Rubber composition and pneumatic tire using the rubber composition
The present invention provides a rubber composition comprising natural rubber and/or diene synthetic rubbers, silica in an amount of 10 to 85 parts by weight per 100 parts by weight of the rubber, a specific silane coupling agent, i.e., a bis-(alkoxysilylalkyl) polysulfide having a polysulfide structure in which the distribution of sulfur is specified, in an amount of 1 to 20% by weight of the amount of silica, and provides a pneumatic tire manufactured by using the rubber composition. The pneumatic tire has excellent low heat buildup property, low rolling resistance, and reinforcing property.
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Claims
1. A rubber composition which comprises a rubber component comprising
- at least one member selected from the group consisting of natural rubber and diene synthetic rubbers; silica in an amount of 10 to 85 parts by weight per 100 parts by weight of the rubber component; and in an amount of 1 to 20% by weight of the amount of silica, a silane coupling agent represented by the following general formula:
- wherein n represents an integer of 1 to 3, m represents an integer of 1 to 9, y represents a positive number of 1 or more having a distribution, the distribution of --S.sub.y -- satisfying the relation:
- and the content of component S.sub.3 is 19.4% or more.
2. A rubber composition according to claim 1, wherein the distribution of --S.sub.y -- satisfies the relation:
3. A rubber composition according to claim 1, wherein the distribution of --S.sub.y -- satisfies the relation:
4. A rubber composition according to claim 1, further comprising 80 parts by weight or less of carbon black as a reinforcing filler per 100 parts by weight of the rubber component.
5. A rubber composition according to claim 2, further comprising 80 parts by weight or less of carbon black as a reinforcing filler per 100 parts by weight of the rubber component.
6. A rubber composition according to claim 3, further comprising 80 parts by weight or less of carbon black as a reinforcing filler per 100 parts by weight of the rubber component.
7. A rubber composition according to claim 1, wherein anhydrous sodium sulfide (Na.sub.2 S) and sulfur (S) are reacted with each other in a mol ratio in a range of 1:1 to 1:2.5 in an atmosphere of an inert gas in a polar solvent to obtain sodium polysulfide, the obtained sodium polysulfide is reacted in an atmosphere of an inert gas with a halogenoalkoxysilane represented by the following general formula: ##STR3## wherein R.sup.1 and R.sup.2 each represents an alkyl group having 1 to 3 carbon atoms, R.sup.3 represents a divalent hydrocarbon group having 1 to 9 carbon atoms, X represents a halogen atom, and k represents an integer of 1 to 3, and the obtained compound is used as the silane coupling agent.
8. A rubber composition according to claim 2, wherein anhydrous sodium sulfide (Na.sub.2 S) and sulfur (S) are reacted with each other in a mol ratio in a range of 1:1 to 1:2.5 in an atmosphere of an inert gas in a polar solvent to obtain sodium polysulfide, the obtained sodium polysulfide is reacted in an atmosphere of an inert gas with a halogenoalkoxysilane represented by the general formula of claim 7, and the obtained compound is used as the silane coupling agent.
9. A rubber composition according to claim 3, wherein anhydrous sodium sulfide (Na.sub.2 S) and sulfur (S) are reacted with each other in a mol ratio in a range of 1:1 to 1:2.5 in an atmosphere of an inert gas in a polar solvent to obtain sodium polysulfide, the obtained sodium polysulfide is reacted in an atmosphere of an inert gas with a halogenoalkoxysilane represented by the general formula of claim 7, and the obtained compound is used as the silane coupling agent.
10. A pneumatic tire which is manufactured by using the rubber composition described in claim 1 for tread rubber.
11. A pneumatic tire which is manufactured by using the rubber composition described in claim 2 for tread rubber.
12. A pneumatic tire which is manufactured by using the rubber composition described in claim 3 for tread rubber.
13. A pneumatic tire which is manufactured by using the rubber composition described in claim 4 for tread rubber.
14. A pneumatic tire which is manufactured by using the rubber composition described in claim 5 for tread rubber.
15. A pneumatic tire which is manufactured by using the rubber composition described in claim 6 for tread rubber.
16. A pneumatic tire which is manufactured by using the rubber composition described in claim 7 for tread rubber.
5580919 | December 3, 1996 | Agostini et al. |
5029741 | September 1975 | JPX |
5120208 | June 1976 | JPX |
3252431 | November 1991 | JPX |
7228588 | August 1995 | JPX |
A10732362 | September 1996 | JPX |
- Chem Abstract 128:116176 "Rubber Compositions and Pneumatic Tires Procduced Therefrom Draki et al."
Type: Grant
Filed: Aug 25, 1997
Date of Patent: Sep 7, 1999
Assignee: Bridgestone Corporation (Tokyo)
Inventors: Shunji Araki (Tokyo), Kazuhiro Yanagisawa (Tokyo)
Primary Examiner: Duc Truong
Law Firm: Sughrue, Mion, Zinn, Macpeak & Seas, PLLC
Application Number: 8/917,234
International Classification: C08J 532; C08K 524;