Abstract: A system for producing ammonia comprises a reactor configured for receiving nitrogen feed gas and hydrogen feed gas, the reactor comprising a catalyst configured to convert at least a portion of the nitrogen gas and at least a portion of the hydrogen feed gas to ammonia to form a reactant mixture comprising the ammonia and unreacted nitrogen feed gas and unreacted hydrogen feed gas, an adsorbent configured to selective adsorb at least a portion of the ammonia from the reactant mixture, and a recycle line to recycle the unreacted nitrogen feed gas, the unreacted hydrogen feed gas, and unabsorbed ammonia to the reactor.

Abstract: A method for the processing of potassium containing materials comprises: (i) Separation of a potassium containing mineral from gangue minerals; (ii) Acid leaching whereby substantially all potassium, iron, aluminum and magnesium is solubilized and mixed potassium/iron double salt formed; (iii) Selectively crystallizing the mixed potassium/iron double salt formed in the leach step (ii); (iv) Second separation to separate the mixed potassium/iron double salt formed in step (iii); (v) Thermal decomposition to produce an iron oxide, a potassium salt and one or more phosphates; (vi) Leaching the product of the thermal decomposition; (vii) Third separation to separate the iron oxide and phosphate from the potassium salt; (viii) Recovering the potassium salt by crystallization; (ix) Separating the iron oxide and phosphate of step (vii) by leaching and subsequent solid liquid separation; and (x) Precipitating phosphate from liquor produced in step (ix) through the addition of a base.

Abstract: Methods of forming two-dimensional transition metal dichalcogenide sheets are provided. The methods include adding a cross-linking agent to an activating agent to form a solution and mixing a two-dimensional transition metal dichalcogenide with the solution to form a mixture. The methods also include adding a cleaving agent to the mixture to form one or more contiguous sheets of transition metal dichalcogenide.

Abstract: A process is provided for obtaining a hematite-containing material that can be used for ironmaking. The process includes separating a leach residue from a hydrometallurgical refining plant into an overflow and an underflow using a wet cyclone under a condition that the wet cyclone is adjusted to have a setting between 1 ?m or less and 2 ?m or less as a classification particle size for the overflow. The process then includes separating the overflow into a strong magnetic substance and a weak magnetic substance using a strong-magnetic-field magnetic separator under a condition that magnetic field intensity is 5 to 20 [kGauss]. The process then includes using a superheated steam drying system for adjusting a moisture content of the strong magnetic substance after the separation, to be 10 wt % to 17 wt %.

Abstract: A composition of matter is disclosed which is a perovskite having a composition A2?xA?xB2?yB?yO6??, where A is a praseodymium (Pr) element at the A-site of the perovskite, A? is a strontium (Sr) element at the A-site of the perovskite, B is a cobalt (Co) element at the B-site of the perovskite, and B? is a manganese (Mn) element at the B-site of the perovskite, and where 0<x ?1 and 0<y<2. Also disclosed is an electrode material Conformally coated with the composition of matter. Also disclosed are methods of producing the composition of matter and conformally coating the electrode material. Also disclosed an electrode is conformally coated with a praseodymium strontium manganese perovskite and a method for the coating.

Abstract: A water treatment unit performs a normal operation during which discharge parts generate an electric discharge in a state where water flows into a treatment vessel and treated water flows out of the treatment vessel. When the water treatment unit starts operating, the water treatment unit performs a preparatory operation for a predetermined period of time before starting the normal operation. During the preparatory operation, the discharge parts generate an electric discharge in a state where an outflow of the water from the treatment vessel is stopped. As a result, the water which has been stagnating in the treatment vessel while the water treatment unit is not operating and in which bacteria have grown is sufficiently sterilized.

Abstract: A sandwich suppressor in an ion chromatography system in which loosely packed ion exchange resin of low density is disposed in the central sample stream flow channel. Also, a method of using the suppressor is described.

Abstract: Provided are a water treatment system and a water treatment process, which are capable of reproducing water containing salts with high water recovery. In the water treatment system (400) and the water treatment process of the present invention, after a calcium scale inhibitor and a silica scale inhibitor are supplied to water to be treated containing Ca ions, SO4 ions, carbonate ions, and silica, and the water to be treated is separated in a second demineralizing section (210) into second concentrated water in which the Ca ions, the SO4 ions, the carbonate ions, and the silica are concentrated and treated water. In a second crystallizing section (220), seed crystals of gypsum are supplied to the second concentrated water, whereby gypsum is crystallized and removed from the second concentrated water.

