Abstract: A method of producing one of magnetite and ferrite nanoparticles comprising the step of mixing an iron containing metal chemical with a fatty acid.
Type:
Grant
Filed:
December 18, 2015
Date of Patent:
July 3, 2018
Assignee:
Board of Supervisors of Louisiana State University and Agricultural and Mechanical College
Abstract: There are disclosed activated carbon for use in an electric double-layer capacitor electrode, the carbon being capable of improving rate characteristics and float characteristics of the electric double-layer capacitor electrode, and a method for manufacturing the activated carbon. The method for manufacturing the activated carbon for use in the electric double-layer capacitor electrode, comprising the steps of: grinding a carbon raw material to adjust an average particle diameter of the carbon raw material into a range of 1 ?m to 15 ?m; mixing the carbon raw material whose average particle diameter has been adjusted, with an alkali activator to obtain a mixture; and an activation treatment comprising heating the mixture under an atmosphere of an inert gas and then under an atmosphere of a mixed gas of the inert gas and water vapor.
Abstract: A porous graphene, a graphene quantum dot and a green preparation method for the porous graphene and the graphene quantum dot. The method includes adding a starting material, graphite, into an acetic acid aqueous solution of chitosan, using chitosan as a stripping agent, obtaining the porous graphene by an ultrasonic treatment, centrifugation and precipitation, and obtaining the graphene quantum dot by dialyzing a supernatant from the centrifugation. The obtained porous graphene has fewer layers and a larger lateral dimension of sheet. The obtained graphene quantum dot has good dispersity and a uniform particle size distribution. The preparation method is simple to perform and a graphitization degree of the prepared porous graphene and graphene quantum dot is high. The obtained porous graphene can be used as a carrier for a reverse gene transfection, and the graphene quantum dot can be used for cell imaging.
Abstract: The present description relates to activated carbon and methods of making and using the same. The activated carbon is produced from textile and plastic waste materials. The activated carbon may further include graphitic fibers, carbon fibers, CNTs, metals and metal oxides dispersed in the activated carbon matrix. The activated carbon can be in the form of granular manufactures, powder manufactures, nanoparticles, sheets and any other form.
Abstract: A method of exfoliating graphite into graphene uses a sequence of flow and sonication on graphite suspensions. Graphite particles after intense mixing/grinding in a liquid are found to be altered, graphite having curled-up edges, which increases its sensitivity to ultrasound. Quadrupled graphene yield is achieved through introducing chaotic flow pretreatment.
Abstract: A method for conversion of carbon dioxide to carbon monoxide comprises: introducing a flow of a dehumidified gaseous source of carbon dioxide into a reaction vessel; and irradiating dried, solid carbonaceous material in the reaction vessel with microwave energy. Heating of the irradiated carbonaceous material drives an endothermic reaction of carbon dioxide and carbon that produces carbon monoxide. At least a portion of heat required to maintain a temperature within the reaction vessel is supplied by the microwave energy. Carbon monoxide thus produced is allowed to flow out of the reaction vessel.
Abstract: A method for preparing nanosized sulfide catalysts includes providing an aqueous solution having an organometallic complex, mixing the organometallic complex with a sulfiding agent, an emulsifier, and a hydrocarbon oil to prepare a water-in-oil nanoemulsion; subjecting the water-in-oil nanoemulsion to thermal decomposition and isolating a solid product from the liquid.
Type:
Grant
Filed:
April 10, 2017
Date of Patent:
June 12, 2018
Assignee:
KUWAIT INSTITUTE FOR SCIENTIFIC RESEARCH
Abstract: The present invention relates to a catalyst for synthesizing multi-wall carbon nanotubes and, more specifically, to a catalyst for synthesizing multi-wall carbon nanotubes, capable of easily disperse the synthesized multi-wall carbon nanotubes and significantly improving conductivity, to a method for producing the catalyst, and to multi-wall carbon nanotubes synthesized by the catalyst.
