Circular secondary clarifier for wastewater treatment and an improved solids-liquid separation process thereof
The improved circular secondary clarifier of the present invention requires less surface area and low HRT and provides efficient solids-liquid separation. The improved clarifier has better SS and BOD reduction and provides high under flow solids concentrations, as compared to conventional secondary clarifiers. The improved clarifier is even capable of treating wastewaters containing low MLSS concentration. One of the biggest advantages of improved clarifier is that it does not require a separate sump cum pump house as it removes the settled sludge using suction mechanism thereby reduces capital and recurring cost. Further, it provides natural flocculation, which is essential for agglomeration of solids and increases particle size referred to as ‘floc’ and eliminates provision for a separate flocculation facility thereby reduces capital and recurring costs.
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The present invention relates to “An Improved Circular Secondary Clarifier for Wastewater Treatment and an Improved Solids-liquid Separation Process Thereof”. The improved circular secondary clarifier of the present invention enables treatment of wastewaters having suspended solids (SS) concentration in the range 500-5000 mg/l and above, and provides improved solids-liquid separation and enhanced biochemical oxygen demand (BOD) reduction with reduced surface area and low hydraulic retention time (HRT). The improved circular secondary clarifier capable of removing up to 99% of SS also ensures, high under flow solids concentration in the range 15000-17000 mg/l, to be returned to aeration tank using sludge removal suction mechanism. The improved circular secondary clarifier also increases particle size referred to as ‘floc’ through natural flocculation and does not require separate flocculation facility.
BACKGROUND AND PRIOR ARTA conventional circular secondary clarifier for treatment of wastewaters as depicted in
The design of secondary clarifier is primarily based on solids loading rate (SLR) and surface overflow rate (SOR) usually expressed in kg/m2.d and m3/m2.d, respectively. The surface area of clarifier, for a given solids concentration (expressed in mg/l) and flow rate (expressed in m3/d) is governed by above-referred parameters (SLR, SOR), and the greater of the two is provided.
Reference may be made to Wastewater Engineering, Treatment and Reuse IV edition (2003), Metcalf & Eddy Inc., wherein the average SLR and SOR for clarifier following extended aeration unit, range from 1 to 5 kg/m2.hr (24 to 120 kg/m2.d) and 8 to 16 m3/m2.d, respectively, and the depth of clarifier varies from 3.5-6 m. Under these conditions, for a conventional clarifier, the surface area required for a given flow rate is more as compared to the improved clarifier, described in the present invention. Further, the recommended depth of conventional clarifier is also on the higher side, as compared to the improved clarifier described in the present invention. In other words, the design parameters for a clarifier, viz. SLR and SOR, can be reset to higher ranges to obtain a compact clarifier, which is capable of providing improved solids-liquid separation. However, in the conventional clarifiers it is not feasible to provide higher ranges for design parameters (SLR, SOR) due to the problem of effective solids-liquid separation.
Reference may be made to “Clarifier Design Manual of Practice, FD-8, WPCF, (1985, 2005)”, wherein the various conventional circular secondary clarifiers comprising center and peripheral feed arrangements with flow patterns are shown. In the clarifiers with central feed arrangement, the diameter of feed well is about 20-25% of the diameter of the clarifier, which in turn reduces the surface area for clarification. Therefore to account for diameter of feed well, the diameter of clarifier is increased by 20-25%, which increases the capital cost of the unit, whereas in the improved clarifier described in the present invention, the surface area required is less, as no feed well is provided. Conventionally, the solids enter the clarifier through a high level inlet (3), get dispersed immediately and mostly settle as individual solid. Some times, therefore to increase the floc size, a flocculation mechanism is also provided (not shown). This in turn increases the size and cost of the clarifier, whereas that described in the present invention, the floc size increases due to natural flocculation, and solids settle as a zone of sludge layer uniformly.
In the conventional peripheral feed type of clarifiers, the wastewater is fed through inlet ports all along the perimeter or through spiral roll pattern by introducing the flow into the clarifier near the bottom, wherein the flow pattern induced may carry away the solids accumulated at the bottom along with the incoming wastewater, thereby resulting in higher SS concentrations in the treated effluent. Further, the peripheral feed clarifiers with open ports or orifices have inherent problem of unequal distribution as flow changes, whereas in the improved clarifier described in the present invention, the flow is uniformly distributed, ensuring uniform thickening of sludge layer at the bottom of the clarifier.
