Patents by Inventor Muhammad Shahzad

Muhammad Shahzad has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 12031086
    Abstract: A method of removing a sulfate scale from a surface is provided. The method includes contacting the sulfate-comprising scale with a conversion solution including 1 to 10 wt. % of an alkali metal carbonate, 0.5 to 10 wt. % of a borate salt or hydrate thereof, and 0.5 to 2.5 wt. % of a base to produce a carbonate-comprising scale. The method further includes exposing the carbonate-comprising scale with an acid solution including 2.5 to 25 wt. % of an acid.
    Type: Grant
    Filed: March 18, 2024
    Date of Patent: July 9, 2024
    Assignee: King Fahd University of Petroleum and Minerals
    Inventors: Mohamed Mahmoud, Muhammad Shahzad Kamal
  • Publication number: 20240218238
    Abstract: A method of removing a sulfate scale from a surface is provided. The method includes contacting the sulfate-comprising scale with a conversion solution including 1 to 10 wt. % of an alkali metal carbonate, 0.5 to 10 wt. % of a borate salt or hydrate thereof, and 0.5 to 2.5 wt. % of a base to produce a carbonate-comprising scale. The method further includes exposing the carbonate-comprising scale with an acid solution including 2.5 to 25 wt. % of an acid.
    Type: Application
    Filed: March 18, 2024
    Publication date: July 4, 2024
    Applicant: King Fahd University of Petroleum and Minerals
    Inventors: Mohamed MAHMOUD, Muhammad Shahzad KAMAL
  • Publication number: 20240218237
    Abstract: A method of removing a sulfate scale from a surface is provided. The method includes contacting the sulfate-comprising scale with a conversion solution including 1 to 10 wt. % of an alkali metal carbonate, 0.5 to 10 wt. % of a borate salt or hydrate thereof, and 0.5 to 2.5 wt. % of a base to produce a carbonate-comprising scale. The method further includes exposing the carbonate-comprising scale with an acid solution including 2.5 to 25 wt. % of an acid.
    Type: Application
    Filed: March 18, 2024
    Publication date: July 4, 2024
    Applicant: King Fahd University of Petroleum and Minerals
    Inventors: Mohamed MAHMOUD, Muhammad Shahzad KAMAL
  • Publication number: 20240218236
    Abstract: A method of removing a sulfate scale from a surface is provided. The method includes contacting the sulfate-comprising scale with a conversion solution including 1 to 10 wt. % of an alkali metal carbonate, 0.5 to 10 wt. % of a borate salt or hydrate thereof, and 0.5 to 2.5 wt. % of a base to produce a carbonate-comprising scale. The method further includes exposing the carbonate-comprising scale with an acid solution including 2.5 to 25 wt. % of an acid.
    Type: Application
    Filed: March 18, 2024
    Publication date: July 4, 2024
    Applicant: King Fahd University of Petroleum and Minerals
    Inventors: Mohamed MAHMOUD, Muhammad Shahzad KAMAL
  • Patent number: 11981856
    Abstract: A drilling fluid composition includes an aqueous base fluid, 0.01 to 10 wt. % of a date palm leaves extract (DPLE), 1 to 10 wt. % of clay particles, and 0.01 to 1 wt. % of a base, where each wt. % based on a total weight of the drilling fluid composition. The DPLE is homogenously disposed on surfaces of the clay particles. The clay particles disposed with the DPLE are present in the drilling fluid composition in the form of a composite. A pellet made from the clay particles treated with the DPLE has a swelling value at least 75% less than a swelling value of the pellet in an aqueous composition that does not contain the DLPE. A method of making the drilling fluid composition.
    Type: Grant
    Filed: March 10, 2023
    Date of Patent: May 14, 2024
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Tawfik Abdo Saleh, Azeem Rana, Mobeen Murtaza, Muhammad Shahzad Kamal, Mohamed Mahmoud
  • Patent number: 11965132
    Abstract: A method of removing a sulfate scale from a surface is provided. The method includes contacting the sulfate-comprising scale with a conversion solution including 1 to 10 wt. % of an alkali metal carbonate, 0.5 to 10 wt. % of a borate salt or hydrate thereof, and 0.5 to 2.5 wt. % of a base to produce a carbonate-comprising scale. The method further includes exposing the carbonate-comprising scale with an acid solution including 2.5 to 25 wt. % of an acid.
    Type: Grant
    Filed: August 3, 2023
    Date of Patent: April 23, 2024
    Assignee: King Fahd University of Petroleum and Minerals
    Inventors: Mohamed Mahmoud, Muhammad Shahzad Kamal
  • Patent number: 11866641
    Abstract: A surfactant of formula (I) wherein each of R1 and R2 are independently a hydrogen, an optionally substituted alkyl, an optionally substituted cycloalkyl, or an optionally substituted arylalkyl, R3 and R4 are independently an optionally substituted alkyl, an optionally substituted cycloalkyl, or an optionally substituted arylalkyl, x is an integer in a range of 2-8, y is an integer in a range of 1-15, z is an integer in a range of 4-10, n is an integer in a range of 2-5, and A is one of a carboxybetaine group, a sulfobetaine group, or a hydroxy sulfobetaine group. An oil and gas well servicing fluid containing the surfactant and methods of servicing an oil and gas well are also described.