Abstract: The present disclosure is directed to methods for producing indium nanoparticles. The methods comprise dissolving indium chloride in a solution that includes a solvent and a surfactant, adding a reducing agent to the reaction mixture to form an agglomerate of In nanoparticles, and exposing the reaction mixture to a gas including oxygen to disperse the agglomerate into a plurality of individual indium nanoparticles.
Abstract: A process for producing a highly oriented graphitic film, consisting of (a) preparing a dispersion having graphene oxide (GO) or chemically functionalized graphene (CFG) dispersed in a liquid to form a liquid crystal phase (but not in a GO gel state); (b) depositing the dispersion onto a supporting substrate to form a layer of GO or CFG under an orientation-inducing stress; (c) removing the liquid to form a dried GO or CFG layer having an inter-plane spacing d002 of 0.4 nm to 1.2 nm; (d) thermally reducing the dried layer at a first temperature higher than 100° C. to produce a porous layer of reduced GO or CFG; (e) further heat-treating the porous layer at a second temperature to produce a porous graphitic film having an inter-plane spacing d002 less than 0.4 nm; and (f) compressing the porous graphitic film to produce the highly oriented graphitic film.
Abstract: The present invention includes an apparatus and a method of making a three dimensional graphite structure with a controlled porosity comprising: plating a metal layer on at least one of a nickel, an iron or a cobalt foam substrate; annealing the metal and the nickel, iron or cobalt foam into a porous metal-nickel, iron or cobalt catalyst, wherein the catalyst has a smooth and a porous surface; etching the smooth surface of the annealed porous metal-nickel, iron or cobalt catalyst; growing a carbonaceous layer on the porous surface of the annealed porous metal-nickel, iron or cobalt catalyst; and completely etching the porous metal-nickel, iron or cobalt catalyst to obtain the graphite layer.
Type:
Grant
Filed:
June 12, 2015
Date of Patent:
May 1, 2018
Assignee:
Board of Regents, The University of Texas System
Abstract: The present disclosure provides for methods for preparing ruthenium nanoparticles characterized by face centered cubic crystallographic structure characterized by small particle size, substantially homogeneous particle size distribution, substantially uniform spherical shape, and substantial high temperature stability. The present disclosure further provides for methods for preparing ruthenium nanoparticles characterized by face hexagonal close packed crystallographic structure characterized by small particle size, substantially homogeneous particle size distribution, substantially uniform spherical shape, and substantial high temperature stability.
Abstract: The present invention relates to a method for the production of cross-linked graphene and graphene oxide networks, which are selected from aerogels and xerogels with improved performance and characteristics thereof. The invention is also concerned with graphene and graphene oxide networks, which are selected from aerogels and xerogels produced by such processes and uses thereof.
Type:
Grant
Filed:
March 7, 2013
Date of Patent:
April 24, 2018
Assignees:
THE BIO NANO CENTRE LIMITED, KING ABDULAZIZ UNIVERSITY
Inventors:
Ainara Garcia Gallastegui, Milo Shaffer, Abdulrahman O. Alyoubi, Abdullah M Asiri
Abstract: A method of inhibiting an irregular aggregation of a nanosized powder includes (A) providing a nanosized ceramic powder to perform thereon a thermal analysis and thereby attain an endothermic peak temperature; (B) performing an impurity-removal heat treatment on the nanosized ceramic powder at a temperature higher than the endothermic peak temperature; (C) switching the nanosized ceramic powder from a temperature environment of the impurity-removal heat treatment to an environment of a temperature higher than a phase change temperature of the nanosized ceramic powder, followed by performing a calcination heat treatment on the nanosized ceramic powder in the environment of the temperature higher than the phase change temperature of the nanosized ceramic powder, wherein the nanosized ceramic powder skips the temperature environment between impurity-removal heat treatment and calcination heat treatment to shun generating a vermicular structure, avoid crystalline irregularity and abnormal growth, reduce particle
Type:
Grant
Filed:
May 10, 2016
Date of Patent:
April 17, 2018
Assignee:
NATIONAL CHUNG SHAN INSTITUTE OF SCIENCE AND TECHNOLOGY
Abstract: Methods of making carbon nanostructures are disclosed with including examples having heat treatment of a mixture having a fibrous organic reagent and a catalyst in the presence of a reducing agent for a time sufficient to produce a quantity of carbon nanostructures which may be nanotubes or other related structures. The reducing agent may be hydrogen, nitrogen or ammonia.