Reference may be made to U.S. Pat. No. 4,005,019 (1977) wherein the disclosure relates to rectangular clarifiers for use in the gravity separation of suspended solids from liquids. The invention basically relates to the apparatus used in the gravity separation of suspended solids from liquids, comprising a gantry supported for movement above the liquid surface; gantry drive to cause the gantry to perform repeated passes over the said liquid surface; a sludge conveyor device to move sludge which has settled at the bottom of the clarifier. The gravitational separator described in the above-referred US patent clearly indicates that the invention is related to sludge removal mechanism for rectangular clarifiers and does not include measures like hydraulic energy dissipation and improved geometrical configuration to improve solid-liquid separation described in the present invention.
Reference may be made to U.S. Pat. No. 4,761,239 (1988), wherein the process for wastewater purification is disclosed, which is particularly suitable for raw wastewater clarification by reducing BOD and SS concentrations employing sequential addition of chemicals, viz. salts of aluminium, iron or copper or composition thereof, followed by addition of fly-ash upstream of primary clarifier and downstream of salt feed to increase the dry solids content of the influent raw wastewater by 10-50%, and then finally adding water soluble, surface active, branched polyether amine compound having specific gravity of 1.08, to the raw wastewater, upstream of the primary clarifier and downstream of the feed point of fly ash, in an amount sufficient to increase the settling rate of sludge forming material, and clarify the effluent water at the top of primary clarifier.
In the above process, the clarification is mainly achieved by sequential addition of chemicals, polymers and fly ash rather than the gravity clarification occurring in the clarifier itself. External addition of solids in the raw wastewater not only increases the size of clarifiers to accommodate increased sludge blanket, but also requires large sludge dewatering facilities. Further, the management of solids handling and disposal becomes tedious and means additional recurring cost due to increase in quantity of sludge generated, whereas the clarifier described in the present invention, can be used for primary clarification of raw wastewater without addition of fly ash.
Reference may be made to U.S. Pat. No. 5,306,422 (1994), which discloses a compact clarifier system for municipal wastewater treatment. The clarifier system is in general based on the principles of dissolved air floatation (DAF), wherein compressed air is released at the bottom of the tank in the form of microscopic bubbles that attach to the suspended solids, the bubbles carry the solids to the surface, where they form floating sludge. The method disclosed in the above-referred patent is energy intensive and requires highly skilled supervision as compared to method described in the present invention. The solids-liquid separation described in the present invention is based on the principle of gravitation, wherein solids and liquid are separated under quiescent condition, due to difference in specific gravity.
Reference may be made to U.S. Pat. No. 5,961,826 (1999) wherein a biological wastewater treatment system having a sedimentation tank vertically combined with an aeration tank has been disclosed. The inventors claim a sedimentation tank vertically combined with an upside aeration tank and connected with the said aeration tank through a through-hole, the sedimentation tank having a clarified water outlet for discharge of clarified water from the sedimentation tank. This system is only suitable for small-scale treatment plants, since such an installation is not feasible for large-scale wastewater treatment systems. Further, the treatment system described in the U.S. Pat. No. 5,961,826 does not claim any improvement in solids-liquid separation described in the present invention.
Reference may be made to U.S. Pat. No. 6,099,743 (2000) wherein a method and basin for sedimentation of solids in wastewater treatment has been disclosed. The method of removing solids from wastewater by flocculation comprises of forcing a flow of sludge containing wastewater to abruptly change direction a number of times in succession to form whirls that create an optimum velocity for formation of sludge flocs. A method and basin for sedimentation is suitable for a designed flow rate in order to obtain optimum velocity to promote flocculation; any change in the incoming flow rate will change the optimum velocity which will affect flocculation as described in the above referred invention, hence requires highly skilled supervision, whereas in the improved clarifier, the resistance to flow is offered gradually by solids itself as described in the present invention.
OBJECTS OF THE INVENTIONThe main object of the present invention is to provide an improved circular secondary clarifier for wastewater treatment and an improved solids-liquid separation process thereof, which obviates the drawbacks of the hitherto known prior art as detailed above.
Another object of the present invention is to provide an improved circular secondary clarifier having reduced surface area and operating at low HRT and achieving enhanced solids-liquid separation and BOD reduction.