    Type: Grant
    Filed: December 23, 2022
    Date of Patent: January 9, 2024
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: S. M. Shakil Hussain, Muhammad Shahzad Kamal
  • Patent number: 11858878
    Abstract: The invention concerns synthesized amido-amine-based cationic gemini surfactants with flexible and rigid spacers and different hydrophobic. These gemini surfactants were prepared by modified procedure through amidation of long chain carboxylic acids using 3-(dimethylamino)-1-propylamine followed by treatment with halohydrocarbons and showed excellent thermal stability and surface properties useful for various oilfield applications such as enhanced oil recovery.
    Type: Grant
    Filed: November 3, 2022
    Date of Patent: January 2, 2024
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Syed M. Shakil Hussain, Muhammad Shahzad Kamal, Abdullah S. Sultan
  • Publication number: 20230374368
    Abstract: A method of removing a sulfate scale from a surface is provided. The method includes contacting the sulfate-comprising scale with a conversion solution including 1 to 10 wt. % of an alkali metal carbonate, 0.5 to 10 wt. % of a borate salt or hydrate thereof, and 0.5 to 2.5 wt. % of a base to produce a carbonate-comprising scale. The method further includes exposing the carbonate-comprising scale with an acid solution including 2.5 to 25 wt. % of an acid.
    Type: Application
    Filed: August 3, 2023
    Publication date: November 23, 2023
    Applicant: King Fahd University of Petroleum and Minerals
    Inventors: Mohamed MAHMOUD, Muhammad Shahzad KAMAL
  • Patent number: 11795372
    Abstract: A method of removing a sulfate scale from a surface is provided. The method includes contacting the sulfate-comprising scale with a conversion solution including 1 to 10 wt. % of an alkali metal carbonate, 0.5 to 10 wt. % of a borate salt or hydrate thereof, and 0.5 to 2.5 wt. % of a base to produce a carbonate-comprising scale. The method further includes exposing the carbonate-comprising scale with an acid solution including 2.5 to 25 wt. % of an acid.
    Type: Grant
    Filed: February 14, 2022
    Date of Patent: October 24, 2023
    Assignee: King Fahd University of Petroleum and Minerals
    Inventors: Mohamed Mahmoud, Muhammad Shahzad Kamal
  • Publication number: 20230313023
    Abstract: A method, system, and drilling fluid for treating a wellbore for filter cake removal, including providing the drilling fluid having thermochemical reagents that are encapsulated and acid-generating material that is encapsulated into a wellbore in a subterranean formation to attack filter cake in the wellbore, and attacking the filter cake via the drilling fluid.
    Type: Application
    Filed: April 4, 2022
    Publication date: October 5, 2023
    Inventors: Ayman Raja Al-Nakhli, Mohamed Mahmoud, Zeeshan Tariq, Alade Olalekan Saheed, Muhammad Shahzad Kamal
  • Publication number: 20230138419
    Abstract: A surfactant of formula (I) wherein each of R1 and R2 are independently a hydrogen, an optionally substituted alkyl, an optionally substituted cycloalkyl, or an optionally substituted arylalkyl, R3 and R4 are independently an optionally substituted alkyl, an optionally substituted cycloalkyl, or an optionally substituted arylalkyl, x is an integer in a range of 2-8, y is an integer in a range of 1-15, z is an integer in a range of 4-10, n is an integer in a range of 2-5, and A is one of a carboxybetaine group, a sulfobetaine group, or a hydroxy sulfobetaine group. An oil and gas well servicing fluid containing the surfactant and methods of servicing an oil and gas well are also described.
    Type: Application
    Filed: December 23, 2022
    Publication date: May 4, 2023
    Applicant: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: S. M. Shakil HUSSAIN, Muhammad Shahzad KAMAL
  • Publication number: 20230132932
    Abstract: The invention concerns synthesized amido-amine-based cationic gemini surfactants with flexible and rigid spacers and different hydrophobic. These gemini surfactants were prepared by modified procedure through amidation of long chain carboxylic acids using 3-(dimethylamino)-1-propylamine followed by treatment with halohydrocarbons and showed excellent thermal stability and surface properties useful for various oilfield applications such as enhanced oil recovery.
    Type: Application
    Filed: November 3, 2022
    Publication date: May 4, 2023
    Applicant: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Syed M. Shakil HUSSAIN, Muhammad Shahzad KAMAL, Abdullah S. SULTAN
  • Publication number: 20230076912
    Abstract: A method of removing a sulfate scale from a surface is provided. The method includes contacting the sulfate-comprising scale with a conversion solution including 1 to 10 wt. % of an alkali metal carbonate, 0.5 to 10 wt. % of a borate salt or hydrate thereof, and 0.5 to 2.5 wt. % of a base to produce a carbonate-comprising scale. The method further includes exposing the carbonate-comprising scale with an acid solution including 2.5 to 25 wt. % of an acid.
