Patents Issued in September 20, 2011
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Patent number: 8021985Abstract: The process of the present invention to form a mask made of inorganic material containing silicon reduces the plasma damage induced in the semiconductor layers due to the plasma-ashing. The semiconductor material is heat-treated at a high temperature after the growth thereof to form an oxide layer positively in the surface of the semiconductor material before it is covered by the silicon inorganic film. This inorganic film is dry-etched by an etchant containing fluorine to get a mask for forming a mesa and for growing burying layer selectively.Type: GrantFiled: December 17, 2010Date of Patent: September 20, 2011Assignee: Sumitomo Electric Industries, Ltd.Inventor: Tomokazu Katsuyama
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Patent number: 8021986Abstract: A method for producing a transistor with metallic source and drain including the steps of: a) producing a gate stack, b) producing two portions of a material capable of being selectively etched relative to a second dielectric material and arranged at the locations of the source and of the drain of the transistor, c) producing a second dielectric material-based layer covering the stack and the two portions of material, d) producing two holes in the second dielectric material-based layer forming accesses to the two portions of material, e) etching of said two portions of material, f) depositing a metallic material in the two formed cavities, and also including, between steps a) and b), a step of deposition of a barrier layer on the stack, against the lateral sides of the stack and against the face of the first dielectric material-based layer.Type: GrantFiled: June 8, 2010Date of Patent: September 20, 2011Assignee: Commissariat à l'énergie atomique et aux energies alternativesInventors: Bernard Previtali, Thierry Poiroux, Maud Vinet
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Patent number: 8021987Abstract: An insulting film is modified by subjecting the insulting film to a modification treatment comprising a combination of a plasma treatment and a thermal annealing treatment. There is provided a method of enhancing the characteristic of an insulating film by improving deterioration in the characteristic of the insulating film due to carbon, a suboxide, a dangling bond or the like contained in the insulating film.Type: GrantFiled: December 7, 2009Date of Patent: September 20, 2011Assignee: Tokyo Electron LimitedInventors: Takuya Sugawara, Yoshihide Tada, Genji Nakamura, Shigenori Ozaki, Toshio Nakanishi, Masaru Sasaki, Seiji Matsuyama, Kazuhide Hasebe, Shigeru Nakajima, Tomonori Fujiwara
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Patent number: 8021988Abstract: The present invention provides a semiconductor device having an improved silicon oxide film as a gate insulation film of a Metal Insulator Semiconductor structure and a method of making the same.Type: GrantFiled: April 21, 2008Date of Patent: September 20, 2011Assignee: Kabushiki Kaisha ToshibaInventor: Kouichi Muraoka
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Patent number: 8021989Abstract: One inventive aspect is related to a method for isolating structures of a semiconductor material, comprising providing a pattern of the semiconductor material comprising at least one elevated line, defining device regions in the pattern, the device regions each comprising at least said at least one elevated line, and modifying the conductive properties of the semiconductor material outside said device regions, such that the device regions are electrically isolated.Type: GrantFiled: May 26, 2006Date of Patent: September 20, 2011Assignee: IMECInventors: Staf Verhaegen, Axel Nackaerts
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Patent number: 8021990Abstract: A MOSFET structure including silicate gate dielectrics with nitridation treatments of the gate dielectric prior to gate material deposition.Type: GrantFiled: April 9, 2009Date of Patent: September 20, 2011Assignee: Texas Instruments IncorporatedInventors: Antonio L. P. Rotondaro, Luigi Colombo, Mark R Visokay, Rajesh Khamankar, Douglas E Mercer
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Patent number: 8021991Abstract: Oxide films are deposited under conditions generating a silicon-rich oxide in which silicon nanoclusters form either during deposition or during subsequent annealing. Such deposition conditions include those producing films with optical indices (n) greater than 1.46. The method of the present invention reduces the TID radiation-induced shifts for the oxides.Type: GrantFiled: February 28, 2006Date of Patent: September 20, 2011Assignee: The United States of America as represented by the Secretary of the NavyInventors: Harold L Hughes, Bernard J Mrstik, Reed K Lawrence, Patrick J McMarr
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Patent number: 8021992Abstract: A high density plasma chemical vapor deposition process including exciting gas mixture to create a plasma including ions, and directing the plasma into a dense region above the upper surface of the semiconductor wafer, heating the wafer using an additional heat source, and allowing a material from the plasma to deposit onto the semiconductor wafer.Type: GrantFiled: September 1, 2005Date of Patent: September 20, 2011Assignee: Taiwan Semiconductor Manufacturing Co., Ltd.Inventors: Joung-Wei Liou, Tsang-Yu Liu, Chien-Feng Lin, Cheng-Liang Chang, Ming-Te Chen, Chia-Hui Lin, Ying-Hsiu Tsai, Szu-An Wu, Yin-Ping Lee
