Patents Issued in March 30, 2004
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Patent number: 6713398Abstract: A method of planarizing a polysilicon plug. A dielectric layer has an opening therein. Polysilicon is deposited into the opening to form a polysilicon layer so that the opening is completely filled and the top surface of the dielectric layer is covered. A high molecular weight compound is deposited to form a sacrificial film over the polysilicon layer. An anisotropic etching of the sacrificial film and the polysilicon layer is carried out to remove the sacrificial film and the polysilicon layer outside the opening.Type: GrantFiled: November 16, 1999Date of Patent: March 30, 2004Assignee: Taiwan Semiconductor Manufacturing Co., Ltd.Inventor: Bor-Wen Chan
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Patent number: 6713399Abstract: A embedded resistor printed circuit board fabrication includes the steps of preparing a substrate having a top conductive layer and a bottom insulating layer and etching the top conductive layer to form a first conductive layer having recesses in it; embedding resistive material in the recesses, enabling the first conductive layer to be electrically connected to lateral sides of the resistive material; plating a thin conductive film on the first conductive layer and the resistive material to form a second conductive layer; and etching the first conductive layer and second conductive layer to let the second conductive layer be electrically connected to the thin film type resistors.Type: GrantFiled: December 23, 2002Date of Patent: March 30, 2004Assignee: Uni-Circuit Inc.Inventor: Hsi-Song Kao
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Patent number: 6713400Abstract: A method of producing a metastable degradation resistant amorphous hydrogenated silicon film is provided, which comprises the steps of growing a hydrogenated amorphous silicon film, the film having an exposed surface, illuminating the surface using an essentially blue or ultraviolet light to form high densities of a light induced defect near the surface, and etching the surface to remove the defect.Type: GrantFiled: November 16, 2000Date of Patent: March 30, 2004Assignee: Midwest Research InstituteInventor: Howard M. Branz
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Patent number: 6713401Abstract: Disclosed is a method for manufacturing a semiconductor device which efficiently carries out a process on a semiconductor substrate, such as dry etching, and cleaning for removing a foreign matter after the process. The method includes a step of removing a foreign matter by using both an electric action of a plasma generated by plasma generation means and a physical action caused by a frictional stress of a fast gas stream formed by a pad structure which is arranged close to a wafer surface.Type: GrantFiled: August 28, 2001Date of Patent: March 30, 2004Assignee: Hitachi, Ltd.Inventors: Kenetsu Yokogawa, Yoshinori Momonoi, Kazunori Tsujimoto, Shinichi Tachi
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Patent number: 6713402Abstract: Cleaning methods are disclosed for removing sidewall polymers from interconnect vias or trenches, wherein a wafer is exposed to a plasma comprising hydrogen and an inert gas in a plasma cleaning chamber following etch-stop etching.Type: GrantFiled: May 31, 2002Date of Patent: March 30, 2004Assignee: Texas Instruments IncorporatedInventors: Patricia Beauregard Smith, Heungsoo Park
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Patent number: 6713403Abstract: A method for manufacturing a semiconductor device having a movable unit includes a step of forming an SOI substrate that includes a semiconductor substrate, an insulating layer, and a semiconductor layer. The method further includes a step of dry etching the semiconductor layer to form a trench and a step of dry etching a sidewall defining the trench at a portion adjacent to a bottom of the trench to form the movable unit. The later dry etching is implemented with a charge building up on a surface of the insulating layer that is exposed during the former dry etching to etch the portion. In addition, the later dry etching is implemented at an etching rate higher than that at which the former dry etching is implemented to reduce the deposition amount of a protection film deposited on a reverse side of the movable unit during the later dry etching.Type: GrantFiled: March 11, 2003Date of Patent: March 30, 2004Assignee: Denso CorporationInventors: Junji Oohara, Kazuhiko Kano, Hiroshi Muto
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Patent number: 6713404Abstract: The invention includes a semiconductor construction comprising a semiconductor substrate, and a first layer comprising silicon and nitrogen over the substrate. A second layer comprising at least 50 weight % carbon is over and physically against the first layer, and a third layer consisting essentially of a photoresist system is over and physically against the second layer. The invention also includes methodology for forming the semiconductor construction.Type: GrantFiled: March 5, 2002Date of Patent: March 30, 2004Assignee: Micron Technology, Inc.Inventor: Yoshiki Hishiro
