Abstract: The invention relates to Quench box assembly comprising quench pipe and quench box, to mix quench gas and vapor-liquid effluent from previous catalyst bed to achieve equilibrium temperature before entering the next bed. The quench pipe is in the form of ring having aperture while quench box consists of swirling section and a mixing chamber. The swirling section consists of inclined baffles to provide swirling action to incoming stream and the turbulence created by the swirling action increases the heat transfer rate thus requiring the smaller reactor volume to attain equilibrium temperature. The perforated plate being open from all the sides allowing the liquid to flow uniformly from all directions thus providing uniform distribution on the distributor tray. Hence, eliminates the requirement of rough liquid distributor before the distribution tray.

Abstract: The present invention relates to a method based on proton NMR technique to differentiate genuine and spurious Hand-rub formulations. This method identifies and estimates all four components present in WHO-recommended Hand-rub formulations. Further, this method also identifies the presence of non-recommended/additional components present in WHO-recommended Hand-rub formulations. The method described in this invention utilizes experimental parameters and derived equations to quantify all four components in just fifteen minutes without using any organic solvents.

Abstract: The present invention relates to a process for producing ultrahigh molecular weight polymer in powder form which is highly efficient drag reducing polymer. The process consists of polymerizing using titanium halide-based catalyst, co-catalyst, optionally a solvent, and monomer to a polymerization reactor, having stirring device and inlet charging and discharge outlet. The resulting ultrahigh molecular weight drag reducing polymers is free flowing, having intrinsic viscosity >10 dL/g. The process reduces polymerization time, temperature, and achieves high conversion, i.e., >90%.

Abstract: An advantageous process for pre-treating lignocellulosic biomass to hydrolysable polysaccharide enriched biomass with reduced amount of inhibitors of catalysis comprising steps of: providing a feedstock comprising cellulosic biomass; chopping of cellulosic biomass to have a cellulosic biomass feed material of uniform size; feeding of uniform sized feed material to a horizontal counter current extraction unit; removing excess of water from the feed material obtained from the extraction unit; soaking the extruded feed material obtained from the extraction unit; optionally removing excess of water from the feed material obtained after acid soaking; steam pre-treating the feed material obtained after removing excess of water from the acid soaked feed material; neutralizing the slurry obtained from the steam pre-treating; and optionally saccharifying the neutralized slurry.

Abstract: The present invention relates to an improved method of second generation ethanol production from a lignocellulosic biomass. The process comprises subjecting a slurry of pre-treated lignocellulosic biomass comprising C5 and C6 sugars in a fermentor; preferentially fermenting mainly C5 sugars by incubating the pretreated lignocellulosic biomass of step (i) with first cellulase enzyme, co-fermenting microorganism, nutrient in the fermentor at 30-37° C. for a period of 16 to 24 hours; adding second cellulase enzyme to the fermentation broth of step (ii) and increasing the temperature to 45-55° C. for hydrolysis; allowing the fermentation broth of step (iii) to cool to a temperature of 35-38° C.; and preferentially fermenting C6 sugars by incubating the broth of step (iv) with a second dose of co-fermenting microorganism for a period of 6-8 hours to obtain ethanol. The process results in high ethanol productivity in shortest duration of time.

Abstract: An apparatus for purifying impure hydrogen fuel is described that includes a first chamber and a second chamber. The first chamber is configured to receive impure hydrogen fuel in the form of a first mixture of gases with hydrogen gas and carbon monoxide at the first concentration while the second chamber is configured to receive a second mixture of gases with hydrogen gas at the second concentration. The apparatus also includes a solid-state electrolyte that separates the first chamber and the second chamber and includes an adsorbing catalyst. The apparatus also includes a pair of electrodes installed each in the first chamber and the second chamber to create a potential difference is created across the solid-state electrolyte.

