Patents Examined by William R. Dixon, Jr.
  • Patent number: 5139901
    Abstract: The invention provides a lithium secondary battery using hydric boron carbonitride which is a layered compound represented by BC.sub.x N.sub.y H.sub.z, where 0.5.ltoreq.x.ltoreq.12, 0.7.ltoreq.y.ltoreq.1.5, and 0.01.ltoreq.z.ltoreq.3, as the active material of the negative electrode. This compound is obtained by a CVD process. The electrolyte is a solution of a lithium salt in an organic solvent. The material of the positive electrode is an oxide such as MnO.sub.2 or V.sub.2 O.sub.5, a sulfide such as MoS.sub.2 or TiS.sub.2 or a conductive organic polymer such as polyaniline. In this secondary battery Li is smoothly intercalated in and released from the hydric boron carbonitride of the negative electrode, and the energy density with respect to the active material of the negative electrode is sufficiently high. This battery bears a fairly large number of charge-discharge cycles.
    Type: Grant
    Filed: November 26, 1990
    Date of Patent: August 18, 1992
    Assignee: Central Glass Company, Limited
    Inventors: Masayuki Kawaguchi, Koji Nozaki, Yasushi Kita
  • Patent number: 5139574
    Abstract: Disclosed is an ink composition which comprises an aqueous liquid vehicle, a water-soluble dye, and particles of a block copolymer of the formula ABA, wherein A represents a hydrophilic segment and B represents a hydrophobic segment, said ABA particles having an average diameter of about 300 Angstroms or less. The ink is particularly suitable for use in ink jet printing systems, especially thermal ink jet printing systems.
    Type: Grant
    Filed: January 28, 1991
    Date of Patent: August 18, 1992
    Assignee: Xerox Corporation
    Inventors: Francoise M. Winnik, Marcel P. Breton, William Riske
  • Patent number: 5139978
    Abstract: The method of the present invention is useful in preparing an improved alpha alumina-based ceramic. The improvement consists of the addition of a precursor of an alpha phase nucleating to transition alumina. The method is particularly useful in preparing alpha alumina-based abrasive grain.
    Type: Grant
    Filed: July 16, 1990
    Date of Patent: August 18, 1992
    Assignee: Minnesota Mining and Manufacturing Company
    Inventor: Thomas E. Wood
  • Patent number: 5139977
    Abstract: There is disclosed a method for making a self-supporting ceramic composite article having a porous core bearing a dense surface layer formed integrally with said core. A preform comprises a filler material and parent metal distributed therethrough, wherein the volume percent of parent metal is sufficient to form a volume of oxidation reaction product exceeding the total volume available within said preform. The parent metal is melted and reacted with an oxidant to form an oxidation reaction product filling the spatial volume and leaving voids. The reaction is continued to further transport molten parent metal through the oxidation reaction product to at least one surface of the preform to form oxidation reaction product on said surface substantially free of voids thereby forming a relatively dense surface layer.
    Type: Grant
    Filed: May 13, 1991
    Date of Patent: August 18, 1992
    Assignee: Lanxide Technology Company, LP
    Inventor: Ratnesh K. Dwivedi
  • Patent number: 5139537
    Abstract: A titanium nitride coating is applied over the cubic boron nitride layer of conventional CBN tools by the process of arc physical-vapor-deposition at temperatures below the tempering temperature of the core metal. The titanium nitride coating stabilizes and reinforces the existing bond between the cubic boron nitride and the core, resulting in a grinding tool with greater efficiency and longer life. Specific operating conditions are required during the deposition process in order to ensure the proper level of adhesion of the titanium nitride layer.
    Type: Grant
    Filed: June 13, 1991
    Date of Patent: August 18, 1992
    Inventor: D. Lynn Julien
  • Patent number: 5139571
    Abstract: A semiconductor wafer polishing slurry that does not contaminate a wafer processing area utilizes an aqueous organic base to suspend the slurry's fine abrasive particles. The organic base has large cations (13,16,19) that do not diffuse into semiconductor wafers. Therefore ionic contamination from the polishing slurry is substantially eliminated.
    Type: Grant
    Filed: April 24, 1991
    Date of Patent: August 18, 1992
    Assignee: Motorola, Inc.
