Abstract: Dual zone reverse phase packing materials for use in liquid chromatographic blood serum analysis are prepared by contacting a porous support, such as porous silica, with a fluorocarbon silane, such as a perfluorobutylsilyl compound, to form a lipophobic phase in the external zone of the porous support, and, then contacting the porous support with a lipophilic silane, such as an octadecylsilyl compound, to form a lipophilic partitioning phase in the internal zone of the porous support. Ketal blocked diol groups, which later may be hydrolyzed to diol groups, are also attached to both zones of the packing materials. The dual zone reverse phase packing materials display a reduced degree of serum protein adsorption in the external zone while drug substances are retained and separated by the lipophilic partitioning phase in the internal zone.

Abstract: Packing materials for use in liquid chromatographic analysis are prepared by contacting a porous support, such as porous silica, with a ketal silane to form ketal blocked diol groups on the surfaces thereof. An end-capping reagent such as a trimethylsilyl reagent may be added. In addition, the ketal blocked diol groups may be further hydrolyzed to diol groups.

Abstract: The steering system includes a rotatable steering control member located remotely from a steerable dirigible wheel unit, a drive sprocket mounted for common rotation with the steering control member, a short length of roller or sprocket chain trained about the drive sprocket, a driven sprocket mounted for common rotation with the dirigible wheel unit, a short length of roller or sprocket chain trained about the driven sprocket, and flexible members, such as wire cables, interconnecting the chains so that the driven sprocket is rotated in response to rotation of the drive sprocket. Two sets of coaxially aligned pairs of pulley are located between the drive and driven sprockets and the cables are trained over the same sides of the pulleys in each set and thereby are guided through a circuitous route between the sprockets. One set of pulleys is adjustably mounted relative to the cables for adjusting the tension applied on the cables to remove slack therefrom.

Abstract: Disclosed herein is a device for introducing soil treatment liquids into the ground including a plurality of injection tines having a downwardly directed tip portion and connected to a rotatable crankshaft for reciprocative movement between a raised or non-injection position and an injection position wherein the tine portion is located beneath the ground surface. Flow of the treatment liquid to the tines is controlled by a rotary flow distribution valve which is connected directly to a chain drive sprocket mounted on the crankshaft and which is arranged to selectively supply the treatment liquid to the tines only when they are in the injection position. Each tine has a generally spherical tip made from a high aluminum ceramic material and an internal check valve located near the tip for minimizing the amount of residual liquid which can be shaken from the tine while it is in the non-injection position.

Abstract: Disclosed herein is a canopy for vehicles, such as golf cars, which canopy is adapted for mounting on a plurality of upstanding support posts carried by a vehicle. The canopy includes brackets for mounting thereof on the vehicle support posts, a resilient, perimeter frame supported by the support brackets and having opposed arcuate end sections, which in their free form, lie in a generally horizontally, outwardly bowed relation to each other, and a flexible, water-repellent top mounted on the perimeter frame in a manner so as to distort the end sections upwardly from their free form and cause the end sections, in attempting to return to their free form, to apply multi-directional stresses on the top such that the top assumes a generally upwardly convex shape in cross section.