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Patent number: 8021993Abstract: An apparatus for manufacturing a liquid crystal display device is disclosed. A first robot arm at a loading side of the thru-conveyor receives a substrate coated with photoresist and conveys the substrate to a thru-conveyor. A softbake hot plate (SHP) at the unloading side of the thru-conveyor removes solvent from the substrate. A cool plate lowers the substrate temperature from which the solvent is removed. A buffer temporarily stores the substrate having the lowered temperature. A second robot arm between the thru-conveyor, the SHP, the cool plate and a loading side of the buffer, loads/unloads the substrate. A temperature control unit adjusts the substrate temperature unloaded from the buffer. A third robot arm between the unloading side of the buffer, the temperature control unit and an exposure unit that exposes the substrate, loads/unloads the substrate.Type: GrantFiled: December 22, 2005Date of Patent: September 20, 2011Assignee: LG Display Co., Ltd.Inventors: Yong Hun Kim, Sang Min Kwak, Jin Woo Seo
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Patent number: 8021994Abstract: A textile fabric is presented comprising at least a first and a second twisted thread, the first and the second twisted threads containing at least one cut resistant yarn as one component, and the second twisted thread containing a non-cut resistant yarn as a further component, and the non-cut resistant yarn of the second twisted thread consisting of elastomeric fibers. Further, protective clothing is presented, which contains the textile fabric.Type: GrantFiled: April 21, 2006Date of Patent: September 20, 2011Assignee: Teijin Aramid GmbHInventor: Regine Maria Zumloh
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Patent number: 8021995Abstract: A fiber mixture according to the invention comprises fibers A comprising a polymer A containing a thermoplastic polyurethane elastomer and fibers B comprising a thermoplastic polymer B other than the thermoplastic polyurethane elastomer, said thermoplastic polyurethane elastomer having a starting temperature for solidifying of 65° C. or above as measured by a differential scanning calorimeter (DSC) and containing 3.00×106 or less polar-solvent-insoluble particles per g counted on a particle size distribution analyzer, which is based on an electrical sensing zone method, equipped with an aperture tube having an orifice of 100 ?m in diameter. An elastic nonwoven fabric comprises the fiber mixture.Type: GrantFiled: January 23, 2004Date of Patent: September 20, 2011Assignee: Mitsui Chemicals, Inc.Inventors: Kenichi Suzuki, Shigeyuki Motomura, Satoshi Yamasaki, Daisuke Nishiguchi, Hisashi Kawanabe
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Patent number: 8021996Abstract: The present invention provides a nonwoven web prepared from multicomponent fibers which are partially split. The partially split multicomponent fibers have at least one component of the multicomponent fiber separated from the remaining components of the multicomponent fiber along a first section of the longitudinal length of the multicomponent fibers. Along a second section of the longitudinal length of the multicomponent fibers the components of the multicomponent fibers remain together as a unitary fiber structure. In addition, part of the second section of the multicomponent fibers is bonded to part of a second section of an adjacent multicomponent fiber.Type: GrantFiled: December 23, 2008Date of Patent: September 20, 2011Assignee: Kimberly-Clark Worldwide, Inc.Inventors: Susan Kathleen Walser, Leon Eugene Chambers, Jr., Reginald Smith, Nancy J. Zimmerman, Kiran K. Reddy, Nina Frazier, David Myers
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Patent number: 8021997Abstract: A multicomponent spunbonded nonwoven is provided which is composed of at least two polymers which form interfaces toward one another, which are produced by at least one spinning machine having uniform spinning nozzle apertures, and which are hydrodynamically drawn, lapped in a sheet-like manner, and bonded, the multicomponent spunbonded nonwoven being composed of different filaments which contain at least two polymers, or it being composed of a mixture of multicomponent filaments and monocomponent filaments which each contain only one of the polymers, the multicomponent filament being composed of at least two elementary filaments and the titer of the individual filaments varying by the number of elementary filaments contained in the filaments.Type: GrantFiled: July 20, 2005Date of Patent: September 20, 2011Assignee: Carl Freudenberg KGInventors: Robert Groten, Ulrich Jahn, Georges Riboulet
