Patents Examined by Smita S Patel
  • Patent number: 12286541
    Abstract: This surface-treated sol-gel silica is characterized by containing sol-gel silica having an average particle size of 0.05 ?m or more and 2.0 ?m or less as measured by laser diffraction scattering and a surface treatment agent on the surface of the sol-gel silica. In a dispersion produced by dispersing 5 mass % of the sol-gel silica in ethanol by emitting ultrasonic waves at 40W for 10 minutes, the content of particles with particle sizes of 5 ?m or more is 10 ppm or less in a particle number size distribution obtained by a Coulter counter method.
    Type: Grant
    Filed: August 29, 2018
    Date of Patent: April 29, 2025
    Assignee: TOKUYAMA CORPORATION
    Inventors: Hiromasa Fujioka, Osamu Tanaka, Hiroaki Taira, Naoki Mikami, Toshiaki Ootani
  • Patent number: 12269911
    Abstract: Methods for making titanated silica supports, titanated chromium/silica pre-catalysts, and activated titanated chromium/silica catalysts are disclosed in which hydrogen peroxide and an alkali metal precursor are used during catalyst preparation. Resulting titanated chromium/silica pre-catalysts often contain silica, 0.1 to 5 wt. % chromium, 0.1 to 10 wt. % titanium, and less than or equal to 4 wt. % carbon, and further contain an alkali metal or zinc at a molar ratio of alkali metal:titanium or zinc:titanium from 0.02:1 to 3:1 and/or at an amount in a range from 0.01 to 2 mmol of alkali metal or zinc per gram of the silica. High melt index potential activated titanated chromium/silica catalysts can be used to polymerize olefins to produce, for example, ethylene based homopolymers and copolymers having HLMI values of greater than 30 g/10 min.
    Type: Grant
    Filed: April 25, 2023
    Date of Patent: April 8, 2025
    Assignee: Chevron Phillips Chemical Company LP
    Inventors: Anand Ramanathan, Max P. McDaniel, Jared Barr, Andrew Blagg, Christopher E. Wittner, Alan L. Solenberger, Zachary T. Kilpatrick, Micheal P. Stevens
  • Patent number: 12251670
    Abstract: The present invention relates to a method of producing a wood and textile fibre protection composition from tall oil pitch. The present invention also relates to a wood and textile fibre protection composition comprising tall oil pitch and use of the composition as a wood and textile fibre protection agent.
    Type: Grant
    Filed: April 25, 2019
    Date of Patent: March 18, 2025
    Assignee: BDC—TECHNOLOGY OY
    Inventor: Juha Koskela
  • Patent number: 12239960
    Abstract: Zeolites having surface modification with graphene oxide, reduced graphene oxide, or a sulfide have utility in removing pollutants from a water supply. Pollutants include Persistent Organic Pollutants (POPs) and heavy metals, such as lead. POPs are adsorbed onto zeolites having surface modification with graphene oxide and/or reduced graphene oxide. Heavy metals are adsorbed onto zeolites having surface modification with a sulfide.
    Type: Grant
    Filed: January 20, 2021
    Date of Patent: March 4, 2025
    Assignee: UWM Research Foundation, Inc.
    Inventors: Marcia Renata Quadros da Silva, David Garman, Mohsen Manjili, Yan Zhang
  • Patent number: 12215034
    Abstract: Silica particles having a d50 median particle size from 8 to 20 ?m, a sphericity factor (S80) of at least 0.9, a BET surface area from 0.1 to 8 m2/g, a total mercury intrusion pore volume from 0.35 to 0.8 cc/g, and a loss on ignition from 3 to 7 wt. %, are disclosed, as well as methods for making these silica particles, and dentifrice compositions containing the silica particles.
    Type: Grant
    Filed: June 12, 2019
    Date of Patent: February 4, 2025
    Assignee: Evonik Operations GmbH
    Inventors: Karl W. Gallis, William J. Hagar, Terry W. Nassivera, Lawrence Edward Dolan, Sanjeev Midha, Eva Schneiderman
  • Patent number: 12201968
    Abstract: An oxidation catalyst composite, methods, and systems for the treatment of exhaust gas emissions from a diesel engine are described. More particularly, an oxidation catalyst composite including a first washcoat layer comprising a Pt component and a Pd component, and a second washcoat layer including a refractory metal oxide support containing manganese, a zeolite, and a platinum component is described.