    Inventors: Paul W. Deal, Dennis B. Werho
  • Patent number: 5139572
    Abstract: A print of this invention has a color-forming area and a discoloring area. The color-forming area is printed by an ink containing a first color-changing agent which changes from substantially invisible colorlessness to visibleness by applying a color former. The discoloring area is printed by an ink containing a second color-changing agent which changes a from substantially invisible colorlessness to visibleness by applying the color former and returns to invisible colorlessness state as the time passes naturally after changing its color.
    Type: Grant
    Filed: June 6, 1990
    Date of Patent: August 18, 1992
    Inventor: Kiyoharu Kawashima
  • Patent number: 5139573
    Abstract: An ink that includes a liquid medium and a dye represented by the following Formula (I): ##STR1## wherein M represents a cation selected from an alkali metal, ammonium, and an organic ammonium; R.sub.1 and R.sub.2 independently represent a group selected from a hydrogen atom, a methyl group, a methoxy group, an ethoxy group, and an acetylamino group; R.sub.3, R.sub.4, R.sub.5, R.sub.6, R.sub.7 and R.sub.8 independently represent a group selected from a hydrogen atom, a hydroxyl group, a sulfonic acid group, a methoxy group, and an ethoxy group; X represents a hydrogen atom, an acetyl group, a benzoyl group, --SO.sub.2 C.sub.6 H.sub.5, --SO.sub.2 C.sub.6 H.sub.4 CH.sub.3, or ##STR2## where R.sub.9 and R.sub.10 independently represent a hydrogen atom, or --C.sub.2 H.sub.4 OH; and the sulfonic acid group is present as a salt of the same cation as that represented by M.
    Type: Grant
    Filed: August 21, 1991
    Date of Patent: August 18, 1992
    Assignee: Canon Kabushiki Kaisha
    Inventors: Takao Yamamoto, Tsuyoshi Eida, Katsuhiro Shirota, Megumi Saito
  • Patent number: 5139976
    Abstract: A Group IIA metal-Group IIIA metal-silicon substantially homogeneous liquid alkoxide is prepared from a reaction mixture of a Group IIA metal, a Group IIIA metal, a silicon tetraalkoxide, and a liquid defined by the formula ROR' where R is an alkyl group and R' is hydrogen or an alkyl group. The alkoxide can then be hydrolyzed, azeotropically distilled, dried, milled, and calcined to produce a ceramic powder. Advantageously, the ceramic powder can be compacted and sintered at relatively low temperatures which enable it to be used in electrical applications where high sintering temperatures would be deleterious.
    Type: Grant
    Filed: March 9, 1989
    Date of Patent: August 18, 1992
    Assignee: Union Carbide Coatings Service Technology Corporation
    Inventors: John F. Terbot, Richard F. Hill
  • Patent number: 5137540
    Abstract: A composite yet monolithic free abrasive grinding lap includes a sintered porous matrix of ceramic or metal material and a quantity of silicon filler material, substantially completely filling the pores of the sintered porous matrix preform at least throughout an effective region of the lap that is to come in contact with a workpiece to be acted upon by the lap. The lap may further have a multitude of abrasive particles embedded in the filler material at the effective region. The lap is made by first slip-casting a preform, then freezing and freeze-drying the same, followed by lightly sintering the dry preform into a porous matrix preform, bringing the temperature of the preform to above the melting point of the silicon filling material, and filling the pores with the filling material in its molten state.
    Type: Grant
    Filed: December 4, 1990
    Date of Patent: August 11, 1992
    Assignee: United Technologies Corporation
    Inventors: Pinke Halpert, Thomas O'Connell, Royce Platt
  • Patent number: 5137852
    Abstract: Thermodynamically stable ceramic composites are provided for use in high temperature oxidizing environments. The composites comprise high strength alumina fibers (Al.sub.2 O.sub.3) in a ceramic matrix. The ceramic matrix comprises material similar to the fibers to improve compatibility of the composite materials. A material selected from the .beta.-alumina and magnetoplumbite family of materials is used to provide a weakly bonded interface between the fibers and the ceramic matrix. .beta.-aluminas and magnetoplumbites have weak layers as an intrinsic characteristic of their crystal structure, which comprise spinel layers (basically Al.sub.2 O.sub.3) separated by very weakly bonded planes containing the .beta.-forming ions. The weak planes of these materials allow preferential debonding and sliding, and thus inhibit crack growth across the interface between the fibers and the ceramic matrix. The alumina fibers can be coated with .beta.