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Patent number: 6713405Abstract: A humidifying heat treating unit for heating a wafer W having a coated film such as a dielectric film formed thereon under a humidified atmosphere comprises a hot plate for heating the wafer W, a chamber having a plurality of blocks, and provided with a gas supply port for supplying a humidified gas into the chamber and an exhaust port exhausting the chamber for every block, and a control section for controlling the supply-exhaust of the humidified gas into and out of the chamber. The control section controls the supply-exhaust of the humidified gas for every block.Type: GrantFiled: May 6, 2003Date of Patent: March 30, 2004Assignee: Tokyo Electron LimitedInventor: Hirofumi Moriyama
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Patent number: 6713406Abstract: Improved processes for depositing dielectric layers by HDP (High Density Plasma) CVD (Chemical Vapor Deposition) are described. One method controls the RF power applied to the side source RF power to be less than about 2500 Watts during dielectric deposition. A second method controls the thickness of the HDP-CVD deposited dielectric layer to be less than between about 2000 and 3000 Angstroms. These methods of HDP-CVD deposition of dielectric layers result in elimination or suppression of plasma induced damage to MOSFET devices and improved gate oxide integrity of MOSFET devices following deposition of dielectric layers by HDP-CVD.Type: GrantFiled: March 19, 2001Date of Patent: March 30, 2004Assignee: Taiwan Semiconductor Manufacturing CompanyInventors: Chu-Yun Fu, Kuo-Chyuan Tzeng
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Patent number: 6713407Abstract: A method of depositing a plasma enhanced CVD metal nitride layer over an exposed copper surface in a semiconductor wafer manufacturing process to improve the metal nitride layer adhesion and to reduce copper hillock formation including providing a process surface which is an exposed copper surface; preheating the process surface; plasma sputtering the exposed copper surface in-situ to remove copper oxides; and, depositing a metal nitride layer in-situ according to a plasma enhanced CVD process at a selected deposition pressure to reduce plasma ion bombardment energy transfer and to suppress-copper hillock formation.Type: GrantFiled: October 29, 2002Date of Patent: March 30, 2004Assignee: Taiwan Semiconductor Manufacturing Co., LtdInventors: Yi-Lung Cheng, Wen-Kung Cheng, Sez-An Wu, Yi-Lung Wang, Shin-Chi Lin
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Patent number: 6713408Abstract: A lithographic method for producing high aspect ratio silica micro-structures having the steps of: providing a carrier substrate with a confinement boundary placed on the carrier substrate; placing the SOG material within the confinement boundary and soft baking at a temperature above its glass transition temperature; forming a pattern of interest on the soft baked SOG material by x-ray lithography; and heating the SOG material until it is substantially converted to a silica-like oxide.Type: GrantFiled: December 14, 2001Date of Patent: March 30, 2004Assignee: Louisiana Tech University Foundation, Inc.Inventors: Vijay-Anandh Shanmugam, Michael J. Vasile, Philip J. Coane
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Patent number: 6713409Abstract: A manufacturing method using a modular substrate-based processing scheme for producing semiconductor devices, provides multiple modular processing units which may be arranged together to form any of various cohesive processing units or individually or sequentially processed through standard semiconductor processing equipment. The cohesive processing units are processed unitarily providing for multiple modular processing units to be processed simultaneously. The modular processing units may be formed of a thick semiconductor substrate or a semiconductor substrate mounted on a further substrate such as a ceramic material. The modular processing units may each contain ribs, grooves, posts or other features to aid in handling and placement of the individual units.Type: GrantFiled: November 25, 2002Date of Patent: March 30, 2004Assignee: Agere Systems Inc.Inventors: Michael Antonell, Erik Cho Houge, Nitin Patel, Larry E. Plew, Catherine Vartuli
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Patent number: 6713410Abstract: A method of treating textile which is yarn or fabric containing spandex fibres, comprising contracting the textile with a perfume so that the perfume is deposited on the fabric. The perfume contains a mixture of fragrance materials which preferentially deposit on the spandex fibres. The yarn of fabric may be made up into garments.Type: GrantFiled: July 14, 2000Date of Patent: March 30, 2004Assignee: E.I. du Pont de Nemours and Co.Inventors: Keith Douglas Perring, Christopher Francis Clements, Angus Peter MacMaster, Raymond Palmen, Olivier William John
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Patent number: 6713411Abstract: Disclosed is a laminate having flame and chemical resistance, which may be used to form protective fabrics. The laminate contains a first layer of a spunlace fabric having a fire retardant additive applied thereto; and a second layer of a polymeric film.Type: GrantFiled: April 19, 1999Date of Patent: March 30, 2004Assignee: Precision Fabric GroupInventors: William C. Cox, Philip E. Harris