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Patent number: 8021998Abstract: An absorbent structure made at least in part from a superabsorbent material having a retention capacity (CRC) as determined by a Centrifuge Retention Capacity Test of at least about 25 g/g and a free swell gel bed permeability (GBP) as determined by a Free Swell Gel Bed Permeability Test of at least 575×10?9 cm2. In another embodiment, the absorbent structure is made at least in part from a superabsorbent material having a retention capacity (CRC) as determined by a Centrifuge Retention Capacity Test of at least about 25 g/g, an absorbency under load (AUL) at 0.9 psi as determined by an Absorbency Under Load Test of at least 18 and a free swell gel bed permeability (GBP) as determined by a Free Swell Gel Bed Permeability Test of at least about 350×10?9 cm2.Type: GrantFiled: May 26, 2010Date of Patent: September 20, 2011Assignee: Kimberly-Clark Worldwide, Inc.Inventors: Jian Qin, Sandra Marie Rogers, Michael John Niemeyer, Kenneth Raymond Schueler, Jr., Steven Michael Hurley, Lawrence Howell Sawyer, Whei-Neen Hsu, Mark C. Joy, Scott J. Smith, Markus Frank, Nancy Birbiglia Lange
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Patent number: 8021999Abstract: In one aspect the invention is directed to a machinable glass-ceramic having a high degree of crystallinity (greater than 50 Vol. %), high mechanical strength (MOR>150 MPa) In accordance with the invention, the machinable glass-ceramics described herein consists essentially of, in weight percent, 35-55% SiO2, 6-18% Al2O3, 12-27% MgO, 3-12% F, 5-25% SrO, 0-20% BaO and 1-7% K2O. The machinable glass-ceramics of the invention have a dielectric constant of <8 (typically being in the range of 6-8) at 25° C. and 1 KHz; a loss tangent of <0.002 at 25° C. and 1 MHz; a CTE in the range of 80-120×10?7/° C. in the temperature range of 25-300° C.; a Poisson's ration of approximately 0.25; and a porosity of 0%.Type: GrantFiled: May 26, 2009Date of Patent: September 20, 2011Assignee: Corning IncorporatedInventor: George Halsey Beall
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Patent number: 8022000Abstract: A bonding glass containing V2O5: 25 to 50 wt %, TeO2: 20 to 40 wt % and BaO: 5 to 30 wt %, and not containing lead.Type: GrantFiled: January 5, 2007Date of Patent: September 20, 2011Assignee: Hitachi Displays Ltd.Inventors: Yuichi Sawai, Osamu Shiono, Takashi Namekawa, Hiroyuki Akata, Takashi Naito, Keiichi Kanazawa, Yuuichi Kijima, Shigemi Hirasawa, Shunichi Asakura, Mitsuo Hayashibara
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Patent number: 8022001Abstract: A method for producing an aluminum nitride sintered product according to the present invention includes the steps of (a) preparing a powder mixture that contains AlN, 2 to 10 parts by weight of Eu2O3 with respect to 100 parts by weight of AlN, Al2O3 such that a molar ratio of Al2O3 to Eu2O3 is 2 to 10, and TiO2 such that a molar ratio of TiO2 to Al2O3 is 0.05 to 1.2, but not Sm; (b) producing a compact from the powder mixture; and (c) firing the compact by subjecting the compact to hot-press firing in a vacuum or in an inert atmosphere.Type: GrantFiled: November 16, 2009Date of Patent: September 20, 2011Assignee: NGK Insulators, Ltd.Inventors: Naomi Teratani, Toru Hayase, Yuji Katsuda
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Patent number: 8022002Abstract: Regeneration flue gas streams containing unacceptable levels of CO can be effectively combusted (i.e., for more complete combustion or oxidation of CO to CO2) by contact with a second catalyst undergoing regeneration, for example in a second regenerator. While the second catalyst may also be regenerated by contact with an oxygen-containing gas stream, this second catalyst additionally comprises a noble metal, or is present in combination with a combustion comprising a noble metal. Representative catalysts used in an integrated regeneration process are those used for oxygenate conversion and olefin cracking, both for the purpose of producing light olefins (e.g., ethylene and propylene).Type: GrantFiled: March 24, 2009Date of Patent: September 20, 2011Assignee: UOP LLCInventor: Andrea G. Bozzano
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Patent number: 8022003Abstract: A porous crystalline composition having a molar composition as follows: YO2:m X2O3:n ZO, wherein Y is a tetravalent element selected from the group consisting of silicon, germanium, tin, titanium and combinations thereof, X is a trivalent element selected from the group consisting of aluminum, gallium, boron, iron and combinations thereof, Z is a divalent element selected from the group consisting of magnesium, zinc, cobalt, manganese, nickel and combinations thereof, m is between about 0 and about 0.5, n is between about 0 and about 0.5; and the composition has an x-ray diffraction pattern which distinguishes it from the materials. A process for making the composition, and a process using the composition to treat an organic compound are also provided.Type: GrantFiled: August 6, 2010Date of Patent: September 20, 2011Assignee: Intevep, S.A.Inventors: Andres Quesada Perez, Gerardo Vitale Rojas
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Patent number: 8022004Abstract: Various embodiments provide an electrode comprising a conductive substrate, a first layer of a mixture comprising iridium oxide in a crystalline phase and tantalum oxide in an amorphous phase on a portion of an outer surface of the conductive substrate, and a second layer of the mixture comprising iridium oxide in an amorphous phase and tantalum oxide in an amorphous phase on an outer surface of the first layer.Type: GrantFiled: April 29, 2009Date of Patent: September 20, 2011Assignee: Freeport-McMoran CorporationInventors: Scot P Sandoval, Michael D Waite, Masatsugu Morimitsu, Casey J Clayton
