Patents by Inventor Gerhard Mestl

Gerhard Mestl has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Publication number: 20240150261
    Abstract: A method for producing a target compound, includes distributing feed mixture at a temperature in a first temperature range to a plurality of parallel reaction tubes of a shell-and-tube reactor. The method further includes subjecting the feed mixture in first tube sections of the reaction tubes to heating to a temperature in a second temperature range, and in second tube sections of the reaction tubes arranged downstream of the first tube sections to oxidative catalytic conversion using one or more catalysts arranged in the second tube sections. The heating is performed, at least in part, using a catalyst arranged in the first tube sections and having a light-off temperature in the first temperature range.
    Type: Application
    Filed: March 14, 2022
    Publication date: May 9, 2024
    Inventors: Mathieu Zellhuber, Martin Schubert, Andreas Meiswinkel, Wolfgang Muller, Ernst Haidegger, Gerhard Mestl, Klaus Wanninger, Peter Scheck
  • Publication number: 20240150263
    Abstract: A process for producing a target compound includes forming a feed mixture containing at least one reactant compound. The feed mixture is distributed to parallel reaction tubes of one or more shell-and-tube reactors and subjected to oxidative catalytic conversion in the reaction tubes. Steam is added to the feed mixture in an amount such that a steam fraction of the feed mixture is 5 to 95 vol %, oxygen is added to the feed mixture in the form of a fluid containing at least 95 vol % oxygen, and the oxidative catalytic conversion is carried out using one or more catalysts containing the metals molybdenum, vanadium, niobium and optionally tellurium.
    Type: Application
    Filed: March 14, 2022
    Publication date: May 9, 2024
    Inventors: Mathieu Zellhuber, Martin Schubert, Andreas Meiswinkel, Gerhard Mestl, Klaus Wanninger, Peter Scheck, Anina Wohl
  • Publication number: 20230212134
    Abstract: The present invention relates to a process for starting up a reactor for preparation of phthalic anhydride by the catalytic oxidation of ortho-xylene and/or naphthalene, containing a bed of shaped catalyst bodies and within a temperature-controlled salt bath. The industrial production of phthalic anhydride from ortho-xylene and/or naphthalene is affected by selective gas phase oxidation in a shell and tube reactor cooled with a salt bath, which may contain several thousand reactor tubes. There are 4 to 5 different catalyst layers in each reactor, which are introduced into each reactor successively in axial direction.
    Type: Application
    Filed: July 8, 2021
    Publication date: July 6, 2023
    Inventors: Oliver Richter, Gerhard Mestl, Martin Schoenfelder, Werner Pitschi
  • Publication number: 20220266233
    Abstract: The invention relates to a catalyst system for producing maleic anhydride by means of the catalytic oxidation of n-butane, comprising at least one reactor tube, which has two catalyst layers consisting of different catalyst particles, characterized in that the geometric surface area per catalyst particle is greater in the catalyst layer that is first in the gas flow direction than in the second catalyst layer. The invention further relates to a process for producing maleic anhydride by means of the catalytic oxidation of n-butane, wherein a mixture of oxygen and n-butane is fed through the catalyst system according to the invention and the at least one reactor tube is at elevated temperature.
    Type: Application
    Filed: October 9, 2020
    Publication date: August 25, 2022
    Inventors: Sebastian BOECKLEIN, Gerhard MESTL, Anna ADLER, Martin KUTSCHERAUER,
  • Patent number: 11400442
    Abstract: The disclosure relates to a process for producing a VPO catalyst containing molybdenum and a vanadyl pyrophosphate phase, which comprises the steps: a) provision of a reaction mixture comprising a V(V) compound, a P(V) compound, an Mo compound, a reducing agent and a solvent, b) reduction of the V(V) compound by means of the reducing agent at least in parts to give vanadyl hydrogenphosphate in order to obtain an intermediate suspension, c) filtration of the intermediate suspension from step b) in order to obtain an intermediate, d) drying of the intermediate at a temperature of not more than 350° C. in order to obtain a dried intermediate and e) activation of the dried intermediate at a temperature above 200° C., characterized in that not more than 0.2% by weight of water, based on the weight of the reaction mixture, is present in step a) and no water is withdrawn during the reduction in step b).