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Patent number: 6713412Abstract: Specific fabric articles exhibiting very low air and/or gas permeability (even upon application of high inflation pressures) and very high tear strengths are herein disclosed and claimed. Such a specific fabric also permits the incorporation of discrete openings (through cutting, for example) through which air and/or gas introduced by an airbag inflation canister will travel. Such a specific fabric acts as a barrier to the complete introduction of high pressure inflation gases into an airbag cushion, thereby permitting a more controlled, safer inflation upon the occurrence of a collision event. Thus, the specific inventive fabric permits movement of inflation gas and/or air substantially solely through the openings within the fabric and not through the interstices between the individual fiber constituents.Type: GrantFiled: May 6, 2003Date of Patent: March 30, 2004Assignee: Milliken & Co.Inventor: Thomas Wayne Newbill
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Patent number: 6713413Abstract: A buffing or polishing material has a nonwoven fleece layer and a backing layer that adds strength and dimensional stability to the material. The nonwoven fleece layer is a needled blend of natural fibers and synthetic fibers having a uniform density and working surface, resulting in a better polishing or finishing consistency. The material can withstand high heat levels and can be worked quickly, resulting in a more efficient polishing or finishing operation. The buff material can be converted into any preferred shape or tool, such as an endless belt, disc, flapwheel, or spiral band.Type: GrantFiled: December 22, 2000Date of Patent: March 30, 2004Assignee: Freudenberg Nonwovens Limited PartnershipInventor: Gerald F. Kruegler
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Patent number: 6713414Abstract: The present invention is directed to ion-sensitive, water-dispersible polymers. The present invention is also directed to a method of making ion-sensitive, water-dispersible polymers and their applicability as binder compositions. The present invention is further directed to fiber-containing fabrics and webs comprising ion-sensitive, water-dispersible binder compositions and their applicability in water-dispersible personal care products.Type: GrantFiled: May 4, 2000Date of Patent: March 30, 2004Assignee: Kimberly-Clark Worldwide, Inc.Inventors: William S. Pomplun, Franklin M. Chen, Paige A. Dellerman, Eric D. Johnson, Jeffrey D. Lindsay, Ligia A. Rivera, Kim G. Schick, Walter T. Schultz, Varsha K. Shah, Dave A. Soerens, Kenneth Y. Wang, Frederick J. Lang, Yihua Chang, David M. Jackson, Pavneet S. Mumick
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Patent number: 6713415Abstract: A laundry-durable stretchable composite fabric, based on two nonwoven outer layers and a pre-stretched inner layer of elastomeric fibers of at least 400 decitex and at least eight threadlines/inch, and having a flat surface appearance, is provided.Type: GrantFiled: April 12, 2001Date of Patent: March 30, 2004Assignee: E. I. du Pont de Nemours and CompanyInventor: Kenneth E. Martin
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Patent number: 6713416Abstract: A method of making a molecularly imprinted porous structure makes use of a surfactant analog of the molecule to be imprinted that has the imprint molecule portion serving as the surfactant headgroup. The surfactant analog is allowed to self-assemble in a mixture to create at least one supramolecular structure having exposed imprint groups. The imprinted porous structure is formed by adding reactive monomers to the mixture and allowing the monomers to polymerize, with the supramolecular structure serving as a template. The resulting solid structure has a shape that is complementary to the shape of the supramolecular structure and has cavities that are the mirror image of the imprint group. Similarly, molecularly imprinted particles may be made by using the surfactant to create a water-in-oil microemulsion wherein the imprint groups are exposed to the water phase.Type: GrantFiled: January 8, 2003Date of Patent: March 30, 2004Assignee: The United States of America as represented by the Secretary of the NavyInventors: Michael A. Markowitz, Paul E. Schoen, Bruce P. Gaber, Banahalli R. Ratna, Paul R. Kust, David C. Turner, Douglas S. Clark, Jonathan S. Dordick
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Patent number: 6713417Abstract: An insulative ceramic compact is composed of a fired mixture of (A) a MgAl2O4, Mg3B2O6 and/or Mg2B205 ceramic powder, and (B) a glass powder including from about 13 to 50% by weight of silicon oxide in terms of SiO2, from 8 to 60% by weight of boron oxide in terms of B2O3, about 20% by weight or less of aluminum oxide in terms of Al2O3, and from about 10 to 55% by weight of magnesium oxide in terms of MgO. The insulative ceramic compact can be obtained by firing at low temperatures of about 1000° C. or less, can be obtained by sintering with Ag or Cu, has a low dielectric constant and a high Q value, and is suitable for use in the high-frequency range.Type: GrantFiled: July 19, 2001Date of Patent: March 30, 2004Assignee: Murata Manufacturing Co., Ltd.Inventors: Osamu Chikagawa, Naoya Mori, Yasutaka Sugimoto