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Patent number: 8022005Abstract: This invention relates to an activator, catalyst system, and the use thereof. In one aspect, the catalyst system includes one or more polymerization catalysts and at least one activator. The activator comprises one or more heterocyclic heteroatom containing ligands coordinated to an alumoxane, wherein the activator is a reaction product of one or more alumoxanes and one or more heterocyclic heteroatom containing compounds, the one or more heterocyclic heteroatom containing ligands represented by the formula: where Y is O, S, PH or NH; wherein each substituent X2, X3, X4, X5, X6, and X7 is independently selected from the group consisting of hydrogen, chlorine, fluorine, iodine, and bromine, provided at least one of X2, X3, X4, X5, X6 and X7 is not hydrogen when Y is NH; and wherein the ratio of the heterocyclic heteroatom containing ligand to aluminum is between about 0.01 and about 10 molar equivalents. The catalyst system may be supported or non-supported.Type: GrantFiled: November 8, 2007Date of Patent: September 20, 2011Assignee: ExxonMobil Chemical Patents Inc.Inventors: Matthew W. Holtcamp, Renuka N. Ganesh
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Patent number: 8022006Abstract: A catalyst nanoparticle covalently bonded to a surface ligand wherein the surface ligand has a peripheral functional group having a property suitable to ensure solubility in a fluid such as a hydroxylic solvent, water, lower molecular weight alcohol, methanol, ethanol, iso-propanol, or and mixtures thereof. The peripheral functional group can have an ability to couple the catalyst nanoparticle to a second catalyst nanoparticle or to a bridging material. The peripheral functional group can be capable of interacting with a surface functional group on a conductive electrode substrate. The covalently-bound ligand bearing a peripheral functional group can have a charge opposite to or chemical reactivity amenable with that of the surface functional group. A method of making a catalyst nanoparticle comprising bonding a surface ligand to a catalyst nanoparticle wherein the bonding is via a covalent bond and the surface ligand has a peripheral functional group.Type: GrantFiled: August 25, 2006Date of Patent: September 20, 2011Assignee: The United States of America as represented by the Secretary of the NavyInventors: Walter J. Dressick, Cynthia N. Kostelansky, Terence L. Schull
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Patent number: 8022007Abstract: The present invention relates to a ligand and its use in a catalyst for the oligomerization of olefinic monomers, the ligand having the general formula (II); P(R1)(R2)—P(R4)?N(R3)??(II) wherein: the R1 group is selected from a hydrocarbyl, substituted hydrocarbyl, heterohydrocarbyl and substituted heterohydrocarbyl group; the R2 group is selected from a hydrocarbyl, substituted hydrocarbyl, heterohydrocarbyl and substituted heterohydrocarbyl group; the R3 is selected from hydrogen, a hydrocarbyl group, a substituted hydrocarbyl group, a heterohydrocarbyl group, a substituted heterohydrocarbyl group, a silyl group or derivative thereof; the R4 group is an optionally substituted alkylenedioxy, alkylenedimercapto or alkylenediamino structure which is bound to the phosphorus atom through the two oxygen, sulphur or nitrogen atoms of the alkylenedioxy, alkylenedimercapto or alkylenediamino structure or an optionally substituted arylenedioxy, arylenedimercapto or arylenediamino structure which is bound to the phoType: GrantFiled: August 19, 2010Date of Patent: September 20, 2011Assignee: Shell Oil CompanyInventors: Eric Johannes Maria De Boer, Harry Van Der Heijden, Quoc An On, Johan Paul Smit, Arie Van Zon
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Patent number: 8022008Abstract: A method is provided for making a catalyst support, and includes the steps of providing an aqueous suspension of refractory inorganic oxide and refractory inorganic carbide; forming the suspension into droplets; exposing the droplets to a gelling agent whereby the droplets are at least partially solidified so as to provide substantially sphere-shaped portions of refractory inorganic oxide and refractory inorganic carbide; and drying and calcining the sphere-shaped portions so as to provide substantially spherical particles of catalyst support containing refractory inorganic oxide and refractory inorganic carbide. Catalytically active metal phases and hydrogenation processes using the catalyst are also described.Type: GrantFiled: November 30, 2009Date of Patent: September 20, 2011Assignee: Intevep, S.A.Inventors: Jorge M. Martinis, Maria E. Valera, Jose R. Velasquez, Angel R. Carrasquel
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Patent number: 8022009Abstract: The present invention provides a cost effective process of generating LixMyZO4/carbon composite material. Further, this novel method of preparation can be modified by adding a dopant and the calcinations can be carried out using microwave heating to reduce the synthesis time and cost. The LixMyZO4/carbon composite material can be used as a cathode for a secondary electrochemical cell. Selection of one or more metals in the cathode material can be used change the voltage, the capacity, and the energy density of the electrochemical cell.Type: GrantFiled: January 12, 2010Date of Patent: September 20, 2011Assignee: Intematix CorporationInventors: Biying Huang, Xiongfei Shen, Yi-Qun Li