    Type: Grant
    Filed: March 21, 2022
    Date of Patent: January 21, 2025
    Assignee: BASF Mobile Emissions Catalysts LLC
    Inventors: Shiang Sung, Stanley A. Roth, Claudia Zabel, Susanne Stiebels, Andreas Sundermann, Olga Gerlach
  • Patent number: 12202739
    Abstract: Disclosed are a manganese-doped cobaltosic tetroxide, and a preparation method and application thereof, belonging to the field of battery materials. The preparation method of the manganese-doped cobaltosic tetroxide of the disclosure dopes a manganese element into cobalt carbonate with a specific process and matched with a composite surfactant, which can obtain manganese-doped cobaltosic tetroxide particle products with uniform particle size, dispersion and fineness through high-temperature sintering, a proportion of low-valence manganese in the doped manganese is high, and a crystal form of the products obtained by sintering is complete. The preparation method is simple in operation and can realize industrial large-scale production. The manganese-doped cobaltosic tetroxide prepared by the preparation method and the application thereof are also disclosed.
    Type: Grant
    Filed: September 22, 2022
    Date of Patent: January 21, 2025
    Assignees: Guangdong Brunp Recycling Technology Co., Ltd., Hunan Brunp Recycling Technology Co., Ltd.
    Inventors: Xinghua Lu, Changdong Li, Dingshan Ruan, Genghao Liu, Siyuan Zhou, Haihan Hu
  • Patent number: 12179182
    Abstract: A method for making a functional structural body includes a skeletal body of a porous structure composed of a zeolite-type compound, and at least one type of metallic nanoparticles present in the skeletal body, the skeletal body having channels connecting with each other, the metallic nanoparticles being present at least in the channels of the skeletal body.
    Type: Grant
    Filed: April 19, 2023
    Date of Patent: December 31, 2024
    Assignees: NATIONAL UNIVERSITY CORPORATION HOKKAIDO UNIVERSITY, FURUKAWA ELECTRIC CO., LTD.
    Inventors: Takao Masuda, Yuta Nakasaka, Takuya Yoshikawa, Sadahiro Kato, Masayuki Fukushima, Kojiro Inamori, Hiroko Takahashi, Yuichiro Banba, Kaori Sekine
  • Patent number: 12138621
    Abstract: The catalytic cracking catalyst contains a molecular sieve and an alumina substrate material. The alumina substrate material has a crystalline phase structure of ?-alumina. Based on the volume of pores with a diameter of 2-100 nm, the pore volume of the pores with a diameter of 2-5 nm accounts for 0-10%, the pore volume of the pores with a diameter of more than 5 nm and not more than 10 nm accounts for 10-25%, and the pore volume of the pores with a diameter of more than 10 nm and not more than 100 nm accounts for 65-90%.
    Type: Grant
    Filed: March 26, 2020
    Date of Patent: November 12, 2024
    Assignees: CHINA PETROLEUM & CHEMICAL CORPORATION, RESEARCH INSTITUTE OF PETROLEUM PROCESSING, SINOPEC
    Inventors: Jiexiao Zhang, Shanqing Yu, Mingde Xu, Jiasong Yan, Huiping Tian, Jiaxing Li, Min Yang
  • Patent number: 12139411
    Abstract: A method for forming hollow silica spheres by dissolving a hydrolyzable aryl silane in an aqueous solution of water and an acid to form a hydrolyzed silane solution, mixing the hydrolyzed silane solution with a hydroxide base to form a precipitate, and calcining the precipitate in a multi-stage calcination procedure that includes (a) heating to a first temperature of 180 to 240° C. with a first ramp rate of 3 to 10° C./min and holding the first temperature for 2 minutes to 2 hours, then (b) heating to a second temperature of 600 to 740° C. at a second ramp rate of 0.1 to 4° C./min, and holding the second temperature for 2 to 24 hours.
