Abstract: Method and apparatus for generating a gaseous test sample from a liquid sample and for transferring this test sample into a measuring cuvette of an atomic absorption spectrometer, in which an inert gas flow is directed through a sample vessel and into a measuring cuvette and, after the air has been displaced from the sample vessel, a reagent is added for generating a gaseous test sample, the test sample being carried into the measuring cuvette by the inert gas flow, wherein prior to the adding of the reagent, the flow rate of the inert gas flow is changed-over from a higher value to a lower value.

Abstract: A process for the obtention of fructose and fructose-rich syrups from xerophyte plants, particularly of the genus Amarillidaceae, such as Agave, comprises separately collecting the plant material consisting of the leaf portions and the core portions of the plant; admixing and washing with water said plant materials; chopping the washed plant material to form small pieces and recovering the juices released by the chopping operation; subjecting the chopped material to an extraction process with an aqueous liquor expressing the residual solid plant material to expel the enriched extractant therefrom; admixing the plant juice and extractant to obtain a mixed juice, settling and clarifying said mixed juice; acidulating the liquid phase of the process at a preselected moment in the sequence, such that the settled and clarified juice will be brought to a pH of from about 3 to about 4; allowing said acidulated liquid phase to stand for a period of time of from about 2 to 3 hours at a temperature of from about 85.

Abstract: An indicator device for use as a time indicator or a time-temperature indicator. A container is provided for housing a frangible capsule and a porous carrier. A vapor generating chemical is enclosed in the capsule. A mixture, including a second chemical, a pH change responsive indicator, and a gel forming agent are impregnated in the porous carrier. The pH of the vapor is different from the second chemical. A gel is formed from the mixture and provides uniform dispersion of the second chemical and the indicator throughout the porous carrier, as well as provides an impedance to the vapor as it moves through the porous carrier. The device is thus useful as an elapsed time indicator for certain temperature ranges as well as a time-temperature indicator for wider temperature ranges.

Abstract: A battery of horizontal coke ovens which are connected to two gas-collecting mains extending alongside the battery, one of said mains having means for cleaning dust-laden gases emitted from the coke ovens during charging with coal without the use of a flushing liquor and incorporating means for inhibiting the condensation of tar-based matter in the gas. The invention also relates to a method for operating such a battery of horizontal coke ovens.

Abstract: Filtering apparatus comprising a stationary housing and a rotary filter d having a peripheral filter screen with elongated filter openings extending parallel to an axis thereof and disposed within the housing to define a space between the filter drum and the housing. A sludgy liquid supply means is provided for supplying the sludgy liquid from the inside of the filter drum onto the inner surface of the filter screen. Solid component adheres to the filter screen and liquid component passes through the elongated filter openings of the filter screen into the space, said solid component on the filter screen being discharged from the interior of the filter drum through the housing in the form of aggregations of filtration residue and said liquid component being discharged from the space through an outlet opening as filtrate.

Abstract: A sifter, shaped to nest within a similarly shaped sifter, includes a tapered, hollow body, a handle connected to the body and extending outwardly therefrom, and an actuating mechanism extending along the outer surface of the body for driving an agitator positioned within the body.

Abstract: A fluid bed reaction apparatus for providing separate reaction sites for segregated reactions in processes such as coal gasification, wherein the respective gasification and subsequent combustion reactions are separated within a single stage reactor. The fluid bed reactor comprises a shell or housing for containing a shell side fluid bed and one or more vertical standing tubes located within the shell side which form the segregated tube reaction sides. The open lower ends of the standing tubes are displaced a short distance above a distributor plate which operates as the base of the shell side fluid bed column. A Venturi nozzle coaxially oriented below the standing tube mouth provides a high velocity fluid flow into the tube side of the reactor. Carbonaceous particles are first reacted as they travel down the shell side reaction chamber.

Abstract: A nozzle for the injection of urea-formaldehyde foam insulation in a building includes a two-stage foaming chamber in the foam chemical line which includes a plurality of jets for effecting bubbling of the foaming chemical and a bubble-sizing, apertured plate positioned downstream of the jets to further enhance the foaming action of the chamber. The nozzle further includes a body into which the foaming agent is coaxially delivered with respect to an axailly extending resin injector. The end of the resin injector extends from the body of the nozzle and a flexible injection hose is removably attached to the end of the nozzle such that the resin and foaming agent mix in the flexible hose.

Abstract: A generally cylindrical drum of heat stress and corrosion resistant construction, and having an opening therein, is rotatably mounted on a frame movable on rails along the coke side of the coke oven battery. A movable cover is fixed to the shell and covers the opening in the shell through which hot coke passes, when pushed from a coke oven chamber. A hood is fixed to the structure supporting a coke guide and has a movable portion that coacts with the rotatable shell when coke gravitates into the shell. The drum is rotatable to several positions. Means are included to quench the hot coke and to extract the particulate laden steam which is generated by the quenching operation. Additional means are included to remove noxious gases and particulate matter which emanates from the hot coke.

Abstract: Standard chemical laboratory glassware taper joints are retained by a threaded cap which, when screwed onto a male threaded part surrounding the female standard taper element with an O-ring surrounding the glassware part at the shoulder of the standard male taper holds the tapered surfaces together under resilient pressure to maintain tight closure at the taper interface. The O-ring, being compressed between the threaded retainer cap as the applied force, and the shoulder of the male taper element and the top of the male threaded part, as force receiving surfaces, provides a backup seal for the joint.

