Patents Examined by Richard M Rump
  • Patent number: 9650254
    Abstract: A method of production of active carbon by pyrolysis of organic materials, includes pyrolysis unit, reforming unit, drying unit, purification unit, gas storage unit and high temperature regenerative combustion unit. Organic materials are subjected to pyrolysis reaction in pyrolysis unit to produce combustible gas, tar and char. Combustible gas is reformed through reforming unit then enters into the drying unit for drying organic materials. One part of the purified combustible gas is combusted in the direction of combustion channel in the high temperature regenerative combustion unit, and the combustion heat is produced. At the same time, another part of combustible gas exchanges heat in the direction of heat exchanger channel in the regenerative combustion unit. Then it is used as pyrolysis activation medium entering into the pyrolysis unit in process of pyrolysis and activation reaction. The char is activated by the combustible gas in the pyrolysis unit then forms activated carbon.
    Type: Grant
    Filed: April 1, 2011
    Date of Patent: May 16, 2017
    Assignee: DALIAN UNIVERSITY OF TECHNOLOGY
    Inventors: Aimin Li, Ningbo Gao, Liaoyuan Mao
  • Patent number: 9637387
    Abstract: A method for repairing a reduced graphene oxide, the method comprising the following steps: Dispersing the reduced graphene oxide into a solvent to obtain a graphene dispersion liquid, adding a first Lewis acid and a compound containing a methyl or methylene group to obtain the first mixture, reacting the first mixture in a microwave environment of which power is 300˜900 w for 0.5˜2 hours, refluxing for 3˜5 hours; separating, purifying and drying to obtain the first crude product; adding the first crude product into a second Lewis acid, adding an aromatic hydrocarbon repairing agent to obtain the second mixture, reacting the second mixture to obtain a molten solid, separating and purifying same to obtain the second crude product; mixing the second crude product, a metal powder catalyst and a third Lewis acid to obtain the third mixture, this method can repair reduced graphene oxide effectively.
    Type: Grant
    Filed: January 17, 2014
    Date of Patent: May 2, 2017
    Assignee: SHENZHEN CANTONNET ENERGY SERVICES CO., LTD
    Inventors: Mingdong Zhang, Linde Zhang
  • Patent number: 9630160
    Abstract: Disclosed are an apparatus and method for continuously producing carbon nanotubes. More specifically, disclosed are an apparatus for continuously producing carbon nanotubes including i) a reactor to synthesize carbon nanotubes, ii) a separator to separate a mixed gas from the carbon nanotubes transferred from the reactor, iii) a filter to remove all or part of one or more component gases from the separated mixed gas, and iv) a recirculation pipe to recirculate the filtered mixed gas to the reactor for carbon nanotubes. Advantageously, the apparatus and method for continuously producing carbon nanotubes enable rapid processing, exhibit superior productivity and excellent conversion rate of a carbon source, significantly reduce production costs, reduce energy consumption due to decrease in reactor size relative to capacity, and generate little or no waste gas and are thus environmentally friendly.
    Type: Grant
    Filed: January 10, 2014
    Date of Patent: April 25, 2017
    Assignee: LG Chem, Ltd.
    Inventors: Kwang-Hyun Chang, Jin-Do Kim, Kwang-Woo Yoon
  • Patent number: 9605343
    Abstract: Methods of forming carbon films, structures and devices including the carbon films, and systems for forming the carbon films are disclosed. A method includes depositing a metal carbide film using atomic layer deposition (ALD). Metal from the metal carbide film is removed from the metal carbide film to form a carbon film. Because the films are formed using ALD, the films can be relatively conformal and can have relatively uniform thickness over the surface of a substrate.
    Type: Grant
    Filed: November 13, 2013
    Date of Patent: March 28, 2017
    Assignee: ASM IP Holding B.V.
    Inventor: Jereld Lee Winkler
  • Patent number: 9598288
    Abstract: Method for preparing zinc-histidine self-assembly biomimetic complex activating reaction to convert carbon dioxide into bicarbonate ion, zinc-histidine self-assembly biomimetic complex by preparation method, and method for reducing carbon dioxide using zinc-histidine self-assembly biomimetic complex.