    Type: Grant
    Filed: May 10, 2024
    Date of Patent: November 12, 2024
    Assignee: Imam Abdulrahman Bin Faisal University
    Inventors: Ayhan Bozkurt, Seyda Tugba Gunday Anil, Munirah Abdullah Almessiere, Sultan Akhtar
  • Patent number: 12134086
    Abstract: An oxidation catalyst composite, methods, and systems for the treatment of exhaust gas emissions from a diesel engine are described. More particularly, an oxidation catalyst composite including a first washcoat layer comprising a Pt component and a Pd component, and a second washcoat layer including a refractory metal oxide support containing manganese, a zeolite, and a platinum component is described.
    Type: Grant
    Filed: March 21, 2022
    Date of Patent: November 5, 2024
    Assignee: BASF Mobile Emissions Catalysts LLC
    Inventors: Shiang Sung, Stanley A. Roth, Claudia Zabel, Susanne Stiebels, Andreas Sundermann, Olga Gerlach
  • Patent number: 12134563
    Abstract: A porous silica particle has disintegration properties. The porous silica particle has an average particle diameter of 0.5 to 50 ?m, a pore volume of 0.5 to 5.0 cm3/g, a mode of a pore diameter of 2 to 50 nm, a shape factor of 0.8 to 1.0, an average compression strength of 0.1 to less than 1.0 kgf/mm2, a sodium content of 10 ppm or less, and a network structure.
    Type: Grant
    Filed: December 27, 2018
    Date of Patent: November 5, 2024
    Assignee: JGC CATALYSTS AND CHEMICALS LTD.
    Inventors: Miki Egami, Takuji Miyamoto, Ryo Muraguchi
  • Patent number: 12129179
    Abstract: A method for catalytic synthesis of ammonia under normal pressures, including: performing a reaction of hydrogen and nitrogen to synthesize ammonia under normal pressures by taking a liquid alloy as a catalyst in a reactor, where the reactor contains a molten salt, the density of the molten salt is smaller than that of the liquid alloy, and the molten salt is used for providing a reaction interface and isolating the liquid alloy from being introduced impurities. The first metal reacts with the nitrogen to produce the metal nitride, and the molten salt provides a new reaction interface for the metal nitride to react with the hydrogen to synthesize ammonia, so that ammonia is produced continuously. In addition, the molten salt prevents the liquid alloy from contacting with the oxygen and the water vapor, which prevents the liquid alloy from being oxidized, thus prolonging its service life.
    Type: Grant
    Filed: November 19, 2021
    Date of Patent: October 29, 2024
    Assignee: ShanghaiTech University
    Inventors: Xiaofei Guan, Zujian Tang
  • Patent number: 12122967
    Abstract: Materials, methods to prepare, and methods of use for producing an H2 rich synthesis gas stream from coal free of nitrogen is described. One embodiment of the method comprises. The method includes an oxygen carrier at least partially reduced using a fuel in a reactor forming a reduced metal oxide comprised of first series—3d block-transition metals or mixture thereof. The reduced metal oxide is reacted with the solid fuel/steam to produce H2 and CO2/CO in the reactor; and the reduced metal oxide is added separately or simultaneously with a solid fuel while not impregnating the solid fuel with the reduced metal oxide.
    Type: Grant
    Filed: October 19, 2020
    Date of Patent: October 22, 2024
    Assignee: U.S. Department of Energy
    Inventor: Ranjani Siriwardane
  • Patent number: 12077627
    Abstract: Methods for making titanated silica supports, titanated chromium/silica pre-catalysts, and activated titanated chromium/silica catalysts are disclosed in which hydrogen peroxide and an alkali metal precursor are used during catalyst preparation. Resulting titanated chromium/silica pre-catalysts often contain silica, 0.1 to 5 wt. % chromium, 0.1 to 10 wt. % titanium, and less than or equal to 4 wt. % carbon, and further contain a bound alkali metal or zinc at a molar ratio of alkali metal:titanium or zinc:titanium from 0.02:1 to 3:1 and/or at an amount in a range from 0.01 to 2 mmol of alkali metal or zinc per gram of the silica. High melt index potential activated titanated chromium/silica catalysts can be used to polymerize olefins to produce, for example, ethylene based homopolymers and copolymers having HLMI values of greater than 30 g/10 min.