Still another object of the present invention is to provide an improved secondary clarifier that ensures high underflow solids concentration thereby reducing the sludge recycle rate to maintain an active biomass concentration in aeration tank.
Yet another object of the present invention is to provide an efficient sludge removal suction mechanism for recycling of thickened sludge to aeration tank. Still another object of the present invention is to provide this advantage at a substantial cost savings, capital and operational, as compared to conventional clarifier wherein sump cum pump house is essentially required.
Another and related object of the present invention is to provide an improved circular secondary clarifier capable of handling peak loads while also meeting some prescribed Standards.
SUMMARY OF THE INVENTIONThe improved circular secondary clarifier of the present invention requires less surface area and low HRT, and provides efficient solids-liquid separation. The improved clarifier has better SS and BOD reduction and provides high under flow solids concentrations, as compared to conventional secondary clarifiers. The improved clarifier is even capable of treating wastewaters containing low MLSS concentration. One of the biggest advantages of improved clarifier is that it does not require a separate sump cum pump house as it removes the settled sludge using suction mechanism thereby reduces capital and recurring cost. Further, it provides natural flocculation, which is essential for agglomeration of solids, thus eliminates provision for a flocculation mechanism. Following points bring out the novelty and non-obvious inventive steps of the present invention:
-
- Provision of a low level inlet, being enlarged to dissipate the hydraulic energy of incoming wastewater.
- Formation of plume, just above the inlet and extending vertically upwards to some distance.
- Plume formation is indication of natural flocculation and dissipation of hydraulic energy, which in turn indicates that quiescent condition, is prevailing in the clarifier.
- The plume, comprising of dense flocs, being heavier than wastewater, settle as one unit or zone at the bottom of clarifier.
- The clarifier bottom is sloped outwards (i.e. away from the centre of clarifier), which helps in accumulating more dense sludge uniformly towards the outer edge, at the bottom of clarifier.
- The settled sludge is removed uniformly using a suction mechanism without disturbing the settled sludge, thereby preventing the solids to come in re-suspension.
- Provision of a circular baffle wall as a precautionary measure, to prevent escape of solids, in case some air bubbles find way into the plume and burst at the top, thereby disturbing the plume. The baffle wall helps in containing the plume within its diameter under such circumstances, thereby restricts escape of solids along with the treated effluent.
In an embodiment of the present invention, a circular secondary clarifier connected through a low level inlet (13), capable of providing steady uniform flow being gradually enlarged at the outlet (14), is capable of dissipating the hydraulic energy substantially.
In yet another embodiment of the present invention, the bottom (20) having slope 1 in 10, towards the outer edge of the clarifier is provided to ensure uniform distribution of sludge.
In still another embodiment of the present invention a sludge removal mechanism comprising non return valve (21A), vertical rod (21B) connecting the suction manifold tubes (21) and the platform (24), sludge scrapper (21C), suction pump (22), rotor gear arrangement (23), sludge rotation fixture (29) connected to sludge outlet (30) is provided to ensure complete removal of sludge.
The present invention is illustrated through
13—inlet for conveying wastewater containing MLSS, 14—gradually enlarged inlet for hydraulic energy dissipation, 15—baffle wall, as a precautionary measure to prevent escape of solids, 16—triangular notch, for uniform flow distribution, 17—effluent collection channel (Launder), 18—treated effluent outlet, 19—sludge blanket, 20—bottom slope 1 in 10, for uniform sludge distribution and storage, 21—suction tube manifold for sludge removal, 21-A—non return valve for sludge removal, 21-B—support rod for tube manifolds, 21-C—scraper for transporting sludge to outer edges, 22—suction pump for pumping the settled sludge, 23—rotor gear arrangement for rotating sludge removal mechanism, 24—platform for rotor and suction pump, 25—platform rotation fixture, 26—columns, to provide support for rotating bridge, 27—wheel, 28—rail section, 29—rotation fixture for electric supply and sludge line, 30—sludge outlet to aeration tank or thickening, 31—valves for dewatering, 32—sludge clouds (plume).
In
33—initial liquid level, 34—settled solids
In
35—liquid level after some time, 36—plume, 37—sludge blanket
In
38—maximum liquid level, 39—sludge blanket, 40—plume.