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Patent number: 6713418Abstract: A glass article of the present invention has a rate of dissolution in an acidic liquid of from 10 to 100 nm/min in terms of etching rate in immersing in a 0.1% by weight 50° C. aqueous solution of hydrofluoric acid and an average linear thermal expansion coefficient of 70×10−7/° C. or higher as measured in the range of from −50° C. to 70° C., and the working temperature T4 (° C.) and the liquidus temperature TL (° C.) thereof satisfy the relationship: T4−TL≧−100° C.Type: GrantFiled: May 29, 2002Date of Patent: March 30, 2004Assignee: Nippon Sheet Glass Co., Ltd.Inventors: Shoichi Kishimoto, Akihiro Koyama, Hiroyuki Tanaka, Nobuyuki Yamamoto
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Patent number: 6713419Abstract: An optical glass for precision press molding that has desired optical constants, a low glass transformation point (Tg), and a devitrification temperature that is lower than a temperature of a glass melt, at which a viscosity suitable for forming of a preform material is obtained, is provided. The optical glass for precision press molding has a lanthanum borosilicate system glass having optical constants of refractive index (nd) within a range from 1.65 to 1.73 and Abbe number (&ngr;d) within a range from 50 to 60, a Tg within a range of 480-580° C. The optical glass for precision press molding has a devitrification temperature that is lower than a temperature of the glass melt when the glass melt has a viscosity &eegr; (poise) of log &eegr;=2.5. The optical glass for precision press molding has a specific composition range of SiO2—B2O3—La2O3—Y2O3—Ta2O5—CaO—Li2O system composition.Type: GrantFiled: March 19, 2001Date of Patent: March 30, 2004Assignee: Kabushiki Kaisha OharaInventors: Masahiro Onozawa, Takehiro Sakamoto
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Patent number: 6713420Abstract: A porous ceramics body for in vivo or in vitro 1use in which a number of pores are closely distributed in three dimensional directions, adjoining pores thereof being partitioned by wall portions with respective communication ports to bring said adjoining pores into communication with each other such that a series of connected spherical pores are formed therewithin, said porous ceramics body being made of a sintered calcium phosphate body, characterized in that, within said sintered calcium phosphate body, pores each having a diameter of 5 microns (&mgr;m) or more account for 80% or more of all the pores in terms of volume whereas pores having a diameter of less than 5 microns (&mgr;m) account for less than 20% of all the pores in terms of volume as subjected to a mercury porosimeter measurement.Type: GrantFiled: October 10, 2001Date of Patent: March 30, 2004Assignees: Toshiba Ceramics Co., Ltd., Independent Administrative Institution National Institute for Materials Science, Toshiba Denko Co., Ltd.Inventors: Kohichi Imura, Takashi Umezawa, Akihiko Ichikawa, Katsuhiro Chaki
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Patent number: 6713421Abstract: The invention relates to blanks comprising zirconium oxide-based ceramic with an addition of 0.1 to 0.50 wt.-% of at least one of the oxides of the elements aluminium, gallium, germanium, indium and their use.Type: GrantFiled: April 11, 2002Date of Patent: March 30, 2004Assignee: 3M ESPE AGInventors: Holger Hauptmann, Robert Schnagl, Sybille Frank
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Patent number: 6713422Abstract: A process for working up at least partially deactivated polymerization catalysts for the polymerization or copolymerization of THF which are contaminated with the products of the polymerization or copolymerization of THF comprises (a) in a first step, cleaning the polymerization catalyst by treatment with steam at from 80 to 250° C. and a pressure of from 0.5 to 40 bar and, preferably, (b) in a second step, regenerating the clean polymerization catalyst.Type: GrantFiled: July 17, 2001Date of Patent: March 30, 2004Assignee: BASF AktiengesellschaftInventors: Volkmar Menger, Karsten Eller, Anton Meier, Michael Hesse
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Patent number: 6713423Abstract: The present invention generally relates to a method of thermally reactivating activated carbon via a two-step process: steam followed by pyrolysis; whereby the steam is preferably deoxygenated. Activated carbons reactivated by this method resemble their virgin counterpart's physical characteristics (e.g., BET surface area) and often perform better in water treatment. The present invention also includes a method of reactivating activated carbon via conventional processes (i.e. pyrolysis followed by steam) at low dissolved oxygen (DO) concentrations. The third aspect of the present invention is the activation of carbonaceous material comprising of steam treating the carbonaceous material followed by pyrolysis.Type: GrantFiled: January 29, 2003Date of Patent: March 30, 2004Assignee: Engineering Performance Solutions, LLCInventor: David W. Mazyck
