparency and heat resistance.
    Type: Grant
    Filed: August 26, 1999
    Date of Patent: October 31, 2000
    Assignee: Toda Kogyo Corporation
    Inventors: Kazuyuki Hayashi, Mineko Ohsugi, Hiroshi Sumita, Hiroko Morii
  • Patent number: 6140264
    Abstract: The present invention provides a novel process for preparing a catalyst, preferably free of electron donor, useful in gas phase polymerization of olefins having a broad polydispersity.
    Type: Grant
    Filed: May 12, 1998
    Date of Patent: October 31, 2000
    Assignee: Nova Chemicals Ltd.
    Inventors: Mark Kelly, Dusan Jeremic, Victoria Ker, Charles Russell
  • Patent number: 6136748
    Abstract: A catalyst composition for the polymerization of olefins is provided, which comprises a) a catalyst comprising a metal atom complexed with a non-cycloalkadienyl anionic ligand, wherein the chemical hardness, .eta., and chemical potential, .mu., of said non-cycloalkadienyl anionic ligand calculated using the MOPAC (PM3) computer program satisfy the relationship: .eta.=3.0+0.75.mu..+-.0.2 eV; and b) an activating cocatalyst.
    Type: Grant
    Filed: June 12, 1998
    Date of Patent: October 24, 2000
    Assignee: Union Carbide Chemicals & Plastics Technology Corporation
    Inventor: Jack Allen Smith
  • Patent number: 6113682
    Abstract: Disclosed herein is a method for preparation of composite pigments for make-up cosmetics having improved skin-adhesion and spreadability, and excellent skin color-expression, and improved water resistance by silicon polymer coated on the surface of the complex particle of flaky silica and titanium dioxide coated thereon.
    Type: Grant
    Filed: November 6, 1998
    Date of Patent: September 5, 2000
    Assignees: Pacific Corporation, Bokwang Chemical Co. Ltd.
    Inventors: Dal Sik Shin, Dong Myong Kim, Sung Ho Lee, Ok Sob Lee, Kwang Soo Kim, Ju Hong Min
  • Patent number: 6106922
    Abstract: A web of material has a plurality of stems extending from at least one side of the web. The web includes a first layer of material having a first side and a second side and a second layer of material. The second layer of material has a first side which faces the first side of the first layer and a second side from which the plurality of stems extend. The first and second layers of material are joined together while they are both molten, before either layer has cooled. The first and second layers of material can be formed of thermoplastic material or melt processable polymeric material. A method of making a web of material includes selecting a first material for a first layer of material and selecting a second material for a second layer of material. The first and second layers of material are melt formed. Then, the first and second layers of material are joined while the layers are in the molten state to form a multiple layer sheet.
    Type: Grant
    Filed: October 3, 1997
    Date of Patent: August 22, 2000
    Assignee: 3M Innovative Company
    Inventors: John E. Cejka, Mark R. Dupre, Jeffrey O. Emslander, William H. Hartt, Robert D. Kampfer, Francis V. Loncar, Jr., Louis S. Moren, Diane L. Regnier, Jayshree Seth, Robert W. G. Shipman, Alan J. Sipinen, William C. Unruh, Dennis G. Welygan, Leigh E. Wood
  • Patent number: 6103658
    Abstract: Methods for preparing olefin polymers, and catalysts for preparing olefin polymers are disclosed. The polymers can be prepared by contacting the corresponding monomers with a Group 8-10 transition metal catalyst. The polymers are suitable for processing in conventional extrusion processes, and can be formed into high barrier sheets or films, or low molecular weight resins for use in synthetic waxes in wax coatings or as emulsions.
    Type: Grant
    Filed: October 22, 1998
    Date of Patent: August 15, 2000
    Assignee: Eastman Chemical Company
    Inventors: Peter Borden Mackenzie, Leslie Shane Moody, Christopher Moore Killian, James Allen Ponasik, Jr., Jason Patrick McDevitt, Gino Georges Lavoie
  • Patent number: 6099634
    Abstract: A titanyl sulfate solution or a titanium tetrachloride solution is neutralized with an alkali to form orthotitanic acid, to which hydrochloric acid is added such as to adjust the TiO.sub.2 concentration to 80-140 g/L and the HCl concentration to 90-150 g/L and a synthesis reaction is performed at a temperature of 25-60.degree. C. to produce titanium oxide particles in which needles aggregate and/or bind together to yield fan-shaped particles.
    Type: Grant
    Filed: February 27, 1998
    Date of Patent: August 8, 2000
    Assignee: Titan Kogyo Kabushiki Kaisha
    Inventors: Toshiaki Uenishi, Takanori Yamasaki
  • Patent number: 6093673
    Abstract: The invention relates to olefin polymerization using an organosilicon compound from the pyrazolyl family as an external adjuvant.
    Type: Grant
    Filed: September 27, 1999
    Date of Patent: July 25, 2000
    Assignee: Equistar Chemicals, LP
    Inventors: Douglas D. Klendworth, Gregory G. Hlatky
  • Patent number: 6086667
    Abstract: The invention relates, in particular, to pigments in the form of fine particles having enhanced stability with respect to ultraviolet solar radiation and particle radiation (electrons, protons), characterized in that the pigment are coated with a UV filter.Application in the production of paints for spacecrafts.
    Type: Grant
    Filed: February 5, 1999
    Date of Patent: July 11, 2000
    Assignee: Centre National d'Etudes Spatiales
    Inventors: Jean-Claude Guillaumon, Pascale Veronique Nabarra
  • Patent number: 6086669
    Abstract: Describes a free flowing particulate composition comprising, in combination, particulate amorphous precipitated silica, e.g., in the form of granules, hydrocarbon process oil, e.g., an aromatic process oil, and organic carboxylic acid having from 2 to 30 carbon atoms, e.g., stearic acid. The hydrocarbon process oil and organic carboxylic acid are sorbed on the silica and are present in amounts sufficient to measurably improve the dispersibility of the particulate amorphous precipitated silica into an elastomer as measured by percent white area. Optionally, an organosilane coupling agent may also be present in said composition. The free flowing particulate composition of the present invention is useful in reinforcing elastomers, e.g., rubbers used in vehicle tires and the soles of athletic foot wear.
    Type: Grant
    Filed: April 9, 1998
    Date of Patent: July 11, 2000
    Assignee: PPG Industries Ohio, Inc.
    Inventors: Shailesh D. Patkar, Harold E. Swift, William B. Scott
  • Patent number: 6077341
    Abstract: A silica-metal oxide particulate composite comprising silica agglomerates having voids formed by random stacking of scaly silica primary particles, and metal oxide particulates supported on the surfaces, and the inner surfaces in the voids, of the silica agglomerates.
    Type: Grant
    Filed: September 28, 1998
    Date of Patent: June 20, 2000
    Assignees: Asahi Glass Company, Ltd., Dohkai Chemical Industry Co., Ltd.
    Inventors: Kunihiko Terase, Masaharu Tanaka, Masaki Inoue, Eiichi Ono, Takayoshi Sasaki