DETAILED DESCRIPTION OF THE INVENTIONAccordingly, the present invention provides an improved circular secondary clarifier for wastewater treatment and an improved solids-liquid separation process thereof wherein the wastewater containing MLSS passes through a low level inlet (13) being gradually enlarged (14), to dissipate substantial hydraulic energy of the incoming wastewater, a sludge (solids) cloud named as plume (32,36,40) is formed as a result of hydraulic energy dissipation and resistance to incoming flow offered by the bulk mass of solids thereby providing natural flocculation at the central lower portion to increase the floc size and obtaining absolute quiescent conditions in clarification zone, the plume (32,36,40) comprising high solids concentration being dense, settles quickly as one unit at the bottom (20), which is sloped outward and forms a sludge blanket (19,37,39) all along the clarifier, the settled sludge (19) is removed uniformly using suction mechanism comprising a suction pump (22) and suction tube manifolds (21), a non return valve (21-A), a sludge scraper (21-C) being connected to platform (24) through a rod (21-B) and discharged to either aeration tank (not shown) or sludge thickening (not shown) through a stationary sludge outlet (30), the platform (24) being supported on columns (26) through rotation fixture (25), at the centre and other ends of platform (24) being supported on peripheral rail section (28) through a wheel (27) and rotated through rotor gear (23), a baffle wall (15) provided as a precautionary measure to prevent escape of solids, in case some air bubbles come along with the wastewater that disturb the plume (32), two dewatering valves (31) are provided diametrically opposite to remove sludge under hydrostatic pressure, the treated effluent (18) separated from solids, the treated effluent (18) rises in the clarifier and collected uniformly in the launder (17) through triangular notches (16) thereby obtaining clarified treated effluent.
An improved circular secondary clarifier of the present invention as depicted in
The improvement in the secondary clarifier and solids-liquid process due to non-obvious inventive steps resulting in an improved secondary clarifier for wastewater treatment has been described below:
The wastewater containing MLSS enters in clarifier through a low level inlet (13) that is gradually enlarged at the outlet (14) to distribute the wastewater uniformly all over the bottom (20). Gradual increase in pipe diameter reduces velocity of the incoming wastewater thereby reducing hydraulic energy and prevents jetting thus uniformly distributing wastewater at the bottom (20).
The flocs further form a sludge cloud referred to as plume (36), which rises vertically upwards to some distance. The plume comprising of flocs, being heavier than the wastewater and after having lost substantial hydraulic energy, does not have any option, than to settle at the bottom (20) of clarifier. The plume settles as one unit, all over the bottom and is carried away towards the outer edges and forms sludge blanket (37). Initially, gradually enlarged outlet (14) dissipates the hydraulic energy of the incoming wastewater and then the bulk mass of dense solids present in the plume offers resistance to incoming flow thereby further reducing the hydraulic energy. The formation of plume (32, 36) and hydraulic energy dissipation go hand-in-hand, the plume helps in dampening the velocity of solids presents in the wastewater and the solids help in forming the plume. Formation of a well-defined plume (32, 36) indicates absolute quiescent conditions are prevailing in the clarifier, and therefore an indication of efficient solids-liquid separation. The solids are thus separated from liquid and settle uniformly and form sludge blanket (19,37) at the bottom of clarifier. The liquid separated from solids, keeps rising in the clarifier as shown in
The sludge removal mechanism as shown in
The entire assembly consisting of suction mechanism (21, 21-A, 21-B, 21-C), suction pump mechanism (22), connected to platform (24) was rotated through a rotor gear arrangement (23). The rotor gear arrangement was made of 12 V, 6 rpm DC reduction motor. The rotational speed of motor was reduced to 2 revolutions per hour (rph) using reduction gears. The rotor gear arrangement (23) was connected to one of the wheels (27), which drove the entire assembly. Both the (DC) motors were provided continuous electric supply through a commutator, an attachment connected with the armature of a motor, through which electrical contact is made and which ensures the current flow as direct current. The commutator was made of copper foil. A transformer was used to reduce voltage from 230 to 12 V. The 12 V direct current was converted to 12 V alternate current (AC) through a rectifier. The sludge removal mechanism was designed and fabricated to remove sludge (19) from all around the clarifier and discharging it from a stationary outlet (30).
The following example is given by way of illustration of the working of the invention in actual practice, and therefore should not be construed to limit the scope of the present invention.