Abstract: Modular supports for instruments in a sterilization tray having a bottom and a cover each containing an array of apertures, and each support comprising an integrally molded rectangular instrument support base with downward projecting longitudinally split buttons to be inserted in the tray bottom apertures. Each instrument support base has upstanding members with a slot therebetween to receive and hold selected strips notched on their upper edges to cradle and support instruments for sterilization.A hold-down base has upwardly extending buttons to be inserted in the tray cover apertures including a wide slot to hold a downwardly extending block of resilient material for contacting instruments cradled in the strip notches. A bracket with a longitudinal fin inserted in the slot of an instrument support base fixed to the cover may also hold a resilient block to be used as a hold-down.

Abstract: A process of significantly increasing the capacity of and decreasing the pollution from an existing recovery boiler. The spent liquor is concentrated to 55 to 65 weight % solids and divided into two portions. One portion, containing 10 to 65 weight % of the solids is pyrolyzed, reducing the original fuel value of that portion by 25 to 70%. The remaining carboniferous char and inorganic material is carried to the recovery furnace. The other portion, containing the remainder of the solids, is carried directly to the furnace. The two portions may be combined prior to entering the furnace. In the latter case, the solids content of the combined portion should not be greater than 80 weight %.

Abstract: A chemical reactor with a first upstream fluid bed which primarily burns coal and a second downstream fluid bed which primarily desulfurizes.

Abstract: Stopper for an evacuated tube with an open end for collecting fluid such as blood samples. The stopper includes a plug adapted to be mounted in the opening in the tube so as to normally seal the tube. The plug permits access of a fluid sample needle therethrough into fluid communication with the reduced pressure interior of the tube so that fluid is collected in the tube from the needle. A check valve is on the plug to automatically open when the needle is inserted through the plug and subjected to the reduced pressure in the tube and to automatically close when subjected to a predetermined amount of pressure from within the tube such as that caused by backflow thereby preventing any fluid passing into the needle from the tube. The check valve includes a chamber which can be used as a reagent holder prior to the tube use.

Abstract: A catalytic converter for use in the exhaust line of an internal combustion engine wherein the catalytically active noble metal coating is deposited only on the rearward portion of the inert carrier, with respect to the direction of flow of the exhaust gases, said inert carrier being fully coated with a washcoat capable of absorbing catalyst poisons before application of the catalytically active noble metal coating.

Abstract: Impervious graphite tubes, rings and other chemical processing structures made from impervious graphite can be improved with respect to impact strength, safety, shock resistance, pressure capability and heat transfer capability by partially thermally degrading impervious graphite structures and coating the outer surfaces of the treated graphite structures with a layer of metal at an elevated temperature. Upon cooling, the structure is under compression and has the improved properties. Structures are claimed comprising metal armored, partially thermally degraded impervious graphite.

Abstract: The coke forms are produced in four stages, each constituted by a respective oven chamber, and in which the briquets are, respectively, preheated, dehydrated or dried, carbonized and cooled. Hot gas circuits are provided, in which the hot gas is composed substantially of burnt lean gas of the carbonization, and, for each stage, the hot gases are recirculated in a separate respective circuit. In the preheating, dehydrating and carbonization stages, the hot gases are heated and produced, or supplemented, in a respective separate combustion chamber with the recirculating hot gas in the carbonization stage being supplemented with cooled lean gas from this stage. The recirculating hot gases are dedusted separately in a dust settling chamber in which their flow velocity is reduced to approximately 0.2 to 2.0 m/sec, with the dust being collected.

Abstract: A filtering system in which a plurality of filter assemblies are supported in a spaced relation relative to a common header which communicates with each of the assemblies. Each filter assembly consists of a plurality of individual filter units each of which is formed by a perforated tube and a filter material extending around the tube. The fluid to be filtered is drawn through the filter units and the header for passage externally of the system.

Abstract: A unitary reactor system for the alkylation of benzene with olefins. The hydrocarbon reactants are sprayed horizontally from a plurality of openings in a number of vertical conduits which extend upward into a lower portion of the vessel. The conduits are surrounded by a vertical reaction tube having a circular catalyst inlet at its bottom end and which contains a mixing means located above the conduits. A hydrocarbon phase is retained in the upper portion of the vessel and an acid phase surrounds the reaction tube, with the interface of the two liquid phases being maintained above the open upper end of the reaction tube.

Abstract: Coke oven emission control system comprising a traveling hood for collecting the emissions arising from the quench car into which hot coke is pushed from the coke ovens. The hood has a U-shaped snorkel at the top of the hood extending longitudinally of the hood, which connects to an exhaust duct via a water trough. Within the hood are a number of nozzles which are adjusted to provide a fogging mist of atomized water particles at the time a coke oven is "pushed" which cools the emissions which rise from the quench car and thereby reduces their volume as they flow into the exhaust duct. In a modification, a venturi type scrubber in the snorkel tube serves to separate the particulates, and cool the gases as they flow to the exhaust duct. In a further modification, high pressure jets are mounted on the snorkel tube within the water trough to agitate the particulates and solids on the bottom of the water trough to assist in their removal by draining from the trough.