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Patent number: 6713424Abstract: The present methods make fluid diffusion layers having reduced surface roughness. The methods used for adhering the loading material to the substrate surface can reduce the average surface roughness of the fluid diffusion layers, thereby reducing leaks in and damage to ion exchange membranes. When fluid diffusion layers and electrodes having reduced surface roughness are employed in membrane electrode assemblies, better reliability and performance are obtained. A method of calculating the surface roughness of a fluid diffusion layer may be used.Type: GrantFiled: May 16, 2001Date of Patent: March 30, 2004Assignee: Ballard Power Systems Inc.Inventors: Jürgen Stumper, John Robert Gordon, Herwig Robert Haas, Kelvin Keen-Ven Fong
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Patent number: 6713425Abstract: A process of forming a bimetallic catalyst composition comprising a cocatalyst (a trialkylaluminum compound) and a catalyst precursor. The precursor comprises at least two transition metals; a metallocene complex is a source of one of said two transition metals. The precursor is produced in a single-pot process by contacting a porous carrier, in sequence, with a dialkylmagnesium compound, an aliphatic alcohol, a non-metallocene transition metal compound, a contact product of a metallocene complex and a trialkyl-aluminum compound, and methylalumoxane.Type: GrantFiled: June 3, 2002Date of Patent: March 30, 2004Assignee: Univation Technologies, LLCInventors: Robert I. Mink, Yury V. Kissin, Thomas E. Nowlin, Pradeep P. Shirodkar, Grace O. Tsien, Sandra D. Schregenberger
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Patent number: 6713426Abstract: A syndiotactic polyolefin is obtained in a high yield by polymerization or copolymerization of an olefin of the formula Ra—CH═CH—Rb in the presence of a catalyst consisting of a metallocene of the formula I in which M1 is titanium, zirconium, vanadium, niobium or tantalum, and an aluminoxane. This polyolefin has a very high molecular weight, a very narrow molecular weight distribution and a very high syndiotactic index. Shaped articles produced from the polymer are distinguished by a high transparency, flexibility, tear resistance and an excellent surface gloss.Type: GrantFiled: June 5, 1995Date of Patent: March 30, 2004Assignee: Basell Polyolefine GmbHInventors: Andreas Winter, Jürgen Rohrmann, Martin Antberg, Volker Dolle, Walter Spaleck
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Patent number: 6713427Abstract: This invention is directed to alkyl cobalt (II) dioximates and methods for making these dioximates.Type: GrantFiled: February 21, 2003Date of Patent: March 30, 2004Assignee: E. I. du Pont de Nemours and CompanyInventors: Alexei A. Gridnev, Gregorii A. Nikiforov
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Patent number: 6713428Abstract: The present invention concerns a novel, highly dispersible aluminium hydrate. It also concerns a process for preparing said aluminium hydrate by precipitation of an aluminium hydrate in a reactor with no back-mixing and preparation of said aluminium hydrate in a reactor with back-mixing. Finally, it concerns the use of said hydrate for the preparation of catalysts or catalyst supports.Type: GrantFiled: May 9, 2001Date of Patent: March 30, 2004Assignee: Instuit Francais du PetroleInventors: Pierre-Yves Le Goff, Philippe Laval, Michel Martin
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Patent number: 6713429Abstract: A purification catalyst for exhaust gas is provided that uses a hexagonal cell monolithic carrier which is able to demonstrate purification performance that is superior to the case of using a square cell monolithic carrier. This purification catalyst for exhaust gas comprises a monolithic carrier (10) provided with hexagonal cells (15) of 200 cells/in2 or more in which the porosity of partition walls (11) that form the cells (15) is 25% or more; and, a catalyst layer (2) arranged on the surface of the partition walls (11) of the monolithic carrier (10) that contains a catalyst component for purification of exhaust gas. The thickness of catalyst layer (2) is 10-70 &mgr;m at its thin portion (21), and its thick portion (22) has a thickness of no more than 12 times that of thin portion (21).Type: GrantFiled: December 16, 1999Date of Patent: March 30, 2004Assignee: Denso CorporationInventors: Masakazu Tanaka, Yosiyasu Andou, Keiji Ito, Takahiro Kida
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Patent number: 6713430Abstract: A leaf of printed matter has a metachromatic image 2 printed with an ink thermally changing its color and a non-metachromatic image 3 of a colorant not changing its color. A principal figure 5 is formed of the colorant, and a background 6 is formed with the metachromatic ink. The printed matter 1 may be used to transfer its images to a cup 10. The ink of the background scene 6 in the outer layer will turn to colorless within a prescribed range of temperatures, rendering visible only the central principal figure 5. At lower temperatures, the metachromatic ink will restore its color to cause the background for instance a snowy scene to appear, thus affording a novel and fantastic visual effect.Type: GrantFiled: April 9, 2001Date of Patent: March 30, 2004Assignee: Sakura Color Products CorporationInventors: Nakao Tominaga, Yoshinori Murata