    Type: Grant
    Filed: August 11, 2014
    Date of Patent: March 21, 2017
    Assignee: INDUSTRY-ACADEMIC COOPERATION FOUNDATION YONSEI UNIVERSITY
    Inventors: Sang-Yup Lee, Min-Chul Kim, Yu-Kyoung Lee, Sunhyung Kim, Jinyoung Kwak, Youngjoon Lim, Sangwoo Park
  • Patent number: 9590246
    Abstract: Provided is a method for producing a lithium metal phosphate, and the method comprises initiating and allowing to proceed, in the presence of a polar solvent, a conversion reaction of a lithium ion (Li+) source such as lithium hydroxide, a divalent transition metal ion (M2+) source such as a divalent transition metal sulfate, and a phosphate ion (PO43?) source such as phosphoric acid into a lithium metal phosphate at 150° C. or higher. The conversion reaction is initiated and allowed to proceed by bringing solution A containing one of a lithium ion, a divalent transition metal ion, and a phosphate ion into contact with solution B containing the others of these ions at 150° C. or higher, or by adjusting the pH of solution C that has a pH of lower than 4 and contains a lithium ion, a divalent transition metal ion, and a phosphate ion to 4 or higher.
    Type: Grant
    Filed: September 2, 2011
    Date of Patent: March 7, 2017
    Assignee: SHOWA DENKO K.K.
    Inventors: Akihiko Shirakawa, Isao Kabe, Akihisa Tonegawa
  • Patent number: 9580319
    Abstract: A method of making unit cell sized oxide particulates comprising preparing a water solution of a metal or ceramic salt or methanol solution of Pt, adding a 2-fold molar excess of KO2 to the water solution and forming a reaction solution, spinning down the reaction solution, and creating oxide nanoparticles.
    Type: Grant
    Filed: October 29, 2014
    Date of Patent: February 28, 2017
    Assignee: The United States of America, as represented by the Secretary of the Navy
    Inventor: Thomas E. Sutto
  • Patent number: 9577149
    Abstract: The invention relates to a continuous-flow synthesis process for the preparation of high quality indium phosphide/zinc sulfide core/shell semiconduting nanocrystals in particular quantum dots (QD) conducted in a micro-reaction system comprising at least one mixing chamber connected to one reaction chamber.
    Type: Grant
    Filed: November 26, 2012
    Date of Patent: February 21, 2017
    Assignee: Quantum Materials Corporation
    Inventors: Huachang Lu, Werner Hoheisel, Leslaw Mleczko, Stephan Nowak
  • Patent number: 9573823
    Abstract: A closed loop combustion system for the combustion of fuels using a molten metal oxide bed.
    Type: Grant
    Filed: October 22, 2010
    Date of Patent: February 21, 2017
    Assignee: PHILLIPS 66 COMPANY
    Inventors: David C. LaMont, James Seaba, Edward G. Latimer, Alexandru Platon
  • Patent number: 9567225
    Abstract: Methods for forming holey carbon allotropes and graphene nanomeshes are provided by the various embodiments. The various embodiments may be applicable to a variety of carbon allotropes, such as graphene, graphene oxide, reduced graphene oxide, thermal exfoliated graphene, graphene nanoribbons, graphite, exfoliated graphite, expanded graphite, carbon nanotubes (e.g., single-walled carbon nanotubes, double-walled carbon nanotubes, few-walled carbon nanotubes, multi-walled carbon nanotubes, etc.), carbon nanofibers, carbon fibers, carbon black, amorphous carbon, fullerenes, etc. The methods may produce holey carbon allotropes without the use of solvents, catalysts, flammable gas, additional chemical agents, or electrolysis to produce the pores (e.g., holes, etc.) in the carbon allotropes. In an embodiment, a carbon allotrope may be heated at a working window temperature for a working period of time to create holes in the carbon allotrope.