EXAMPLE 1An optimized bench scale reactor of improved circular secondary clarifier was prepared using transparent Perspex cylinder of thickness 6 mm and internal diameter 430 mm and polycarbonate flexible sheet of thickness 2 mm. The influent pipe was made of glass tube of internal diameter 4 mm and thickness 1 mm and the tube diameter was gradually enlarged to 12 mm diameter over a length of 30 mm. The bottom of reactor was made of flexible polycarbonate sheet giving a slope of 1 in 10, away from the center. The water depths in the reactor at center and edges were 15 and 18 cm, respectively. The surface area of reactor was 0.1452 m2 and the volume was 24 L. The effluent collection channel called as launder was made of transparent Perspex ring and flexible polycarbonate sheet. The internal and external diameters of the ring were 432 and 460 mm respectively and the launder side wall was made of polycarbonate sheet of thickness 2 mm. A treated effluent outlet made of glass tube of internal diameter 12 mm was provided at the lower most portion of the launder to collect the treated effluent. A suction removal mechanism consisting of suction pump, rotor gear assembly, rotation fixture and suction tube manifolds was provided to remove the settled sludge from the clarifier bottom.
EXAMPLE 2The wastewater containing MLSS enters in clarifier through a low level inlet (13) that is gradually enlarged at the outlet (14) to distribute the wastewater uniformly all over the bottom (20). Gradual increase in pipe diameter reduces velocity of the incoming wastewater thereby reducing hydraulic energy and prevents jetting thus uniformly distributing wastewater at the bottom (20). The hydraulic energy of the incoming wastewater is substantially reduced due to gradual increase in feed pipe diameter and liquid level (33) starts increasing in the clarifier allowing the solids (34) to be accumulated at the bottom (20) towards the outer edges of clarifier. When the liquid level (35) starts rising the solids present in wastewater collide with each other just above the gradually enlarged outlet (14), thereby undergoing natural flocculation and form bigger solids referred to as flocs. The flocs further form a sludge cloud referred to as plume (36), which rises vertically upwards to some distance. The plume comprising of flocs, being heavier than the wastewater and after having lost substantial hydraulic energy, does not have any option, than to settle at the bottom (20) of clarifier. The plume settles as one unit, all over the bottom and is carried away towards the outer edges and forms sludge blanket (37). The liquid separated from solids, keeps rising in the clarifier just above the weir crest (20) and starts overflowing uniformly and collected in the effluent collection channel (17). The sludge (39) settled at the bottom (20) is removed using suction pump (22) at 4 litres per hour and suction manifold tubes (21), 21-A—Non return valve for sludge removal, 21-B—Support rod for tube manifolds, 21-C—Scraper for transporting sludge to outer edges, 22—suction pump for pumping the settled sludge, 23—rotor gear arrangement for rotating sludge removal mechanism, 24—platform for rotor and suction pump, 25—platform rotation fixture, 26—columns, to provide support for rotating bridge, 27—wheel, 28—rail section, 29—rotation fixture for electric supply and sludge line, 30—sludge outlet to aeration tank or thickening, 31—valves for dewatering, 32—sludge clouds (plume). and discharged to aeration tank or sludge thickening through sludge outlet (30), suction pump being rested on a rotating platform (24) which rotates at the rate of 2 revolution per hour.
EXAMPLE 3The reactor was subjected to various solids concentrations 500-5000 mg/L, and flow rates giving variable HRT ranging from 1.0-1.5 hrs. The various parameters, viz. effluent SS and BOD, Return activated sludge (RAS) concentration, SS profile and particle size analysis at various depths along the radius of the clarifier were carried out to arrive at the optimized performance of the secondary clarifier. Table 1 shows the performance of an improved bench scale secondary clarifier and Table 2 presents a comparison of an improved and conventional secondary clarifier after scale up. The effluent parameters with respect to SS, as shown in Table 1 are well within the prescribed Standards and the RAS concentrations are also high as compared to conventional clarifier. The effluent SS concentrations obtained from improved clarifier are less than those obtained from settling studies carried out in 1 L cylinder, which clearly indicates that the clarifier has capability of providing natural flocculation that increases the particle size, thereby ensuring rapid settling of heavier particles. An analysis of SS profile and particle size along the radius at various depths indicates that solids concentration and mean particle diameter is much higher within the plume as compared to the area outside the plume. For wastewaters, with MLVSS 3000 mg/L and average particle diameter 42 μm, the solids concentration in the plume ranges from 4500-5200 mg/L and the particle diameter varies from 85-100 μm. Increase in solids concentration and particle diameter occurs as a result of formation of plume, which in turn is formed due to collision of particles (natural flocculation) and hydraulic energy dissipation. A comparative study presented in Table 2 shows that the improved circular secondary clarifier requires less surface area and depth and hence operates at low HRT, as compared to the conventional secondary clarifier. The improved clarifier also ensures high RAS and low SS concentrations in the treated effluent under the design parameters mentioned in Table 2.