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Patent number: 8022010Abstract: Nitrogen oxide storage materials and methods of manufacturing nitrogen oxide storage materials are disclosed. The nitrogen oxide storage materials can be used to manufacture catalytic trap disposed in an exhaust passage of an internal combustion engine which is operated periodically between lean and stoichiometric or rich conditions, for abatement of NOx in an exhaust gas stream which is generated by the engine. In one embodiment, the nitrogen oxide storage material comprises alkaline earth material supported on ceria particles having a crystallite size of between about 10 and 20 nm and the alkaline earth oxide having a crystallite size of between about 20-40 nm.Type: GrantFiled: July 6, 2009Date of Patent: September 20, 2011Assignee: BASF CorporationInventors: Marcus Hilgendorff, Stanley A. Roth, Susanne Stiebels
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Patent number: 8022011Abstract: A photocatalyst according to the invention comprises a photocatalytic film of a compound of titanium and oxygen and is characterized in that the photocatalytic film is made porous and has 0.02 or higher value as a value calculated by dividing the arithmetical mean deviation of profile Ra with the film thickness. The photocatalytic film can also be specified by the intensity ratio between x-ray diffraction peaks of the anatase structure of titanium oxide. Such a porous photocatalytic material can be obtained by a reactive sputtering method in conditions of adjusting film formation parameters such as the film formation rate, the sputtering pressure, the substrate temperature, the oxygen partial pressure and the like in proper ranges, respectively, and the photocatalyst material is provided with excellent decomposition and hydrophilization capability.Type: GrantFiled: April 28, 2010Date of Patent: September 20, 2011Assignee: Shibaura Mechatronics CorporationInventors: Junji Hiraoka, Takahiro Doke, Hisato Haraga, Daisuke Noguchi, Yoshio Kawamata
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Patent number: 8022012Abstract: A device for fabricating thin films on a substrate includes a vacuum chamber, a rotatable platen configured to hold one or more substrates within the vacuum chamber, and a housing disposed within the vacuum chamber. The housing contains a heating element and is configured to enclose an upper surface of the platen and a lower portion configured to partially enclose an underside surface of the platen which forms a reaction zone. A heated evaporation cell is operatively coupled to the lower portion of the housing and configured to deliver a pressurized metallic reactant to the reaction zone. The device includes a deposition zone disposed in the vacuum chamber and isolated from the reaction zone and is configured to deposit a deposition species to the exposed underside of the substrates when the substrates are not contained in the reaction zone.Type: GrantFiled: September 11, 2008Date of Patent: September 20, 2011Assignee: Superconductor Technologies, Inc.Inventors: Brian H. Moeckly, Ward S. Ruby
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Patent number: 8022013Abstract: A method of forming a solid-phase support, the method including the steps of providing a substrate having a reaction vessel, dispensing a particle in the reaction vessel, and permanently bonding the particle in the substrate within the reaction vessel. The particle may include a microbead. The particle may include controlled pore glass. A method of synthesis is also disclosed that includes including the steps of providing a solid-phase support including a particle embedded to the substrate adjacent a surface of substrate, the particle being functionalized to covalently attach an intermediate compound of a synthetic reaction, dispensing a liquid including a reagent to the solid-phase support to effect the synthetic reaction, and removing the liquid from the solid-phase support by centrifugation, whereby the intermediate compound remains attached to the substrate by the particle.Type: GrantFiled: August 29, 2003Date of Patent: September 20, 2011Assignee: Illumina, Inc.Inventors: Brett Ellman, Michal Lebl, Aaron Jones, Steve Fambro, David Heiner
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Patent number: 8022014Abstract: A method of solubilizing/removing cellulose or chemically-modified cellulosic polymers utilized in subterranean drilling operations such as fracturing. The method involves introducing a deep eutectic solvent (DES) into a subterranean region. Deep eutectic solvents useful as cellulose solvents include quaternary ammonium compounds, including choline chloride and chlorcholine chloride, reacted with a compound selected from amides, amines, carboxylic acids alcohols, and metal halides. The DES material can be pumped downhole after fracturing operations to remove cellulosic material used, for example, to thicken fracturing fluid which is left behind in the created fractures, on the face of the formation, along the wellbore, or elsewhere within the subterranean region. The DES can be used alone or in a sequential treatment protocol, whereby the DES is introduced into the subterranean region, followed by post-treatment introduction of water, caustic, acid or anhydride into the subterranean as a flush.Type: GrantFiled: March 25, 2009Date of Patent: September 20, 2011Inventor: Richard F. Miller
