Abstract: The present disclosure provides a process of clean production of electronic grade high-purity copper oxide. The process includes (1) preparing a carbon-ammonia system solution with a certain ratio of CO2, NH3 and H2O; (2) dissolving copper under a slightly negative pressure and at a system temperature less than or equal to 60° C.; the reaction ends until the concentration of copper in the carbon-ammonia system solution reaches 80 to 140 g/L; (3) adding sodium polyacrylate; the reaction solution is heated to 60-80° C. under a reduced pressure for deamination; (4) disposing basic copper carbonate to separate the solid from the liquid by a centrifuge to give an filter cake and copper-containing clear solution; (5) calcining the filter cake at 250-600° C.

Abstract: Provided is a method for preparing molybdenum oxide nanoparticles, including (a) preparing a precursor solution by dissolving a molybdenum salt in a first polar solvent, (b) generating an aerosol by applying ultrasonic waves to the precursor solution, and spraying the aerosol to a pre-heated reactor using a carrier gas, (c) obtaining molybdenum oxide micron-sized particles by pyrolyzing the aerosol, and (d) obtaining molybdenum oxide nanoparticles by dispersing the molybdenum oxide micron-sized particles in a second polar solvent and performing a solvothermal reduction reaction.

Abstract: The present invention relates to a method of forming a particulate porous metal oxide or metalloid oxide, as well as uses of the obtained a particulate porous metal oxide or metalloid oxide. A solution of a non-ionic surfactant and either an ionic surfactant or an inorganic salt is formed in an acidic aqueous solution. A metal oxide precursor or a metalloid oxide precursor is added. The formed reaction mixture is heated under reflux upon agitation for a period sufficient to obtain a particulate porous metal oxide or metalloid oxide.

Abstract: The present invention is directed to a process for obtaining a nanostructured titania catalyst with stabilized acidity through the sol-gel method and hydrotreatment and thermal activation; constituted basically by titanium oxide, specially characterized of being as nanostructures in its evolution nanocrystals-nanotubes-nanocrystals, that gives special physicochemical properties such as high specific area, purity and phases stability, acidity stability and different types of active acid sites, such as a capacity to disperse and stabilize metallic particles with high activity mainly in catalytic processes.

Abstract: The present invention relates to formulations comprising at least one hydridosilane of the generic formula SinH2n+2 with n=3-6 and at least one hydridosilane oligomer, to processes for preparation thereof and to the use thereof.

Abstract: The present subject matter relates generally to a method for the removal of oxygen from hydrogen using a manganese, iron, nickel or cobalt based adsorbent. More specifically, the present subject matter relates to the methods for the removal of oxygen from hydrogen using a manganese based adsorbent without the generation of water or other oxides.

Abstract: Processes for producing polycrystalline silicon by thermal decomposition of silane are disclosed. The processes generally involve thermal decomposition of silane in a fluidized bed reactor operated at reaction conditions that result in a high rate of productivity relative to conventional production processes.

Abstract: Processes for producing polycrystalline silicon by thermal decomposition of silane are disclosed. The processes generally involve thermal decomposition of silane in a fluidized bed reactor operated at reaction conditions that result in a high rate of productivity relative to conventional production processes.

Abstract: We provide a process for regenerating a used acidic ionic liquid catalyst which has been deactivated by conjunct polymers in a reactor, by removing at least 57 wt % of the conjunct polymers originally present in the used acidic ionic liquid catalyst in a separate regeneration reactor, so as to increase the activity of the catalyst. We also provide a regenerated used acidic ionic liquid catalyst having increased activity.

Abstract: The present invention relates to formulations comprising at least one hydridosilane of the generic formula SinH2n+2 with n=7-10 and at least one hydridosilane oligomer, to processes for preparation thereof and to the use thereof.

Abstract: A method of producing silica nanoparticles using sand can include mixing white sand with H2SO4 and H3PO4 to form a mixture. The mixture can be stirred in an ice bath. KMnO4 can then be added to the mixture while maintaining the temperature of the mixture below 5° C. The resulting suspension can be reacted for about 3 hours to about 5 hours on ice. The suspension is stirred in an ice bath and then maintained in a water bath at a temperature of 40° C. for about 90 minutes to about 120 minutes. Afterwards, the temperature is adjusted to and maintained at 98° C. for another period of about 90 minutes to about 120 minutes while adding water. H2O2 can be added to the suspension after adding the water to produce a reaction product with a precipitate. The reaction product can then be dried and calcinated to provide the silica nanoparticles.