Abstract: The present invention relates to a process for simultaneous production of citric acid and cellulolytic enzymes. The batch process comprising (i) adding slurry of a pre-treated lignocellulosic biomass or cellulose in a fermentation media; (ii) inoculating 10% (v/v) active liquid seed culture of Penicillium funiculosum MRJ-16 in the fermentation media of step (i); (iii) subjecting the culture of step (ii) to fermentation in an aerated fermenter at a temperature of 28-33° C. for a duration of 96 hours; and (iv) collecting enzyme broth after fermentation of step (iii) to obtain citric acid and cellulolytic enzymes. The batch and fed-batch process of the present invention results in high titer production of citric acid and cellulolytic enzymes in a single step and using single microbial strain.

Abstract: The present invention relates to an apparatus and method for bio-assisted treatment of spent caustic obtained from hydrocarbon and gas processing installations. The present invention also relates to method for recovery of caustic and recovery of sulfur from spent caustic. According to present invention, the sulfide removal is about 96% and the sulphur formation and deposition on the electrode lies in range of 72±8%.

Abstract: The present invention relates to a novel process with lower recycle ratio while eliminating the need for quench column for production of superior quality coke conforming to specifications of anode grade coke. The process of the present invention enables production of lower amounts of coke and fuel oil yields.

Abstract: The invention relates to a device and process for converting organic waste to biogas with high methane content and improved organic conversion efficiency. Disclosed process consists of two stages and in the first stage, shredded organic waste is digested in primary digester in which biodegradable organic fractions present in waste gets converted to volatile fatty acids and alcohols dissolved in aqueous solution by hydrolytic and acidogenic microorganisms. Primary digester effluent pH, is adjusted to about 6.8-7.5 by addition of controlled alkali solution. Neutralized waste slurry is separated into liquid solution called as leachate and digested solid sludge. In the second stage, liquid leachate comprising volatile fatty acids are converted to biogas with methane content in the range 80-86% by methanogenic microbial culture in main digester under anaerobic conditions.

Abstract: A caliper pig for detecting geometrical deformation of a pipeline is disclosed. The caliper pig includes a body and a first sensor arm assembly. The first sensor arm assembly includes a primary caliper sensor ring adapted to be mounted on the body. Further, the first sensor arm assembly includes a plurality of sensor arms adapted circumferentially distributed on the primary caliper sensor ring. Each of the plurality of sensor arms includes a sensing arm adapted to be in contact with an internal surface of the pipeline and a pair of magnets adapted to rotate along the sensing arm. Each of the plurality of sensor arms includes a sensing unit configured to detect a change in magnetic field based on the movement of the sensing arm. The sensing unit is configured to generate an output indicative of an angle of deflection of the sensing arm while traversing on the internal surface of the pipeline.

Abstract: The present invention relates to a biomimetic-hybrid solvent system for simultaneous capture of H2S and CO2 from any gaseous composition. The present invention also relates to a process for upgradation of biogas to bio CNG by removing gaseous contaminants, including microbial removal of H2S, to obtained purified CO2. The biomimetic-hybrid solvent system contains three components selected from tertiary amine compounds, a functional colloidal fluid, and an enzyme mimic.

Abstract: The invention relates to a process configuration for production of light olefins and aromatics from residual hydrocarbon streams. In this configuration a high severity catalytic cracking process is employed for producing higher yields of lighter olefins and various boiling fractions. C4 stream separated from gaseous product is subjected to metathesis and aromatized to form mono aromatics.

Abstract: The present invention relates to a method for reducing or preventing the formation or activity of a corrosion-associated biofilm on a metal surface, wherein the method comprises contacting the metal surface with a liquid composition comprising biocidal preparation. The present invention also relates to a microbicidal composition comprising at least one alcohol, one liquid hydrocarbon, a bacteriophage immobilized on a magnetic nanocomposite, at least one phage releasing reagent and one stabilizer. The microbicide composition and method of the present invention reduces biofilms on surfaces, and consequently, reduces, mitigates, or eliminates MIC in internal surface of the oil transporting pipelines.