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Patent number: 6713431Abstract: A metallic luster tone thermochromic laminate member 1, which comprises a laminate of a metallic luster layer 2 containing a metallic luster pigment prepared by coating the surface of a synthetic mica or thin section aluminum oxide with a metal oxide and a reversible thermochromic layer 3 containing a thermochromic composition comprising an electron-donating color-forming organic compound, an electron-accepting compound and an organic compound medium in which color reactions of both compounds take place reversibly. The metallic luster tone thermochromic laminate member can visualize metallic luster colors having glittering high brightness and distinct changes in color by its reversible thermochromic layer so that it can be used in versatile applications and developments.Type: GrantFiled: June 26, 2002Date of Patent: March 30, 2004Assignee: The Pilot Ink Co., Ltd.Inventors: Michiyuki Yasuda, Yutaka Shibahashi
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Patent number: 6713432Abstract: A thermal transfer recording material comprising a support having thereon an image transferring layer containing a coloring material represented by Formula (I), Formula (I): wherein each R11 and R12 is independently a substituted or unsubstituted aliphatic group; R13 is a substituent and n is an integer of 0 to 4, provided that when n is 2 or more, a plurality of R13s are the same or different; R14 is an alkyl group; and each R15 and R16 is independently an alkyl group having 3 to 8 carbon atoms.Type: GrantFiled: January 28, 2002Date of Patent: March 30, 2004Assignee: Konica CorporationInventors: Dai Ikemizu, Mitsuhiro Fukuda, Motoaki Sugino, Norio Miura
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Patent number: 6713433Abstract: A stable, liquid concentrate herbicidal composition is provided. The composition comprises a water-soluble herbicide in a continuous aqueous phase and an oil-soluble herbicide in a discontinuous oil phase.Type: GrantFiled: February 14, 2002Date of Patent: March 30, 2004Assignee: Monsanto Technology, LLCInventor: Ganiyu A. Jimoh
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Patent number: 6713434Abstract: This invention relates to the control of weeds using (a) a urea herbicide and (b) a 4-benzoylisoxazole or a 2-cyano-1,3-dione herbicide.Type: GrantFiled: February 19, 2002Date of Patent: March 30, 2004Assignee: Rhone-Poulenc AgroInventors: Jean-Claude Millet, Jairo E. Melgarejo Garcia
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Patent number: 6713435Abstract: A method for producing an optically active lactone compound by Baeyer-Villiger oxidation of a cyclic ketone compound with at least one kind of oxidants selected from the group consisting of hydrogen peroxide and urine-hydrogen peroxide adduct (UHP) using a cobalt(salen) complex having a cis-&bgr; structure expressed by the following formula (I) or (II) as a catalyst. in which X and Y independently denote H, a t-butyl group or an electron-withdrawing substituting group and W is a halogen element. in which X and Y independently denote H, a t-butyl group or an electron-withdrawing substituting group and Z− is a monovalent anion. The optically active lactone compounds can be used for the synthesis of medicines and argochemicals.Type: GrantFiled: September 3, 2002Date of Patent: March 30, 2004Assignee: Kyushu UniversityInventors: Tsutomu Katsuki, Tatsuya Uchida, Katsuji Ito
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Patent number: 6713436Abstract: The present invention relates to 1-cycloalkylpyrazolylbenzoyl derivatives of the formula I wherein all variables are as defined in the specification, their agriculturally useful salts, processes for their preparation, and for the use of these compounds or compositions comprising them, for controlling undesirable plants.Type: GrantFiled: February 6, 2002Date of Patent: March 30, 2004Assignee: BASF AktiengesellschaftInventors: Ulf Neidlein, Norbert Götz, Ulf Misslitz, Roland Götz, Ernst Baumann, Wolfgang von Deyn, Steffen Kudis, Klaus Langemann, Guido Mayer, Matthias Witschel, Martina Otten, Karl-Otto Westphalen, Helmut Walter
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Patent number: 6713437Abstract: The method of preparing an oxide superconducting wire comprises steps of preparing a wire by coating raw material powder for a Bi—Pb—Sr—Ca—Cu—O based oxide superconductor including a 2223 phase with a metal and heat treating the wire in a pressurized atmosphere containing oxygen in a prescribed partial pressure, and the total pressure of the pressurized atmosphere is at least 0.5 MPa. The pressure heat treatment apparatus comprises a pressure furnace storing and heat treating a target in a pressurized atmosphere, a pressure regulator for measuring the total pressure in the pressure furnace, an oxygen concentration meter for measuring the oxygen concentration in the pressure furnace and a controller for controlling the oxygen partial pressure in the pressure furnace in response to the total pressure measured by the pressure regulator and the oxygen concentration measured by the oxygen concentration meter.Type: GrantFiled: October 25, 2002Date of Patent: March 30, 2004Assignee: Sumitomo Electric Industries, Ltd.Inventors: Shinichi Kobayashi, Tetsuyuki Kaneko, Ryosuke Hata