Abstract: Silica particles calcined in a calcination step are supplied in a swirling flow generated by a gas introduced in a disintegration container and disintegrated therein, whereby the silica particles can be easily disintegrated and there can be obtained disintegrated silica particles having both low hygroscopicity and high dispersibility in resin. In addition, the introduction of dehumidified air (gas) during the disintegration reduces hygroscopicity and greatly improves dispersibility in resin. Furthermore, performing heating treatment (calcination) again after the disintegration causes the surface modification of the disintegrated silica particles, greatly improving hygroscopicity and dispersibility in resin. The resin composition obtained in this manner including silica particles provides good injectability and filterability when used for an underfill material for semiconductors and an in-plane spacer or sealing spacer of liquid crystal displays.

Abstract: The invention relates to a process for preparing a catalyst comprising a mesoporized zeolite, comprising the steps of: preparation of a protonic mesoporized zeolite, which contains at least one network of micropores and at least one network of mesopores, and treatment in a gas or liquid phase containing ammonia or ammonium ions. The invention also related to the obtained catalyst and the use of this catalyst in hydroconversion processes.

Abstract: An oxidation catalyst composite, methods, and systems for the treatment of exhaust gas emissions from a diesel engine are described. More particularly, an oxidation catalyst composite including a first washcoat layer comprising a Pt component and a Pd component, and a second washcoat layer including a refractory metal oxide support containing manganese, a zeolite, and a platinum component is described.

Abstract: Provided is an adsorbent for carbon dioxide, including: a graphene oxide layer having an interconnected network structure; and carbon nitride formed on the graphene oxide layer.

Abstract: A fuel reforming catalyst which contains an inorganic porous support, a catalytically active species, and catalyst particles including CeO2 and ZrO2 and in which the concentration of ZrO2 in the catalyst particles is higher in the vicinity of the particle surface than in the particle interior and the concentration of CeO2 in the catalyst particles is equal in the particle interior and in the vicinity of the particle surface is proposed for the purpose of providing a new fuel reforming catalyst which can effectively lower the concentration of the hydrocarbon of C2 or more in the gas which has passed through a steam reforming reaction.

Abstract: A method for producing a barium titanate-based powder that includes mixing a titanium compound and a barium compound together with water and chlorine to prepare a slurry, and temporarily firing the mixture of the titanium compound and the barium compound which is contained in the slurry to provide a barium titanate-based powder. The chlorine in the slurry is in the form of chlorine ions in a ratio of 230 to 1100 wt ppm based on the amount of the barium titanate-based powder to be synthesized.

Abstract: Process for production of silica having variable thickening wherein a) a product stream I comprising at least a vaporous, hydrolysable and/or oxidizable silicon compound, b) a product stream II comprising oxygen and c) a product stream III comprising at least a combustible gas are made to react, characterized in that d) a feed port in a pipepiece A, said pipepiece A comprising one or more static mixing elements, is used to import product stream I into product stream II, or vice versa and thereby create product stream IV, then e) a feed port in a pipepiece B, said pipepiece B comprising one or more static mixing elements, is used to import product stream III in product stream IV and thereby create product stream V, f) product stream V leaving pipepiece B is imported into a reaction chamber, ignited therein and reacted in a flame, and g) the resultant solid material is separated off.

Abstract: A reactor for preparing granular polysilicon by deposition of polycrystalline silicon on silicon seed particles has a reaction vessel, an inner reactor tube for a fluidized bed comprising granular polysilicon and a reactor bottom within the reactor vessel, a heating device for heating the fluidized bed in the inner reactor tube, at least one bottom gas nozzle for introduction of fluidizing gas and at least one reaction gas nozzle for introduction of reaction gas, a feed device to introduce silicon seed particles, an offtake line for granular polysilicon, and a device for discharging reactor offgas from the reactor vessel, and has a cylindrical component which has openings on its cylindrical surface, with at least 5% and not more than 95% of the cylindrical surface being open located between the inner reactor tube and the heating device.

Abstract: Methods for separating halosilanes that involve use of a distillation column having a partition that divides the column into portions for producing three product fractions are disclosed. Methods and systems for producing silane by disproportionation of halosilanes that use such columns and methods for producing polycrystalline silicon are also disclosed.