Abstract: A delayed coking furnace (100) for heating coker feedstock (101) is disclosed. The furnace (100) includes a first heating zone (102) adapted to provide heat to the coker feedstock (101) through a convective heat transfer and then a second heating zone (104) positioned below the first heating zone (102) and adapted to heat the coker feedstock (101) through radiative heat transfer, wherein the second heating zone (104) include a lower portion and an upper portion. Further, said furnace (100) includes a plurality of burners (106) located at the lower portion of the second heating zone (104) and at least one baffle (111) disposed in the upper portion of the second heating zone (104). Further, the present disclosure provides that the at least one baffle (111) is adapted to increase a convective heat transfer coefficient associated with a flue gas flowing from the second heating zone (104) to the first heating zone (102).

Abstract: The present invention discloses a single package additive for improving lubricity and conductivity properties of ultra-low sulfur diesel fuels. The single package additive is a reaction product of a fatty acid composition, a glycerol tricarboxylates, a polysulfone, a polyamine, an alkylated benzene sulfonic acid and a phenol derivative. More specifically, the present invention discloses a reaction product of: a fatty acid composition in the range of 60-95% wt/wt; a glycerol tricarboxylate in the range of 0.1-10.0% wt/wt; a polysulfone in the range of 0.1-5.0% wt/wt; a polyamine in the range of 0.1-5.0% wt/wt; an alkylated benzene sulfonic acid in the range of 0.1-5.0% wt/wt; and a phenol derivative in the range of 0.1-10.0% wt/wt. The present invention also discloses a single-pot process for the preparation of said reaction product.

Abstract: The present invention relates to a method of cellulases enzymes production by Penicillium funiculosum MRJ-16 using minimum media components and/or low cost media components like cellulose or pretreated lignocellulosic biomass as carbon source and soya flour or defatted soya flour or de-oiled soya cake as nitrogen source. The present invention also provides a method for production of high titer of cellulases and hemicellulases enzymes using Penicillium funiculosum MRJ-16 using minimum media and/or low cost media components.

Abstract: The invention relates to a method of the oligomerization of C6 and above olefin monomer whereby, at a fixed monomer/Al halide mole ratio, polyalphaolefins having desirable kinematic viscosities are prepared by controlling the oligomerization temperature. The oligomerization is carried out in presence of an oligomerizing catalyst comprising of aluminum halide and a promoter, and oligomerizing temperatures of about 10° C. to about 120° C.

Abstract: An inlet diffuser for the fixed-bed reactor is disclosed. The inlet diffuser comprises a truncated cone adapted to receive a stream of gas-liquid mixture. The truncated cone includes at least one opening formed on a circumference of the truncated cone. Further, the inlet diffuser comprises a vertical baffle plate in each of the openings and at least one horizontal baffle coupled to the truncated cone to absorb momentum of the stream received by the truncated cone. Furthermore, it comprises a cylindrical chamber in fluid communication with the truncated cone and adapted to receive the stream from the truncated cone. The cylindrical chamber includes at least one slot to discharge the stream from the inlet diffuser and a splash plate is disposed at a bottom portion of the cylindrical chamber with apertures to discharge the stream from the inlet diffuser.

Abstract: Organic sulfur compounds which are generally present in the crude oil undergoes various transformations while processing the crude oil in the secondary processing units such as fluid catalytic cracker, hydrocracker, delayed coker, visbreaker, etc. The sulfur present in the feed which enters into these secondary processing units are distributed into various products coming out of the units. Sulfur compounds which are present in the various product fractions are removed to meet the desired specifications before routing to the final product pool. Conventionally, sulfur present in the LPG has been removed by amine treatment followed by caustic and water wash. The present invention relates to a process for removal of sulfur and other impurities from Liquefied Petroleum Gas (LPG) comprising olefins through reactive desulfurization route. The present invention is an eco-friendly process as it minimizes or eliminates the use of caustic which is conventionally used to remove the sulfur from LPG.