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Patent number: 6713438Abstract: High performance engine oils and other liquid lubricants comprise a liquid lubricant basestock of low viscosity from 1.5 to 12 cSt (100C) with two dissolved polymer components of differing molecular weights. The basestock is preferably a single PAO or blend of PAOs with a co-basestock component which is preferably an ester or an alkylated aromatic of comparable viscosity. The lower molecular weight polymer is highly viscoelastic in character and is preferably an HVI-PAO; this component in the lubricant which provides unexpectedly high film thickness and unexpectedly good wear protection under conditions where the second, higher molecular weight polymer may lose some or all of its thickening power. The use of the highly viscoelastic low molecular weight polymer in combination with the higher molecular weight thickener enables the production of very widely cross-graded engine oils, especially oils with a low temperature grading of 0W or better.Type: GrantFiled: March 24, 1999Date of Patent: March 30, 2004Assignee: Mobil Oil CorporationInventors: David J. Baillargeon, Raymond J. Bergstra, Andrew Jackson, William L. Maxwell, G. James Johnston, Robert A. Pache
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Patent number: 6713439Abstract: An energy conserving power transmission fluid composition comprising: (a) from 1 to 49 wt. % of a polyalphaolefin base stock having a kinematic viscosity of from 40 mm2/s at 100° C. to 500 mm2/s at 100° C.; (b) from 1 to 95 wt. % of a lubricant basestock having a kinematic viscosity of from 2 mm2/s at 100° C. to 10 mm2/s at 100° C.; (c) from 1 to 49 wt. % of a polyol ester of a C5 to C30 aliphatic monocarboxylic acid and a polyol of the formula R(OH)n where n is at least 2, and (d) an effective amount of a performance additive package selected from the group consisting of automotive gear oil additive packages, manual transmission fluid additive packages and automatic transmission fluid additive packages, provided that the composition has a kinematic viscosity of at least 4 mm2/s at 100° C.Type: GrantFiled: June 5, 2002Date of Patent: March 30, 2004Assignee: Infineum International Ltd.Inventor: Raymond F. Watts
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Patent number: 6713440Abstract: A resist removing composition having a superior capability for removing a resist, polymer, organometallic polymer and etching by-products such as metal oxide, which does not attack underlying layers exposed to the composition and which does not leave residues after a rinsing step. The resist removing composition contains alkoxy N-hydroxyalkyl alkanamide and a swelling agent.Type: GrantFiled: January 31, 2002Date of Patent: March 30, 2004Assignee: Samsung Electronics Co., Ltd.Inventors: Dong-jin Park, Kyung-dae Kim, Sang-mun Chon, Jin-ho Hwang, Il-hyun Sohn, Sang-oh Park, Pil-kwon Jun
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Patent number: 6713441Abstract: Disclosed is a toilet bowl cleaner that includes a hypochlorite generator and an effervescent system that produces a foam level approximately one inch above a water line in the toilet. The cleaner may be prepared, stored and packaged in a manner that prevents moisture from initiating premature decomposition of the cleaning components. The toilet bowl cleaner may also include a binder, lubricant, fragrance, and a surfactant mixture. Further, the toilet bowler cleaner may be in the form of a tablet, granules, or a powder. The toilet bowl cleaner may also be coated with a surfactant mixture. Also disclosed is a method for producing the toilet bowl cleaner, including the steps of: combining an effervescent system, a hypochlorite generator, and a binder to form a pre-mix; blending the pre-mix in a blender for approximately 15 to 20 minutes; adding a lubricant to the blended pre-mix; and blending the lubricant with the blended pre-mix for approximately three to four minutes to form a cleaner blend.Type: GrantFiled: March 14, 2001Date of Patent: March 30, 2004Assignee: Chemlink Laboratories, LLCInventors: Richard A. DeSenna, Hilton G. Dawson, Ryan Griffin Moore, Kenneth Scott Wiley
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Patent number: 6713442Abstract: A built particulate laundry detergent composition containing anionic sulphonate or sulphate surfactant and conventional ethoxylated alcohol nonionic surfactant also contains a low level of a highly ethoxylated alcohol nonionic surfactant having an average degree of ethoxylation of from 15 to 40, and a low level of a textile softening clay. The composition exhibits increased mildness to the skin without loss of detergency performance, and the softness of washed fabrics is significantly improved despite the low level of softening clay present.Type: GrantFiled: October 10, 2002Date of Patent: March 30, 2004Assignee: Unilever Home & Personal Care USA division of Conopco, Inc.Inventors: Rudolfus Johannes Hendrikus Hafkamp, Rob Menting, Antje Minke Wierenga