Abstract: In a water treatment system and a water treatment process, a scale inhibitor is supplied to water to be treated containing Ca ions, SO4 ions, carbonate ions, and silica, and the water to be treated is adjusted to a pH at which silica is soluble. The pH-adjusted water containing the calcium scale inhibitor is separated in a first demineralizing section into concentrated and treated water. In a first crystallizing section, seed crystals of gypsum are supplied to the first concentrated water, whereby gypsum is crystallized and removed from the first concentrated water. Silica in the water to be treated is removed from the first concentrated water on the downstream side of the first crystallizing section. Calcium carbonate in the water to be treated is removed from the first concentrated water on the upstream side of the first demineralizing section or the downstream side of the first crystallizing section.

Abstract: In the drinking water industry, pilot plants have played a big role in assisting water professionals, utilities, and engineering firms in generating information about the behavior of large full scale systems. Due to the identification of new contaminants, stringent regulations, and demand for improved water quality the demand for novel water treatment challenges across North America have significantly increased. A portable evaluation pilot skid (PEPS) accommodates all water qualities. A vent valve screen is mounted inside the contactor with holes large enough to prevent clogging. Air is introduced into the contactor prior to the screen. The screen is mounted such that it breaks the air into small bubbles creating the effect of a stone diffusor. Air flow is easily adjusted with a needle valve.

Abstract: A water treatment apparatus including a central electrode, and an outer periphery electrode, water to be treated being treated by applying a high voltage between the central electrode and the outer periphery electrode to thereby form a discharge in a discharge space between the central electrode and the outer periphery electrode and supplying the water to be treated as water droplets or a water film into the discharge space from above the discharge space, the water treatment apparatus further including a water droplet reformation unit connected to the outer periphery electrode, wherein the water droplet reformation unit captures, as trapped water, a portion of the water to be treated falling in the discharge space, performs water droplet reformation by causing the captured trapped water and gas containing oxygen supplied via a gas pipe to be mixed, and jets out water droplets formed by water droplet reformation into the discharge space.

Abstract: Disclosed herein is an aeration hose capable of diffusing bubbles of air within a body of water, comprising a) a hose portion derived from a composition, comprising a polyvinyl chloride resin; a first rubber component; a second rubber component; at least one copolymer; at least one low temperature plasticizer; at least one filler comprising titanium dioxide; at least one heat stabilizer; at least one internal lubricant; at least one antioxidant; and at least one biofouling agent, wherein the hose portion comprises an outer hose portion, an inner hose portion and a plurality of hose apertures capable of receiving and diffusing pressurized air, and wherein the hose is flexible and has no memory, wherein the hose apertures are provided therethrough the inner hose portion and the outer hose portion and proportionally spaced about the outer hose portion along a length of the hose portion.

Abstract: A glass fusion draw apparatus for molten glass stream thermal profile control, including: a first enclosure; and a first isopipe situated within the first enclosure, the first enclosure can include at least one first heating element assembly integral with the wall of the first enclosure, and the at least one first heating element is in proximity to a portion of molten glass stream over-flowing the first isopipe within the enclosure. The apparatus can also include a proximity or temperature sensing system associated with the first enclosure that senses and controls the thermal gradient properties of the molten glass stream or streams in the first enclosure. Also disclosed are methods of making and using the fusion apparatus.

Abstract: The invention relates to a process for manufacturing a flat ribbon of precursor glass for a glass-ceramic, comprising the continuous floating of the molten glass on a bath of molten metal in a float chamber, said glass being poured in the molten state at a temperature above its devitrification onset temperature onto the molten metal upstream of the chamber, said glass progressively forming a ribbon that runs along said metal bath, the cooling rate of the glass being at least 18° C./min between, on the one hand, the moment when the glass is at the theoretical temperature for which the devitrification rate is a maximum and, on the other hand, the later moment when the glass is at the theoretical temperature at which the devitrification crystal growth rate becomes less than 1 micron per minute. The glass thus floated does not undergo any devitrification.

Abstract: A process and an apparatus for imparting coloration to a glass container having a strikable glass container composition. One or more portions of the glass container are selectively and locally exposed to a temperature at or above a glass container striking temperature to affect a color change in the one or more portions of the glass container. The coloration process may be carried out by passing the glass container through an interior of an apparatus having a heating system configured to locally heat a first region within the interior to a temperature at or above a glass container striking temperature and a cooling system to locally cool a second region within the interior to a temperature below the glass container striking temperature.