    Type: Grant
    Filed: October 24, 2023
    Date of Patent: September 3, 2024
    Assignee: Chevron Phillips Chemical Company LP
    Inventors: Anand Ramanathan, Max P. McDaniel, Jared Barr, Andrew T. Blagg, Christopher E. Wittner, Alan L Solenberger, Zachary T. Kilpatrick, Micheal P. Stevens
  • Patent number: 12077449
    Abstract: Provided is an alumina-based composite oxide having a large initial specific surface area and a small initial mean pore size, with excellent heat resistance of the specific surface area and pore volume; and a production method therefor. Specifically, provided is an alumina-based composite oxide wherein the initial crystallite diameter is 10 nm or less and the initial specific surface area is 80 m2/ml or more; after calcination at 1200° C. for 3 hours in air, the specific surface area is 10 m2/ml or more; the initial mean pore size is 10 nm or more and 50 nm or less; and after calcination at 1200° C. for 3 hours in air, the pore volume retention rate is 10% or more, which is determined by (P1/P0)×100 wherein P0 represents an initial pore volume (ml/g), and P1 represents a pore volume (ml/g) after calcination at 1200° C. for 3 hours in air.
    Type: Grant
    Filed: October 8, 2021
    Date of Patent: September 3, 2024
    Assignee: DAIICHI KIGENSO KAGAKU KOGYO CO., LTD.
    Inventors: Hiroyuki Hayashida, Yoshikazu Hirose
  • Patent number: 12060277
    Abstract: A reactor 200 according to the present invention includes a heater storage section serving as a space section capable of accommodating a carbon heater for initial heating of silicon core wires. A carbon heater 13 is loaded in a deposition reaction space 20 in the reactor 200 only when necessary for initial heating of silicon core wires 12. After initial heating of the silicon core wires 12 is finished, the carbon heater 13 is unloaded from the deposition reaction space to the heater storage section 30. As a result, the carbon heater 13 is not unduly damaged in the reactor any longer and its deterioration is reduced. In addition, because of reduction in reaction with hydrogen gas in the reactor, the generation of methane is reduced, and thus carbon contamination of polycrystalline silicon is reduced.
    Type: Grant
    Filed: April 15, 2020
    Date of Patent: August 13, 2024
    Assignee: Shin-Etsu Chemical Co., Ltd.
    Inventors: Yasushi Kurosawa, Shigeyoshi Netsu, Naruhiro Hoshino
  • Patent number: 12043690
    Abstract: A method comprising contacting a silica support with a titanium-containing solution to form a titanated silica support, wherein the titanium-containing solution comprises a solvent; a ligand comprising a glycol, a carboxylate, a peroxide, or a combination thereof, and a titanium compound having the formula Ti(acac)2(OR)2, wherein “acac” is acetylacetonate and wherein each R independently is ethyl, isopropyl, n-propyl, isobutyl, or n-butyl.
    Type: Grant
    Filed: January 19, 2022
    Date of Patent: July 23, 2024
    Assignee: Chevron Phillips Chemical Company LP
    Inventors: Max P. McDaniel, Kathy S. Clear, William C. Ellis, Deloris R. Gagan
  • Patent number: 12037252
    Abstract: Silica particles having a BET surface area from 0.1 to 7 m2/g, a pack density from 35 to 55 lb/ft3, an Einlehner abrasion value from 8 to 25 mg lost/100,000 revolutions, a total mercury intrusion pore volume from 0.7 to 1.2 cc/g, and a stannous compatibility from 70 to 99%, are disclosed, as well as methods for making these silica particles.
    Type: Grant
    Filed: December 1, 2017
    Date of Patent: July 16, 2024
    Assignee: Evonik Operations GmbH
    Inventors: Karl W. Gallis, William J. Hagar, Terry W. Nassivera, Lawrence Edward Dolan, Sanjeev Midha, Eva Schneiderman
  • Patent number: 12037253
    Abstract: Provided is a method of preparing a metal oxide-silica composite aerogel and a metal oxide-silica composite aerogel having an excellent weight reduction property prepared by the method. The method comprises adding an acid catalyst to a first water glass solution to prepare an acidic water glass solution (step 1); adding a metal ion solution to the acidic water glass solution to prepare a precursor solution (step 2); and adding a second water glass solution to the precursor solution and performing a gelation reaction (step 3).
    Type: Grant
    Filed: January 26, 2022
    Date of Patent: July 16, 2024
    Assignee: LG Chem, Ltd.
    Inventors: Jong Hun Kim, Je Kyun Lee