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Patent number: 6713443Abstract: Compounds having the following peptide sequence: X Leu Y, wherein X is H or Ala or Leu-Ser-Ala, Y is OH or peptide sequence having from 1 to 10 amino acids, with the terminal carboxy end being amidified by a NH2 group, or esterified by a substituted or non-substituted hydrocarbyloxy, with the proviso that X and Y are not simultaneously H and OH, respectively, The invention also concerns the corresponding compounds wherein the peptide binding group —CO—NH— is replaced by a binding group resisting protease enzymatic degradation, or wherein the peptide backbone comprises one or more intercalated groups making the peptide binding resistant to enzymatic degradation. Also described are compounds comprising a grouping whose spatial structure is substantially identical to that of a peptide of the sequence X-Leu-Y wherein X and Y have the above-mentioned definition.Type: GrantFiled: July 5, 1996Date of Patent: March 30, 2004Assignee: Institut PasteurInventors: Gilles Fillion, Jean-Claude Rouselle, Olivier Massot
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Patent number: 6713444Abstract: The compounds of the invention are generally described by the formula: X1X2B3X4B5X*6X7X8 B9X10B11X12B13X14 B15X16B17X*18X*19B20 X21X22X23Q24F25Z*26X27 X28B29X30B31B32X33X34 B35B36X37Z38Z39 (1) and the salts, esters, amides, and acyl forms thereof. Up to 15 amino acids may be truncated from the N-terminus and up to 6 amino acids may be truncated from the C-terminus. Each position represented by a letter indicates a single amino acid residue wherein B is a basic or polar/large amino acid or a modified form thereof; X is a small or hydrophobic amino acid or a modified form thereof; X* is a small or polar/large amino acid or a modified form thereof; Z is a polar/large or hydrophobic amino acid or a modified form thereof; Z* is Proline or a polar/large or hydrophobic amino acid or a modified form thereof. These compounds may be used to inhibit the protease activity of Botulinum B and tetanus toxins.Type: GrantFiled: May 12, 2000Date of Patent: March 30, 2004Assignee: The United States of America as represented by the Secretary of the ArmyInventors: Gregory E. Garcia, Richard K. Gordon, Debbie R. Moorad, Bhupendra P. Doctor
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Patent number: 6713445Abstract: The HIV-1 envelope protein gp120 is toxic to rodent and human neurons by indirect mechanisms requiring accessory glial cells. Chemokines are known to block gp120 interactions with chemokine receptors on T cells, macrophanges, and microglia, thereby preventing viral infection. Gp120-induced neuronal killing in rat hippocampal cultures was partially or completely prevented by a specific short peptides related to chemokines, specially IKEYFTS (SEQ. ID NO: 2) and LESYT (SEQ. ID NO: 1). These peptides thus have use in the treatment of neurological degenerative diseases having symptoms associated with neuronal cell death.Type: GrantFiled: June 12, 2001Date of Patent: March 30, 2004Assignee: Advanced Immuni T, Inc.Inventors: Candace Pert, Michael Ruff
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Patent number: 6713446Abstract: The present invention provides stable compounds prepared from boronic acid and lyophilized compounds thereof of the formula (1): in which Z1 and Z2 are moieties derived from sugar. The invention also provides methods for preparing such compounds. Lyophilizing a mixture comprising a boronic acid compound and a moiety derived from sugar produces a stable composition that readily releases the boronic acid compound upon reconstitution in aqueous media.Type: GrantFiled: January 25, 2002Date of Patent: March 30, 2004Assignee: The United States of America as represented by the Secretary of the Department of Health and Human ServicesInventor: Shanker Lal Gupta
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Patent number: 6713447Abstract: The present invention relates to a method for purifying marine mammal oil enriched in omega 3 fatty acids and to compositions comprising such oils. The invention also relates to a method of preparing such oils from the seal and other marine mammals. More particularly, the present invention relates to a process for the transformation of subcutaneous and muscular tissues from the seal and other marine mammals. Even more particularly, the present invention relates to a process for obtaining lipid and protein extracts from the carcasses of seal and other marine mammals and to these extracts. In addition, the invention relates to fractions obtained by the methods of the present invention and to food supplements comprising same.Type: GrantFiled: October 7, 2002Date of Patent: March 30, 2004Assignee: Universite de SherbrookeInventors: Adrien Beaudoin, Geneviève Martin