    Type: Grant
    Filed: January 11, 1991
    Date of Patent: August 11, 1992
    Assignee: Rockwell International Corp.
    Inventors: Peter E. D. Morgan, David B. Marshall
  • Patent number: 5137848
    Abstract: A dielectric composition comprising an admixture of finely divided particles of(a) 65-94 wt % of a non-reducing amorphous glass comprising of 15-27% ZnO, 8-30% alkaline earth metal oxides including 7-21% BaO, 40-60% SiO.sub.2, 3-14% Al.sub.2 O.sub.3, 0-5% PbO and 0.5-5% of a metal oxide selected from ZrO.sub.2, up to 2.5% P.sub.2 O.sub.5 and mixtures thereof, the composition being crystallizable and non-reducing when fired at 850.degree.-900.degree. C.(b) 30-5 wt % of a metal oxide of Al.sub.2 O.sub.3, ZrSiO.sub.4 and mixtures thereof,(c) 1-5 wt % of a metal oxide kerf additive of CoAl.sub.2 O.sub.4, Co/CrAl.sub.2 O.sub.4, CoO, CoCr.sub.2 O.sub.4, Cr.sub.2 O.sub.3, TiO.sub.2, and mixtures thereof,where the sum of the components a and b does not exceed 35% by weight of the total particulate admixture, and(d) optionally, 1-10 wt % of either a TCE reducing additive of zircon, mullite, silica, and mixtures thereof or a TCE increasing additive of CaZrO.sub.3, quartz, .alpha.-cristobalite and mixtures thereof.
    Type: Grant
    Filed: December 13, 1990
    Date of Patent: August 11, 1992
    Assignee: E. I. Du Pont de Nemours and Company
    Inventors: Michael F. Barker, William A. Craig, Paul C. Donohue, Kenneth W. Hang, Michael J. Haun, Colin R. Pickering
  • Patent number: 5137849
    Abstract: A sealing glass is provided for the production of glass-to-metal seals, especially for battery headers, in storage batteries having a lithium electrode. The constituents of the glass, expressed in % by weight on an oxide basis, comprise:______________________________________ 16-25 SiO.sub.2 0-8 Li.sub.2 O 0-4 MgO 20-35 B.sub.2 O.sub.3 0-5 Na.sub.2 O 5-12 CaO 15-24 Al.sub.2 O.sub.3 0-10 K.sub.2 O 10-30 BaO + SrO 4-15 .SIGMA. alkali oxide 0-5 ZnO 15-40 .SIGMA. alkaline- earth oxide + ZnO ______________________________________The coefficient of thermal expansion of the glass is closely matched to the metals in the cell housing. This glass also has a good welding strength and corrosion resistance, as well as satisfactory hydrolytic resistance.
    Type: Grant
    Filed: October 22, 1990
    Date of Patent: August 11, 1992
    Assignee: Schott Glaswerke
    Inventors: Peter Brix, Ludwig Gaschler
  • Patent number: 5137574
    Abstract: A method of producing a high opacifying kaolin pigment by separating from one or more iron-stained titania-containing crude kaolins having a titania content of from about 1 to 2 weight percent, one or more titania-enriched kaolin fractions which contain the titania in an amount of above 2 weight percent; subjecting the fraction(s) to media grinding; dewatering and drying the media ground fraction(s); blending the fraction(s) with a fine particle size unground kaolin having a titania content less than 2%, in proportions to provide a calciner feed having at least 2% titania; and calcining the feed at a temperature in the range of 1500.degree. to 2200.degree. F.
    Type: Grant
    Filed: November 30, 1990
    Date of Patent: August 11, 1992
    Assignee: ECC America Inc.
    Inventors: Paul Suitch, Ralph E. Turner, Jr., Dona L. Archer, William B. Smith
  • Patent number: 5137541
    Abstract: A method of cleaning and polishing a variety of porous and non-porous materials including porcelains, plastics, marble, glass, and finished wood. The polishing compound is comprised of an abrasive powder, an hydroflouric acid, and an organic solvent. The polishing compound is applied with a cloth and scouring of the surface to be cleaned and polished is accomplished with a soft cloth or with a polishing machine. The invention effectively removes scratches, stains, and blemishes from the surface to be polished and after scouring the result is a blemish free and polished surface.