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Patent number: 8022015Abstract: Compositions and methods of treating high temperature subterranean formations of up to about 500° F. (260° C.) are provided. The compositions and methods utilize a high molecular weight synthetic copolymer and a pH buffer than maintains a pH in a range of about 4.5 to about 5.25 for the compositions. The high molecular weight synthetic copolymer is derived from acrylamide, acrylamidomethylpropanesulfonic acid, and vinyl phosphonate.Type: GrantFiled: January 28, 2008Date of Patent: September 20, 2011Assignee: Baker Hughes IncorporatedInventors: Paul S. Carman, Jeffrey C. Dawson
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Patent number: 8022016Abstract: There is a viscoelastic fluid. The fluid has one or more cationic surfactants selected from the group consisting of certain quaternary salts, certain amines, and combinations thereof; one or more anionic polymers/anionic surfactants; one or more of certain zwitterionic/amphoteric surfactants; and water. There is also a method of fracturing a subterranean formation. The viscoelastic fluid is pumped through a wellbore and into a subterranean formation at a pressure sufficient to fracture the formation. There is also a method for gravel packing a subterranean formation.Type: GrantFiled: February 25, 2010Date of Patent: September 20, 2011Assignee: Rhodia, Inc.Inventors: Fang Li, Manilal Dahanayake, Allwyn Colaco
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Patent number: 8022017Abstract: Corrosion of metallic tubulars in an oil, gas or geothermal well may be inhibited by introducing into the well a dithiazine of the formula: wherein R is selected from the group consisting of a C1 to C10 saturated or unsaturated hydrocarbyl group or a C1 to C10 ?-hydroxy saturated or unsaturated hydrocarbyl group. The dithiazine may be isolated from a whole spent fluid formed by reaction of hydrogen sulfide and a triazine. Alternately, the whole spent fluid containing the dithiazine may be introduced into the well. In addition, the dithiazine or whole spent fluid may be formulated with at least one component selected from alkyl, alkylaryl or arylamine quaternary salts; mono or polycyclic aromatic amine salts; imidazoline derivative or a quaternary salt thereof; a mono-, di- or trialkyl or alkylaryl phosphate ester; or a monomeric or oligomeric fatty acid.Type: GrantFiled: December 21, 2009Date of Patent: September 20, 2011Assignee: Baker Hughes IncorporatedInventor: Grahame Nigel Taylor
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Patent number: 8022018Abstract: Corrosion of metallic tubulars in an oil, gas or geothermal well may be inhibited by introducing into the well a dithiazine or dithiazine of the formula: wherein R is selected from the group consisting of a C1 to C12 saturated or unsaturated hydrocarbyl group or a C1 to C10 ?-hydroxy saturated or unsaturated hydrocarbyl group; R1 is selected from the group consisting of a C1-C24 straight chain or branched alkyl group or a C1-C24 arylalkyl; R2 is selected from the group consisting of X-R4-X, R4 being a C1-C6 alkyl group; and X is chlorine, bromine or iodine. The dithiazine may he isolated from a whole spent fluid formed by reaction of hydrogen sulfide and a triazine. Alternately, the whole spent fluid containing the dithiazine may be introduced into the well. The dithiazines of formulae (II) and (III) are quaternized derivatives of the dithiazine of formula (I).Type: GrantFiled: August 24, 2010Date of Patent: September 20, 2011Assignee: Baker Hughes IncorporatedInventor: Grahame Nigel Taylor
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Patent number: 8022019Abstract: Method and system for making a spherical proppant having a selected grade from a naturally occurring mined mineral having a hardness of over 6.0 Mohs. The method and system involves preprocessing the mineral mechanically into a semi-dry feedstock comprising a mass of particles with initial sphericity values generally less than 0.60; subjecting the semi-dry feedstock to an aggressive abrasive attrition operation for a process time; and, controlling the process time to a value wherein the particles of the feedstock are converted to final processed particles having a sphericity greater than 0.60 by increasing the sphericity of the feedstock particles by at least 0.10. In addition, the processed particles are screened to obtain a proppant having a selected grade.Type: GrantFiled: November 20, 2009Date of Patent: September 20, 2011Assignee: Unimin CorporationInventors: David John Rush, Juan Leal Gonzalez