    Type: Grant
    Filed: October 14, 2014
    Date of Patent: February 14, 2017
    Assignee: The United States of America as represented by the Administrator of the National Aeronautics and Space Administration
    Inventors: Yi Lin, Jae-Woo Kim, John W. Connell, Michael R. Funk, Caroline J. Campbell
  • Patent number: 9561489
    Abstract: A process for the preparation from a partially decomposed organic material like peat a granulated or pelletized sorption medium using low-temperature, thermal activation of the sorption medium to produce a high degree of granule or pellet hardness balanced against an efficacious level of ion-exchange and adsorption capacity, followed by chemical treatment of the thermally-activated sorption material via an acid solution and a salt solution to increase its ion-exchange and adsorption performance while minimizing the transfer of natural impurities found in the sorption medium to an aqueous solution is provided by this invention. The sorption medium of this invention can be used in a variety of aqueous solution treatment processes, such as wastewater treatment.
    Type: Grant
    Filed: March 14, 2014
    Date of Patent: February 7, 2017
    Assignees: American Peat Technology, LLC, Reagents of the University of Minnesota
    Inventors: Igor V. Kolomitsyn, Peggy Wallgren Jones, Douglas A. Green
  • Patent number: 9564653
    Abstract: A production method for producing a fuel cell, includes spinning a precursor consisting of a salt of at least one metal chosen from Sc, Y, La, Ce, Pr, Nd, Sm, Gd, Dy, Ho, Yb, Sr, Ba, Mn, Co, Mg, and Ga, a solvent, and a macromolecular polymer to produce nanofibers of the precursor containing the salt of the metal. The method further includes calcining the nanofibers of the precursor at a temperature ranging from 550° C. to 650° C. for 2 to 4 hours, and making a solid electrolyte material composed of the nanofibers obtained from the calcining. The resulting solid electrolyte material constitutes a part of a fuel cell.
    Type: Grant
    Filed: March 6, 2015
    Date of Patent: February 7, 2017
    Assignees: Toyota Jidosha Kabushiki Kaisha, Tsinghua University
    Inventors: Wei Pan, Bin Li, Yanyi Liu, Masashi Kawai
  • Patent number: 9561493
    Abstract: A template-free reverse micelle (RM) based method is used to synthesize pyrochlore nanostructures having photocatalytic activity. In one embodiment, the method includes separately mixing together a first acid stabilized aqueous solution including pyrochlore precursor A and a second acid stabilized aqueous solution including pyrochlore precursor B with an organic solution including a surfactant to form an oil-in-water emulsion. Next, equimolar solutions of the first and second acid stabilized oil-in-water emulsions are mixed together. Then, the mixture of the first and second acid stabilized oil-in-water emulsion is treated with a base to produce a precipitate including pyrochlore precursors A and B. After which, the precipitate is dried to remove volatiles. The precipitate is then calcined in the presence of oxygen to form a pyrochlore nanostructure, such as a bismuth titanate (Bi2Ti2O7) pyrochlore nanorod. The method of synthesizing the pyrochlore nanorod is template-free.
    Type: Grant
    Filed: November 24, 2014
    Date of Patent: February 7, 2017
    Assignee: Board of Regents of the Nevada System of Higher Education, on Behalf of the University of Nevada, Reno
    Inventors: Vaidyanathan Subramanian, Sankaran Murugesan
  • Patent number: 9564632
    Abstract: The invention generally relates to new materials based on C49 titanium disilicide (TiSi2) as a new, layered anode material, within which lithium ions can react with the Si-only layers. Stabilization by a coating a thin layer of oxide on the surface of TiSi2 significantly improves the charge and discharge performance.
    Type: Grant
    Filed: March 11, 2014
    Date of Patent: February 7, 2017
    Assignee: The Trustees of Boston College
    Inventors: Dunwei Wang, Sa Zhou
  • Patent number: 9549948
    Abstract: The invention relates to acid neutralizer technology, specifically involving a pure nano calcium powder and its preparation method, the nano calcium powder purity include the weight of the raw material: 3-7 parts pearl, 8-12 parts mother of pearl, 2-3 parts red coral, 20-30 parts oyster shell, clam shell 35-55 parts, Giant Clam 5-10 parts, pangolin shell 1-3 and 1-7 parts “ore” defined as limestone, cold water stone, and goose pipe rock. The preparation methods include cleaning, primary grinding, heat decomposition, rules grinding, nano grinding and mixing. Nano calcium pure powder of the present invention relates to the specific natural raw materials, and strict control of the nano calcium powder purity can provide human body absorption rates over 99%. The preparation method of the invention process is simple, convenient operation and control, stable quality, high yield, can be large-scale industrial production.