    Type: Application
    Filed: February 14, 2022
    Publication date: March 9, 2023
    Applicant: King Fahd University of Petroleum and Minerals
    Inventors: Mohamed MAHMOUD, Muhammad Shahzad KAMAL
  • Patent number: 11566167
    Abstract: Amidoamine-based gemini surfactants having dual chains connected via an alkenylene or alkynylene linker. Each chain contains a quaternary ammonium head group and an ethoxylated alkyl tail. A water-based drilling fluid containing the gemini surfactant is also provided. As examined by linear swelling and free swelling tests, the gemini surfactant is effective in reducing clay swelling.
    Type: Grant
    Filed: December 18, 2019
    Date of Patent: January 31, 2023
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Muhammad Shahzad Kamal, S. M. Shakil Hussain, Mobeen Murtaza, Mohamed Mahmoud
  • Patent number: 11555143
    Abstract: A surfactant of formula (I) wherein each of R1 and R2 are independently a hydrogen, an optionally substituted alkyl, an optionally substituted cycloalkyl, or an optionally substituted arylalkyl, R3 and R4 are independently an optionally substituted alkyl, an optionally substituted cycloalkyl, or an optionally substituted arylalkyl, x is an integer in a range of 2-8, y is an integer in a range of 1-15, z is an integer in a range of 4-10, n is an integer in a range of 2-5, and A is one of a carboxybetaine group, a sulfobetaine group, or a hydroxy sulfobetaine group. An oil and gas well servicing fluid containing the surfactant and methods of servicing an oil and gas well are also described.
    Type: Grant
    Filed: January 22, 2020
    Date of Patent: January 17, 2023
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: S. M. Shakil Hussain, Muhammad Shahzad Kamal
  • Publication number: 20230001164
    Abstract: A method for monitoring a flowrate of cerebrospinal fluid (CSF) in a ventriculo-peritoneal (VP) shunt implanted in a human patient includes: (i) receiving, at a device external to the human patient, data sensed by a plurality of sensors within the device and positioned relative to the VP shunt to drain excess cerebrospinal fluid from the human patient's brain; (2) determining, by the device and based on the sensed data, a rate of flow of the CSF in the VP shunt; and (3) transmitting (e.g., wirelessly), by the device, data indicating the rate of flow to a computing server.
    Type: Application
    Filed: August 31, 2021
    Publication date: January 5, 2023
    Inventors: Muhammad Shahzad Shamim, Saleem Sayani, Syed Sarmad Bukhari, Muhammad Abdul Muqeet, Hafiz Imtiaz Ahmed
  • Patent number: 11512045
    Abstract: The invention concerns synthesized amido-amine-based cationic gemini surfactants with flexible and rigid spacers and different hydrophobic. These gemini surfactants were prepared by modified procedure through amidation of long chain carboxylic acids using 3-(dimethylamino)-1-propylamine followed by treatment with halohydrocarbons and showed excellent thermal stability and surface properties useful for various oilfield applications such as enhanced oil recovery.
    Type: Grant
    Filed: February 21, 2019
    Date of Patent: November 29, 2022
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Syed M. Shakil Hussain, Muhammad Shahzad Kamal, Abdullah S. Sultan
  • Patent number: 11459499
    Abstract: Amidoamine-based gemini surfactants having dual chains connected via an alkyl linker. Each chain contains a quaternary ammonium head group and an ethoxylated alkyl tail. Properties of the surfactant including thermal stability, critical micelle concentration, and foam stability are specified. A method of recovering oil from a reservoir using an aqueous composition that contains the surfactant and a polymer (e.g. AM-AMPS) is also provided. This method is particularly effective for oil recovery in reservoirs of high temperature and/or high salinity.
    Type: Grant
    Filed: September 27, 2019
    Date of Patent: October 4, 2022
    Assignee: King Fahd University of Petroleum and Minerals
    Inventors: Syed M. Shakil Hussain, Muhammad Shahzad Kamal
  • Patent number: 11447688
    Abstract: Methods of controlling clay swelling and stabilizing subterranean geological formations containing swellable clays (e.g., montmorillonite, bentonite) are described. The methods involve treating the swellable clays with a composition containing an amidoamine-based gemini surfactant. The gemini surfactant has dual chains connected via an alkylene linker, whereby each chain contains a quaternary ammonium head group and an ethoxylated alkyl tail. As examined by linear swelling and free swelling tests, use of the gemini surfactant is effective in reducing swelling of the clays.
    Type: Grant
    Filed: January 30, 2020
    Date of Patent: September 20, 2022
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Muhammad Shahzad Kamal, S.M. Shakil Hussain, Mobeen Murtaza, Mohamed Mahmoud