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Patent number: 8022020Abstract: A penetrating lubricant with the capacity to offer a both penetration into rust and corrosion. Further, this lubricant actively penetrates the crystalline surface of the metal while exhibiting extreme pressure lubrication, non-migrating with lasting protection. Further lubricant exhibits dielectric strength of over 8000 volts, at the same time cleaning electrical contacts, thereby reducing resistance and associated heat. The preferred embodiment may contain alpha-olefins, low-odor aromatic solvents, base oils, and high flash mineral spirits.Type: GrantFiled: April 1, 2008Date of Patent: September 20, 2011Assignee: Bestline International Research, Inc.Inventor: Ronald J. Sloan
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Patent number: 8022021Abstract: The present invention relates to a controlled release gel with an ashless component and defined ash-producing component. Further, the invention relates to the use of a controlled release gel with a controlled level of ash-producing (i.e., metal) components for delivery of additives into lubricants wherein the gel has reduced ash and SAPS producing components.Type: GrantFiled: February 5, 2007Date of Patent: September 20, 2011Assignee: The Lubrizol CorporationInventors: James D. Burrington, Lewis A. Williams, Jack C. Kelley, David A. McCaughey, Frank M. van Lier, David B. Skursha
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Patent number: 8022022Abstract: A molybdated succinimide complex is disclosed which is prepared by a process comprising (a) reacting an alkyl or alkenyl succinimide of a polyamine of formula I wherein R is an about C12 to about C30 alkyl or alkenyl group; a and b are independently 2 or 3, and x is 0 to 10, with an ethylenically unsaturated carboxylic acid or anhydride thereof; and (b) reacting the product of step (a) with an acidic molybdenum compound. Also disclosed is a lubricating oil composition containing at least (a) a major amount of a base oil of lubricating viscosity and (b) a minor amount of the molybdated succinimide complex.Type: GrantFiled: June 30, 2008Date of Patent: September 20, 2011Assignee: Chevron Oronite Company LLCInventors: Kenneth D. Nelson, Edward A. Chiverton
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Patent number: 8022023Abstract: A molybdated succinimide complex is disclosed which is prepared by a process comprising (a) reacting a succinimide of a polyamine of formula I: wherein R is a hydrocarbon radical having a number average molecular weight of about 500 to about 5,000, a and b are independently 2 or 3, and x is 0 to 10, with an ethylenically unsaturated carboxylic acid or anhydride thereof, in a charge mole ratio of the ethylenically unsaturated carboxylic acid or anhydride thereof to the succinimide of formula I of about 0.9:1 to about 1.05:1; and (b) reacting the succinimide product of step (a) with an acidic molybdenum compound. Also disclosed is a lubricating oil composition containing at least (a) a major amount of a base oil of lubricating viscosity and (b) a minor amount of the molybdated succinimide complex.Type: GrantFiled: June 30, 2008Date of Patent: September 20, 2011Assignee: Chevron Oronite Company LLCInventors: Kenneth D. Nelson, Edward A. Chiverton
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Patent number: 8022024Abstract: A functional fluid comprising a base oil with a high viscosity index, wherein the functional fluid has a kinematic viscosity at 100° C. between 2.5 and 5.0 mm2/s, a low Brookfield viscosity, a high aniline point, and excellent air release. Shock absorber fluids with improved performance, comprising a particular base oil, wherein the improved performance includes high viscosity index, low Brookfield viscosity, high aniline point, excellent air release and high flash point.Type: GrantFiled: June 28, 2007Date of Patent: September 20, 2011Assignee: Chevron U.S.A. Inc.Inventors: Chantal R. Swartele, John M. Rosenbaum, Marc J. De Weerdt, Thomas Plaetinck, Stephen J. Miller, Mark L. Sztenderowicz
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Patent number: 8022025Abstract: A heterocoagulate comprises first particles, having a particle size of at most 999 nm, on a second particle, having a particle size of at least 3 microns. The first particles comprise cerium oxide, and second particle comprises at least one member selected from the group consisting of silicon oxides, aluminum oxides and zirconium oxides.Type: GrantFiled: January 27, 2010Date of Patent: September 20, 2011Assignee: Nanophase Technologies CorporationInventors: Abigail R. Farning, Harry W. Sarkas, Patrick G. Murray
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Patent number: 8022026Abstract: A method and composition for deodorizing soft surfaces such as carpeting and upholstery are disclosed. The method includes the spraying of a liquid composition on a soft surface and allowing the composition to absorb into the soft surface, form liquid agglomerations within the soft surface to the agglomerations can make contact with malodorants disposed within the soft surface. The composition is capable of penetrating rapidly and deeply into the soft surfaces for contacting odor-causing substances embedded therein. The composition comprises an active ingredient such as a glycol or triethanolamine. Other ingredients that contribute to the surface penetration and/or agglomeration formation include ethanol, water, fragrance and a combination of at least one nonionic and at least one ionic surfactant.Type: GrantFiled: June 7, 2007Date of Patent: September 20, 2011Assignee: S.C. Johnson & Son, Inc.Inventors: Peter N. Nguyen, Cary E. Manderfield, Maciej K. Tasz