    Type: Grant
    Filed: March 18, 1991
    Date of Patent: August 11, 1992
    Inventor: John D. Foster
  • Patent number: 5137853
    Abstract: A beta alumina sintered body having no tantalum component in an intergranular phase is manufactured by mixing raw materials consisting essentially of 8.0-10.0 wt % of sodium oxide, 3.0-5.5 wt % of magnesium oxide and/or 0.1-2.0 wt % of lithium oxide, 0.01-0.5 wt % of tantalum oxide, and the remainder of aluminum oxide to obtain raw material powders; forming the raw material powders to obtain a formed body; and sintering the formed body.
    Type: Grant
    Filed: August 5, 1991
    Date of Patent: August 11, 1992
    Assignee: NGK Insulators, Ltd.
    Inventors: Shuichi Ichikawa, Tomonori Takahashi
  • Patent number: 5137576
    Abstract: Quinacridones having selectively adjusted triboelectric effects, which quinacridones contain about 0.05% to 100 percent by weight of triboelectrically active compounds of the general formula IQ--A--Y].sub.n (I),in which Q is a quinacridone radical which is unsubstituted or substituted by halogen atoms, alkyl, alkoxy H.sub.2 N--CO--, alkyl--NH--CO-- or (alkyl).sub.2 N--CO groups, A is a direct bond or --O--, --S--, --NR.sup.1 --, --CO--, --SO.sub.2 --, --CR.sup.2 R.sup.3 -- or arylene and Y is an --NR.sup.4 R.sup.5 group or a five-, six- or seven-membered heterocycle which contains one to three heteroatoms from the series comprising nitrogen and/or oxygen and/or sulfur and which can be substituted by alkyl, alkoxy, hydroxyphenyl, halogen, --CN, --COOH, --CO-- NRR', --SO.sub.2 --NRR', hydroxyalkyl or alkylaminoalkyl, in which R and R' together with the nitrogen atom can be a heterocycle, R and R' are hydrogen atoms or alkyl and R.sup.1 to R.sup.
    Type: Grant
    Filed: September 28, 1989
    Date of Patent: August 11, 1992
    Assignee: Hoechst Aktiengesellschaft
    Inventors: Hans-Tobias Macholdt, Adolf Kroh, Alexander Sieber, Erwin Dietz
  • Patent number: 5137577
    Abstract: An additive to cement comprises a granular zinc salt of a copolymer of an olefin having 2 to 8 carbon atoms and an ethylenically unsaturated dicarboxylic anhydride, prepared by reacting the powder of the copolymer with powder of zinc oxide or zinc hydroxide in the presence of water.
    Type: Grant
    Filed: March 26, 1991
    Date of Patent: August 11, 1992
    Assignee: Kao Corporation
    Inventors: Masanori Iizuka, Tatsuya Mizunuma, Fuzio Yamato, Toshiharu Kojima, Akitoshi Tuji
  • Patent number: 5137567
    Abstract: The pigment is constituted by zinc phosphate dihydrate or tetrahydrate with an excess of from 0.5 to 6% of zinc oxide over the stoichiometric amount and has the form of rough surfaced spheroids having a maximum dimension lying between 0.5 and 6 microns and a mean size lying between 1.5 and 2.5 microns.
    Type: Grant
    Filed: November 20, 1989
    Date of Patent: August 11, 1992
    Assignee: Colores Hispania S.A.
    Inventors: Juan Aubareda Vallvey, Oscar Leblanc Francia, Martorell Sole
  • Patent number: 5138078
    Abstract: A compound of the formula (I) ##STR1## wherein R is hydrogen, methyl of C.sub.2 -C.sub.5 alkyl and R.sup.1 is O-phenylene, a saturated or unsaturated 1,2-cyclohexylene group; a 2,3-bicyclo[2.2.2]-hept-5-enyl group of the formula (II) ##STR2## or a saturated or unsaturated aliphatic group of about 2 to about 20 carbon atoms; said O-phenylene is optionally substituted in the ring by one or two alkyl groups of from 1 to 4 carbon atoms; said 1,2-cyclohexylene and bicyclo groups are optionally substituted by one or two alkyl groups of from 1 to 4 carbon atoms and/or by one to six chlorine or bromine atoms; and said aliphatic group is optionally substituted by one or more chlorine or bromine atoms. This compound can be used as a coating compound when mixed with curing agents.
    Type: Grant
    Filed: December 10, 1990
    Date of Patent: August 11, 1992
    Assignee: Ciba-Geigy Corporation
    Inventor: Vincent Brytus