    Type: Grant
    Filed: January 16, 2020
    Date of Patent: August 2, 2022
    Assignee: CLARIANT INTERNATIONAL LTD
    Inventors: Sebastian Boecklein, Gerhard Mestl, Gabriele Bindseil, Rene Hausmann, Sarah Limbrunner, Anna Waldschuetz
  • Patent number: 11161096
    Abstract: A novel mixed oxide material is disclosed which comprises molybdenum, vanadium, tellurium and niobium and the use of the mixed oxide material as catalyst for the oxidative dehydrogenation of ethane to ethene or the oxidation of propane to acrylic acid and a process for producing the mixed oxide material.
    Type: Grant
    Filed: January 26, 2018
    Date of Patent: November 2, 2021
    Assignee: CLARIANT PRODUKTE (DEUTSCHLAND) GMBH
    Inventors: Gerhard Mestl, Klaus Wanninger, Daniel Melzer, Maria Cruz Sanchez-Sanchez, Julia Tseglakova, Johannes Lercher
  • Patent number: 11097254
    Abstract: A novel mixed oxide material is disclosed which contains molybdenum, vanadium, tellurium and niobium and the use of the molybdenum mixed oxide material as catalyst for the oxidative dehydrogenation of ethane to ethene or the oxidation of propane to acrylic acid and a process for producing the mixed oxide material.
    Type: Grant
    Filed: January 26, 2018
    Date of Patent: August 24, 2021
    Assignee: CLARIANT PRODUKTE (DEUTSCHLAND) GMBH
    Inventors: Gerhard Mestl, Klaus Wanninger, Daniel Melzer, Maria Cruz Sanchez-Sanchez, Julia Tseglakova, Johannes Lercher
  • Patent number: 11059032
    Abstract: A novel coated catalyst having an outer shell which is composed of a catalyst material having high surface area and contains molybdenum, vanadium, tellurium and niobium, and the use of this catalyst for the oxidative dehydrogenation of ethane to ethene or the oxidation of propane to acrylic acid and also a process for producing the catalyst is disclosed.
    Type: Grant
    Filed: September 13, 2018
    Date of Patent: July 13, 2021
    Assignee: CLARIANT INTERNATIONAL LTD
    Inventors: Gerhard Mestl, Klaus Wanninger, Silvia Neumann, Peter Schinke
  • Patent number: 11014075
    Abstract: A novel catalyst and process for producing a mixed oxide material containing molybdenum, vanadium, tellurium and niobium is disclosed. The material can be used as a catalyst for the oxidative dehydrogenation of ethane to ethene or the oxidation of propane to acrylic acid.
    Type: Grant
    Filed: January 26, 2018
    Date of Patent: May 25, 2021
    Assignee: Clariant Produkte Gmbh
    Inventors: Gerhard Mestl, Klaus Wanninger, Daniel Melzer, Maria Cruz Sanchez-Sanchez, Julia Tseglakova, Johannes Lercher
  • Patent number: 11007509
    Abstract: A simple, scalable, inexpensive, and reproducible method of selectively preparing the M1 phase of a MoVNbTe mixed oxide in a hydrothermal synthesis using tellurium dioxide is disclosed which can utilize inexpensive metal oxides as starting compounds.
    Type: Grant
    Filed: January 26, 2018
    Date of Patent: May 18, 2021
    Assignee: CLARIANT PRODUCKTE GMBH
    Inventors: Gerhard Mestl, Klaus Wanninger, Silvia Neumann
  • Publication number: 20200290026
    Abstract: A novel catalyst and process for producing a mixed oxide material containing molybdenum, vanadium, tellurium and niobium is disclosed. The material can be used as a catalyst for the oxidative dehydrogenation of ethane to ethene or the oxidation of propane to acrylic acid.