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Patent number: 8022027Abstract: The present invention relates to a composition comprising: (i) a lipase; and (ii) a bleach catalyst that is capable of accepting an oxygen atom from a peroxyacid and transferring the oxygen atom to an oxidizeable substrate.Type: GrantFiled: January 22, 2007Date of Patent: September 20, 2011Assignee: The Procter & Gamble CompanyInventors: Philip Frank Souter, Neil Joseph Lant, Alan Thomas Brooker, Gregory Scot Miracle, Nicola Jane Binney, David Lee Daugherty
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Patent number: 8022028Abstract: The invention encompasses liquid cleaning compositions, for example, dish washing liquids, and methods of their manufacture and use, which possess enhanced cleaning ability. The cleaning compositions of the invention include acidic light duty liquid cleaning compositions with low toxicity and antibacterial efficacy on surfaces, for example, hard surfaces.Type: GrantFiled: June 17, 2008Date of Patent: September 20, 2011Assignee: Colgate-Palmolive CompanyInventors: Gregory Szewczyk, Caryn R. Westphal, Karen Wisniewski, Cynthia McCullar Murphy, David Frank Suriano
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Patent number: 8022029Abstract: Fabric softening compositions comprising polymeric materials capable of retaining volatile perfume ingredients are disclosed, as well as methods of softening fabrics.Type: GrantFiled: July 14, 2010Date of Patent: September 20, 2011Assignee: Colgate-Palmolive CompanyInventors: Guy Broze, Alain Jacques, Alexandrine Tuzi, Georges Yianakopoulos
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Patent number: 8022030Abstract: The present invention relates to the field of perfumery. More particularly, it concerns co-polymers, derived from a maleic anhydride derivative and a ethylenic derivative, comprising at least one ?-oxy or ?-thio carbonyl moiety capable of liberating an active molecule such as, for example, an ?,?-unsaturated ketone, aldehyde or carboxylic ester. The present invention concerns also the use of polymers or co-polymers in perfumery as well as the perfuming compositions or perfumed articles comprising the invention's compounds.Type: GrantFiled: October 5, 2007Date of Patent: September 20, 2011Assignee: Firmenich SAInventors: Damien Berthier, Andreas Herrmann
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Patent number: 8022031Abstract: A liquid aqueous composition comprising (i) a factor VII polypeptide, (ii) an agent suitable for keeping pH in the range of from about 4.0 to about 8.0; (iii) an agent selected from the list of: a calcium salt, a magnesium salt, or a mixture thereof; wherein the concentration of (iii) is at least 15 mM.Type: GrantFiled: June 24, 2003Date of Patent: September 20, 2011Assignee: Novo Nordisk Health Care A/GInventors: Birthe Lykkegaard Hansen, Michael Bech Jensen, Troels Kornfelt
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Patent number: 8022032Abstract: The method set out herein involves identifying the concentration of each of two or more active therapeutics tailored to treat a particular patient's unique metabolism and one or more diseases, communicating that information to a producer who has multiple fixed or variable concentrations of each active available, where the producer then combines the individual concentrations of each active into single units such as a tablets or pills, and distributes those indirectly or directly to the patient.Type: GrantFiled: November 18, 2005Date of Patent: September 20, 2011Assignee: SmithKline Beecham CorporationInventors: Richard L. Kirsh, Steven D. Finkelmeier, Robert Glinecke, Luigi Martini
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Patent number: 8022033Abstract: A complex of an echinocandin compound with a carbohydrate is described having improved thermal stability and water solubility. A process for making the echinocandin/carbohydrate complex is also described as well as the use of the complex in pharmaceutical formulations and treatments of fungal infections.Type: GrantFiled: May 21, 2009Date of Patent: September 20, 2011Assignee: Eli Lilly and CompanyInventors: Larry Arnold Larew, Nathaniel Milton, James Lawrence Sabatowski, Kenneth Philip Moder
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Patent number: 8022034Abstract: The present invention concerns combination of an amount of a GPR119 agonist with an amount of a dipeptidyl peptidase IV (DPP-IV) inhibitor such that the combination provides an effect in lowering a blood glucose level or in increasing a blood GLP-1 level in a subject over that provided by the amount of the GPR119 agonist or the amount of the DPP-IV inhibitor alone and the use of such a combination for treating or preventing diabetes and conditions related thereto or conditions ameliorated by increasing a blood GLP-1 level. The present invention also relates to the use of a G protein-coupled receptor to screen for GLP-1 secretagogues.Type: GrantFiled: November 2, 2009Date of Patent: September 20, 2011Assignee: Arena Pharmaceuticals, Inc.Inventors: Zhi-Liang Chu, James N. Leonard, Hussien A. Al-Shamma, Robert M. Jones