    Type: Grant
    Filed: March 7, 2015
    Date of Patent: January 24, 2017
    Inventor: Tieh-Chun Tang
  • Patent number: 9533281
    Abstract: Porositized/activated carbon processed from carbon or carbonaceous raw materials. The porositization process comprises: (1) loading porositizing agents; (2) thermal treatment; and (3) porous generation. In another embodiment, the porositization process comprises: (1) loading porositizing agents; and (2) thermal treatment wherein the carbon or carbonaceous materials undergo carbonization and self-activation during the thermal treatment. Activated carbon products that exhibit magnetic functionality.
    Type: Grant
    Filed: March 14, 2014
    Date of Patent: January 3, 2017
    Assignee: UNIVERSITY OF NORTH TEXAS
    Inventors: Sheldon Q. Shi, Changlei Xia
  • Patent number: 9537149
    Abstract: Disclosed is a method for manufacturing a lithium transition metal phosphate. The disclosed method for manufacturing a lithium transition metal phosphate comprises the steps of: injecting reaction materials containing lithium, a transition metal, and a phosphate, into a reactor, and mixing the raw materials at the molecular level in the reactor; and allowing the reaction materials to chemically react in the reactor so as to cause nucleation.
    Type: Grant
    Filed: April 20, 2011
    Date of Patent: January 3, 2017
    Assignee: SAMSUNG SDI CO., LTD.
    Inventors: Chun Joong Kim, Yun Jung Park, Dong Gyu Chang, Ji Ho Park, Woo Young Yang
  • Patent number: 9527742
    Abstract: Provided are a graphene sheet and a process of preparing the same. Particularly, a process of economically preparing a large-area graphene sheet having a desired thickness and a graphene sheet prepared by the process are provided.
    Type: Grant
    Filed: November 28, 2011
    Date of Patent: December 27, 2016
    Assignee: SAMSUNG ELECTRONICS CO., LTD.
    Inventors: Jae-young Choi, Hyeon-Jin Shin, Seon-mi Yoon
  • Patent number: 9528170
    Abstract: Disclosed is a method for producing a high-purity nanometer zinc oxide from steel plant smoke and dust by ammonia decarburization. The method comprises: leaching with an ammonia water-ammonium carbonate solution as a leaching agent, adding 0.3-0.5 kg of sodium fluorosilicate to per cubic meter of the leaching agent to obtain a leaching solution, then adding 50-60 kg slaked lime to per cubic meter of the leached solution to carry out decarburization with heating, and carrying out purification and impurity removal and then refining treatment. According to the method, the ammonia process is used for treating smoke and dust, and the existing ammonia process is adaptively improved, the leaching speed and the leaching rate of zinc in the smoke and dust are improved, and the zinc oxide with the purity of more than 99.
    Type: Grant
    Filed: September 25, 2012
    Date of Patent: December 27, 2016
    Assignee: SICHUAN XINHONG TECHNOLOGY CO., LTD
    Inventors: Shangquan Chen, Shichun Li, Xiaohong Li
  • Patent number: 9527739
    Abstract: There is provided a method for preparing a graphite film by using a single continuous heater, the method including: converting a polymer film to a carbonized film by introducing the polymer film into a first heater having a first temperature section; and converting the carbonized film to the graphite film by introducing the carbonized film into a second heater having a second temperature section where a temperature linearly increases.
    Type: Grant
    Filed: November 6, 2014
    Date of Patent: December 27, 2016
    Assignee: Guardnec Co., Ltd.
    Inventors: Ki-Ho Park, Won-Seok Choi, Woo-Jeong Kim