The improved circular secondary clarifier is capable of providing effective separation in wastewaters containing biological solids (MLSS), wherein the difference in densities of solids and liquid is very less. For effective solids-liquid separation, it is essential that a well-defined plume is formed, which settles as one unit. Formation of a plume is an indication of natural flocculation and prevailing of quiescent conditions in the clarification zone.
The main advantages of the present invention are:
- 1. An improved solids-liquid separation is obtained, thereby ensuring minimum SS concentration in the treated effluent.
- 2. High underflow solids concentration is obtained that minimizes pumping rate, and maintains desired active biomass concentration in aeration tank.
- 3. It requires less surface area and depth and operates at low HRT, thereby facilitates savings in capital cost.
- 4. The improved clarifier does not require a separate sump cum pump house for sludge recycling/removal, thereby saves capital and recurring costs.
- 5. The improved secondary clarifier provides natural flocculation and does not require separate flocculation facility, thereby reduces capital and recurring cost.
Claims
1. A circular secondary clarifier for wastewater treatment, which comprises
- (a) a circular confinement wall,
- (b) a circular bottom wall sloping outwardly and downwardly from a center thereof and joined at outer edges thereof with lower portions of said confinement wall to form a containment vessel,
- (c) a low level wastewater inlet duct positioned below said bottom wall and having an upwardly opening outlet at the center of, and substantially at the level of said bottom wall for the discharge of wastewater upwardly into said containment vessel,
- (d) a confinement baffle structure positioned centrally in upper portions of said vessel, spaced above said sloping bottom wall and said outlet,
- (e) said baffle structure being positioned in alignment with a flow of wastewater discharged from said outlet and being operative to substantially confine a plume of solids formed in upwardly flowing liquid discharged from said outlet, whereby said solids are caused to settle downward toward said bottom wall,
- (f) a rotatable scraper positioned in close relation to central portions of said bottom wall and operative to distribute solids on said central portions radially outward on said bottom wall,
- (g) a suction manifold positioned over radially outer portions of said bottom wall,
- (h) said suction manifold being associated with said scraper and being rotatable therewith over said bottom wall,
- (i) a suction pump connected to said suction manifold through a non-return valve and operative to withdraw settled sludge resting on said bottom wall from said containment vessel,
- (j) a support structure positioned at an upper portion of said containment vessel and connected to and supporting said scraper and said suction manifold, and
- (k) a drive motor for controllably rotating said support structure and thereby said scraper and said suction manifold.
2. A circular secondary clarifier according to claim 1, characterized by said low level inlet duct, being gradually enlarged at the outlet thereof to substantially dissipate the hydraulic energy of inflowing wastewater.
3. A circular secondary clarifier according to claim 1, characterized by the bottom slope of 1 in 10, towards outer edge portions.
4. A circular secondary clarifier according to claim 1, characterized by said baffle structure being of cylindrical form and of size to prevent escape of solids and to contain the plume within its diameter.
5. A circular secondary clarifier according to claim 1, further including a platform, a rotation fixture supporting a central portion of said platform, a circular peripheral rail extending about upper edge portions of said confinement wall, one or more support wheels mounted at outer portions of said platform and supported by said peripheral rail, a rotor gear mechanism connected to at least one of said wheels to rotate said platform, said suction manifold and scraper being secured by a rod structure to said platform.
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Type: Grant
Filed: Nov 6, 2007
Date of Patent: Dec 29, 2009
Patent Publication Number: 20080135473
Assignee: Council of Scientific & Industrial Research
Inventors: Girish Ramesh Pophali (Nagpur), Tapas Nandy (Nagpur), Santosh Narain Kaul (Nagpur), Sukumar Devotta (Nagpur)
Primary Examiner: Christopher Upton
Attorney: St. Onge Steward Johnston & Reens LLC
Application Number: 11/935,525
International Classification: B01D 21/06 (20060101); B01D 21/24 (20060101);