    Type: Application
    Filed: January 26, 2018
    Publication date: September 17, 2020
    Inventors: Gerhard MESTL, Klaus WANNINGER, Daniel MELZER, Maria Cruz SANCHEZ-SANCHEZ, Julia TSEGLAKOVA, Johannes LERCHER
  • Publication number: 20200222893
    Abstract: The disclosure relates to a process for producing a VPO catalyst containing molybdenum and a vanadyl pyrophosphate phase, which comprises the steps: a) provision of a reaction mixture comprising a V(V) compound, a P(V) compound, an Mo compound, a reducing agent and a solvent, b) reduction of the V(V) compound by means of the reducing agent at least in parts to give vanadyl hydrogenphosphate in order to obtain an intermediate suspension, c) filtration of the intermediate suspension from step b) in order to obtain an intermediate, d) drying of the intermediate at a temperature of not more than 350° C. in order to obtain a dried intermediate and e) activation of the dried intermediate at a temperature above 200° C., characterized in that not more than 0.2% by weight of water, based on the weight of the reaction mixture, is present in step a) and no water is withdrawn during the reduction in step b).
    Type: Application
    Filed: January 16, 2020
    Publication date: July 16, 2020
    Inventors: Sebastian BOECKLEIN, Gerhard MESTL, Gabriele BINDSEIL, Rene HAUSMANN, Sarah LIMBRUNNER, Anna WALDSCHUETZ
  • Publication number: 20200215516
    Abstract: A novel coated catalyst having an outer shell which is composed of a catalyst material having high surface area and contains molybdenum, vanadium, tellurium and niobium, and the use of this catalyst for the oxidative dehydrogenation of ethane to ethene or the oxidation of propane to acrylic acid and also a process for producing the catalyst is disclosed.
    Type: Application
    Filed: September 13, 2018
    Publication date: July 9, 2020
    Inventors: Gerhard MESTL, Klaus WANNINGER, Silvia NEUMANN, Peter SCHINKE
  • Patent number: 10668453
    Abstract: The present invention relates to a process for producing a composite material and also the composite material itself. The composite material contains a bismuth-molybdenum-nickel mixed oxide or a bismuth-molybdenum-cobalt mixed oxide and a specific SiO2 as pore former. The present invention also relates to the use of the composite material according to the invention for producing a washcoat suspension and also a process for producing a coated catalyst using the composite material according to the invention. Furthermore, the present invention also relates to a coated catalyst which has a catalytically active shell comprising the composite material according to the invention on a support body. The coated catalyst according to the invention is used for preparing [alpha],[beta]-unsaturated aldehydes from olefins.
    Type: Grant
    Filed: April 24, 2018
    Date of Patent: June 2, 2020
    Assignee: CLARIANT INTERNATIONAL LTD
    Inventors: Inga Walzel, Gerhard Mestl, Silvia Neumann, Magdalena Pritzl, Gabriele Donabauer, Robert K. Grasselli
  • Publication number: 20200139349
    Abstract: The invention relates to a mixed oxide material comprising the elements molybdenum, vanadium, niobium and tellurium, which, when using the Cu-K? radiation, has diffraction reflections h, i, k and l in the XRD spectrum, said diffraction reflexes having their apex points at the diffraction angles (2·) 26.2°±0.5° (h), 27.0°±0.5° (i), 7.8°±0.5° (k) and 28.0°±0.5° (l), characterized in that the mixed oxide material has a pore volume of >0.1 cm3/g. The mixed oxide material according to the invention is produced by a method comprising the steps of: a) producing a mixture of starting compounds containing molybdenum, vanadium, niobium and tellurium dioxide as a tellurium-containing starting compound as well as oxalic acid and a further oxoligand selected from the group consisting of dicarboxylic acids and diols, b) hydrothermally treating the mixture of starting compounds at a temperature of 100 to 300° C.
    Type: Application
    Filed: January 26, 2018
    Publication date: May 7, 2020
    Inventors: Gerhard MESTL, Klaus WANNINGER, Daniel MELZER, Maria Cruz SANCHEZ-SANCHEZ, Julia TSEGLAKOVA, Johannes LERCHER
  • Publication number: 20200061583
    Abstract: A novel mixed oxide material is disclosed which contains molybdenum, vanadium, tellurium and niobium and the use of the molybdenum mixed oxide material as catalyst for the oxidative dehydrogenation of ethane to ethene or the oxidation of propane to acrylic acid and a process for producing the mixed oxide material.
