Abstract: A system and method for measuring viscosity, melt flow index (MFI), and melt volume rate (MVR) of a polymer melt in real-time during an extrusion process to provide quick and accurate feedback for process control. The system includes a polymer processing rate sensor (36), a polymer melt temperature sensor (30), an extruder pressure sensor (32), and a die head temperature sensor (34) for taking in-line measurements during the extrusion process. The in-line measurements are made on the main process stream of the polymer melt, with the determination of viscosity, MFI, and MVR based on these measured values and those obtained during a calibration run with polymers having known properties. The invention can be used in any polymer compounding and extrusion process utilizing die opening with any constant geometry for monitoring quality and providing feedback for process control.

Abstract: A system and method for measuring viscosity, melt flow index (MFI), and melt volume rate (MVR) of a polymer melt in real-time during an extrusion process to provide quick and accurate feedback for process control. The system includes a polymer processing rate sensor (36), a polymer melt temperature sensor (30), an extruder pressure sensor (32), and a die head temperature sensor (34) for taking in-line measurements during the extrusion process. The in-line measurements are made on the main process stream of the polymer melt, with the determination of viscosity, MFI, and MVR based on these measured values and those obtained during a calibration run with polymers having known properties. The invention can be used in any polymer compounding and extrusion process utilizing die opening with any constant geometry for monitoring quality and providing feedback for process control.

Abstract: Thirty substantially pure and biologically active peptides are disclosed. Nucleic acids that have sequences coding for the biologically active peptides and pharmaceutical formulations produced thereform are also disclosed.

Abstract: A method and apparatus for measuring the rheological properties of a polymer melt includes flowing the polymer melt from a first reactor to a device through a conduit at a predetermined flow rate, measuring a first pressure of the polymer melt at a first location in the conduit, measuring a second pressure at a second location downstream from the first location, measuring a temperature at a third location in the conduit, wherein the third location is between the first location and the second location, and calculating the Theological property of the polymer melt as it flows through the conduit. The method and apparatus do not require diversion of the polymer melt from the main process stream.

Abstract: A system for providing process control information, such as viscosity, concerning a polymer melt comprises a means containing a polymer melt under pressure; means for diverting a stream of the polymer melt directly from said containing means to and through an orifice of predetermined geometrical shape wherein the flow of said diverted portion to and through said orifice is unobstructed and directly dependent on the pressure of said main polymer melt wherein the cross sectional area is sized to permit the flow of said diverted melt polymer therethrough absence additional independent means acting on said diverted melt polymer for increasing flow through said orifice; temperature sensing means for measuring the temperature of the diverted melt stream and producing a resultant temperature signal; pressure sensing means for measuring the pressure of the diverted melt stream and producing a resultant pressure signal, said pressure signal being directly dependent on the pressure of polymer in said main polymer melt

Abstract: Yaw rate sensors are provided, the use of which permits quantitative measurement of yaw rate. The yaw rate sensor comprises at least a base, a first suspension and a second suspension with a proof mass supported between the two suspensions, which together form a resonator. The first suspension has a pair of thin-wire driving electrodes double side patterned on the surfaces. When a driving voltage is applied to the driving electrodes, it imposes an electric field to piezoelectrically induce a driving resonance. When the sensor is rotated around its sensing axis, the resonator will be forced to generate a sensing resonance out of the driving resonance plane to compensate the change in the linear momentum which must be conserved. The piezoelectric charge signal generated by the sensing resonance on the sensing electrodes which are double side patterned on the surfaces of the second suspension is used to detect the yaw rate. Specifically, the amplitude of the sensing resonance is in proportion to the yaw rate.

Abstract: Linear polyesters are branched by transesterification with resins having the formula: ##STR1## wherein n is an integer of from 1 to 10.

Abstract: The disclosure describes reacting a multi-functional phenolic or carboxylic branching agent with a transesterification catalyst to form an organic salt prior to reactive extrusion of said organic salt branching agent with linear polycarbonate resin as a means to dramatically increase the efficiency of the branching agent in the preparation of branched polycarbonate.

Abstract: A system for providing process control information, such as viscosity, concerning a polymer melt comprises a means containing a polymer melt under pressure; means for diverting a stream of the polymer melt directly from said containing means to and through an orifice of predetermined geometrical shape wherein the flow of said diverted portion to and through said orifice is unobstructed and directly dependent on the pressure of said main polymer melt wherein the cross sectional area is sized to permit the flow of said diverted melt polymer therethrough absence additional independent means acting on said diverted melt polymer for increasing flow through said orifice; temperature sensing means for measuring the temperature of the diverted melt stream and producing a resultant temperature signal; pressure sensing means for measuring the pressure of the diverted melt stream and producing a resultant pressure signal, said pressure signal being directly dependent on the pressure of polymer in said main polymer melt

Abstract: Branched polycarbonates are prepared by the reaction of a linear or branched polycarbonate with a branching resin having a molecular weight up to about 3,000, typically a novolak or a bisphenol polymer. The reaction preferably takes place in the presence of a carbonate equilibration catalyst such as a quaternary bisphenolate.

Abstract: A composition comprising a phosphorus containing acid and an ester of a phosphorus containing acid useful for imparting improved physical and chemical properties to polymers containing polyesters, copolyester carbonates, polycarbonates, and mixtures thereof, a method of treating said polymers with said composition, and articles of manufacture comprising said polymers and said composition.

Abstract: Solid state gas sensors are provided, the use of which permits quantitative measurement of gaseous contaminants or change of composition of a gas or atmosphere being monitored. The gas sensor comprises at least a base, a first electrode, a second electrode. The first electrode has a finely tapered end to strengthen the electric field intensity in the gap between the first and the second electrodes. The sensing is based on ionization potential difference between the molecules of the contaminating gas and of the atmosphere. When a high voltage is applied to the electrodes, it creates a strong electric field between the electrodes, especially a very strong electric field around the tapered end of the first electrode. When the potential is sufficiently high, the gas in the vicinity of the tapered end of the first electrode will be ionized. The ions and electrons generated by the ionization create an electric current flows between the two electrodes and across the gap.