Abstract: Conjugated polymers composed of bi-pyridine units linked to 9,9-dialkyl fluorenyl-2,7-diyl units via imine linkages along the polymer backbone are provided. Also provided are semiconducting single-walled carbon nanotubes coated with the conjugated polymers and methods of sorting and separating s-SWCNTs from a sample comprising a mixture of s-SWCNTs and metallic single-walled carbon nanotubes using the conjugated polymers.
Type:
Grant
Filed:
October 12, 2016
Date of Patent:
April 10, 2018
Assignee:
Wisconsin Alumni Research Foundation
Inventors:
Padma Gopalan, Michael Scott Arnold, Catherine Kanimozhi Kansiusarulsamy, Gerald Joseph Brady, Matthew John Shea
Abstract: The present invention relates to a preparation method of graphene oxide based on anthracite. The method consists of the following steps. a. Preparation of ultra-clean anthracite powder; b. Pretreatment of ultra-clean anthracite powder; c. Preparation of anthracite oxide dispersion; d. Preparation of graphene oxide colloid solution; e. Preparation of graphene oxide. The invention also relates to a preparation method of graphene using graphene oxide obtained by method mentioned before. The method consists of the following steps. f. Preparation of graphene oxide-dispersant solution; g. Reduction of graphene oxide; h. Obtaining graphene by suction filtration and drying process. Based on the preparation of anthracite, the invention could reduce production costs effectively comparing to traditional preparation methods of graphene and graphene oxide, and make the reaction more fast and complete, facilitating the achievement of large scale industrial production.
Type:
Grant
Filed:
December 31, 2013
Date of Patent:
April 10, 2018
Assignee:
SHENZHEN CANTONNET ENERGY SERVICES CO., LTD.
Abstract: Methods of ex situ synthesis of graphene, graphene oxide, reduced graphene oxide, other graphene derivative structures and nanoparticles useful as polishing agents are disclosed. Compositions and methods for polishing, hardening, protecting, adding longevity to, and lubricating moving and stationary parts in devices and systems, including, but not limited to, engines, turbos, turbines, tracks, races, wheels, bearings, gear systems, armor, heat shields, and other physical and mechanical systems employing machined interacting hard surfaces through the use of nano-polishing agents formed in situ from lubricating compositions and, in some cases, ex situ and their various uses are also disclosed.
Abstract: Highly purified carbon nanotubes (CNT) having virtually no carbonaceous impurities (amorphous carbon) nor inorganic impurities (metal and metal oxides), and methods of their preparation are described. The purified CNT feature excellent electrical, mechanical, and thermal properties due to the near total absence of detrimental impurities. The CNT starting material is preferably in the form of wafer, film, or buckypaper for efficient diffusion of purifying media. The highly pure CNT are prepared by heat treating a CNT starting material in a specified amount of oxygen, then treating the CNT in a solution comprising water and acid, or further heat treating the CNT in an atmosphere comprising chlorine (Cl2). Extremely low levels of inorganic impurities may be achieved by treating sequentially with a treatment solution followed by chlorine. Removal of chloride from purified CNT may be achieved by further treating the chlorine-treated material in an atmosphere comprising hydrogen (H2).
Abstract: The present invention provides a method for producing a random-structure GIC in which exfoliated graphite having a low regularity of a graphene stacked state and a small number of stacked graphene layers can be easily obtained by exfoliation treatment. The method includes the steps of providing an alkali metal-GIC having an alkali metal intercalated between graphene layers and bringing a polar protic solvent into contact with the alkali metal-GIC in a non-oxidizing atmosphere.
Type:
Grant
Filed:
March 4, 2014
Date of Patent:
March 20, 2018
Assignees:
SEKISUI CHEMICAL CO., LTD., OITA UNIVERSITY