    Type: Application
    Filed: January 26, 2018
    Publication date: February 27, 2020
    Inventors: Gerhard MESTL, Klaus WANNINGER, Daniel MELZER, Maria Cruz SANCHEZ-SANCHEZ, Julia TSEGLAKOVA, Johannes LERCHER
  • Publication number: 20190366311
    Abstract: The invention relates to a method for producing a mixed oxide material containing the elements molybdenum, vanadium, niobium and tellurium, comprising the following steps: a) producing a mixture from starting compounds containing molybdenum, vanadium, niobium and a tellurium-containing starting compound, present in the tellurium in the +4 oxidation state, b) hydrothermal treatment of the mixture from starting compounds at a temperature of between 100° C. to 300° C., in order to obtain a product suspension, c) separating off and drying the solid material from the product suspension obtained in step b), d) activating the solid material in inert gas in order to obtain the mixed oxide material. The invention is characterized in that the tellurium-containing starting compound has a particle size D90 of less than 100 ?m.
    Type: Application
    Filed: January 26, 2018
    Publication date: December 5, 2019
    Inventors: Gerhard MESTL, Klaus WANNINGER, Silvia NEUMANN
  • Patent number: 10227319
    Abstract: A catalytic converter arrangement for producing phthalic anhydride by means of a gas phase oxidation of aromatic hydrocarbons, comprising a reactor with a gas inlet side for a reactant gas, a gas outlet side for a product gas, a first catalytic converter layer made of catalytic converter elements, and at least one second catalytic converter layer made of catalytic converter elements. The first catalytic converter layer is arranged on the gas inlet side, and the second catalytic converter layer is arranged downstream of the first catalytic converter layer in the gas flow direction. The catalytic converter elements have an outer layer of an active compound. The invention is characterized in that the active compound content in the first catalytic converter layer and/or in the second catalytic converter layer is below 7 wt.
    Type: Grant
    Filed: April 23, 2015
    Date of Patent: March 12, 2019
    Assignee: CLARIANT INTERNATIONAL LTD.
    Inventors: Oliver Richter, Gerhard Mestl, Felix Schulz, Werner Pitschi, Nadine Fromm, Peter Schinke
  • Publication number: 20190022629
    Abstract: The present invention relates to a process for producing a composite material and also the composite material itself. The composite material contains a bismuth-molybdenum-nickel mixed oxide or a bismuth-molybdenum-cobalt mixed oxide and a specific SiO2 as pore former. The present invention also relates to the use of the composite material according to the invention for producing a washcoat suspension and also a process for producing a coated catalyst using the composite material according to the invention. Furthermore, the present invention also relates to a coated catalyst which has a catalytically active shell comprising the composite material according to the invention on a support body. The coated catalyst according to the invention is used for preparing [alpha],[beta]-unsaturated aldehydes from olefins.
    Type: Application
    Filed: April 24, 2018
    Publication date: January 24, 2019
    Applicant: Clariant International Ltd.
    Inventors: Inga WALZEL, Gerhard MESTL, Silvia NEUMANN, Magdalena PRITZL, Gabriele DONABAUER, Robert K. GRASSELLI
  • Patent number: 10155713
    Abstract: The invention relates to a catalyst arrangement for preparing phthalic anhydride by gas-phase oxidation of aromatic hydrocarbons, which comprises a reactor having a gas inlet end for a feed gas and a gas outlet end for a product gas and also a first catalyst zone made up of catalyst bodies and at least one second catalyst zone made up of catalyst bodies, where the first catalyst zone is arranged at the gas inlet end and the second catalyst zone is arranged downstream of the first catalyst zone in the gas flow direction and the length of the first catalyst zone in the gas flow direction is less than the length of the second catalyst zone in the gas flow direction, characterized in that the first catalyst zone has a higher gap content compared to the second catalyst zone.
    Type: Grant
    Filed: April 23, 2015
    Date of Patent: December 18, 2018
    Assignee: Clariant International Ltd.
    Inventors: Oliver Richter, Gerhard Mestl, David Lesser, Robert Marx, Nadine Fromm, Felix Schulz, Peter Schinke, Werner Pitschi