Abstract: A sensitized, photo-structurable glasses and methods for producing are provided. The glasses includes Si4+, one or more crystal-agonist, one or more crystal-antagonist, and one or more pair of nucleating agents. The glasses are sensitized in that the glass reacts more sensitive to irradiation with UV-light and can be crystallized easier and with higher aspect ratios than a non-sensitized glass with equal composition. Furthermore, the sensitized glasses of this invention have smaller crystal sizes after irradiation and tempering than a non-sensitized glass with equal composition. The invention also relates to a structured glass product. Such product can be obtained by submitting the crystallized glass product to a subsequent etching step. The structured product can be used in components or as component for the application fields micro-technology, micro-reaction-technology, electronic packaging, micro-fluidics, FED spacer, bio-technology, interposer, and/or three-dimensional structured antennae.

Abstract: Certain example embodiments of this invention relate to articles including anticondensation and/or low-E coatings that are exposed to an external environment, and/or methods of making the same. In certain example embodiments, the anticondensation and/or low-E coatings may be survivable in an outside environment. The coatings also may have a sufficiently low sheet resistance and hemispherical emissivity such that the glass surface is more likely to retain heat from the interior area, thereby reducing (and sometimes completely eliminating) the presence condensation thereon. The articles of certain example embodiments may be, for example, skylights, vehicle windows or windshields, IG units, VIG units, refrigerator/freezer doors, and/or the like.

Abstract: A prepreg having low water absorption, and having remarkably suppressed deterioration in insulation resistance over time, and further having excellent heat resistance, a metal foil-clad laminate using the prepreg, and a printed wiring board using the metal foil-clad laminate are provided. A prepreg of the present invention is obtained by impregnating or coating a base material (D) with a resin composition comprising: a naphthol-modified dimethylnaphthalene formaldehyde resin (A); an epoxy resin (B) having an epoxy equivalent of 200 to 400 g/eq.; and an inorganic filler (C).

Abstract: A manufacturing facility for quicklime is provided, which can manufacture highly active quicklime by a simple manufacturing facility, and which can also separate and recover, in a high concentration, CO2 gas generated at the time of manufacturing quicklime.

Abstract: Denitrifying bypass exhaust gases in a cement clinker producing plant. The plant comprises a rotary kiln connected to a calciner for the deacidification of raw material or to a rotary kiln riser shaft via a rotary kiln inlet chamber, and the bypass exhaust gas being drawn off in the region of the rotary kiln inlet chamber. The method comprises: cooling the bypass gas to between 260 C and 400 C in a cooling device, injecting an ammonia-, urea-, and/or ammonium-containing substance into the cooled bypass gas, introducing the cooled and mixed bypass gas into a ceramic filter system to filter out any halide and sulfate of the alkali metals and alkaline-earth metals precipitated during cooling the gas, and any nitrogen not reacted by the injected substances is chemically selectively reduced over a catalytic converter which is located in or directly downstream of the ceramic filter system.

Abstract: A method for producing granulates, particularly for use as thermal insulation for a metal melt may include mixing a powdery mineral with a binder, and the mixture may be granulated in order to produce a semi-finished product. The granulate mixture or the semi-finished product may be heated rapidly to a temperature above the melting temperature or decomposition temperature of the binder, which may be in the form of a salt, so that the binder decomposes, whereby gas is released and the volume increases. The apparent density of the granulate mixture may decrease, and therefore the apparent density of the finished product may decrease with respect to the semi-finished product.

Abstract: A nanoheterostructure includes a first inorganic component and a second inorganic component one of which is a matrix, and the other of which is three-dimensionally and periodically arranged in the matrix, and has a three-dimensional periodic structure whose average value of one unit length of a repeated structure is 1 nm to 100 nm.

Abstract: A friction material including two or more kinds of titanates and a ceramic fiber. The friction material includes no copper component. The two or more kinds of titanates may optionally include two or more kinds of alkali metal titanates, or the two or more kinds of titanates may optionally include an alkaline earth metal-alkali metal titanate and an alkali metal titanate.

Abstract: A composition that may be used to retain moisture within fresh concrete as it cures to optimize the curing of the concrete may include one or more hardening and densifying agents and one or more temporary moisture sealing agents. Additionally such a composition may include a siliconate. The hardening and densifying agent of such a composition may penetrate the surface of fresh concrete to react with free lime, providing the fresh concrete with a strong surface. The temporary moisture sealing agent may form a moisture barrier on the surface of the fresh concrete to prevent moisture from escaping from the fresh concrete before the fresh concrete has sufficiently cured. The temporary moisture sealing agent may degrade within a matter of days, facilitating its removal from the surface of the concrete once the concrete has cured and enabling further treatment of the surface without undue delay.

Abstract: The disclosed invention relates to a liquid treatment system comprising a fluid input channel and a plasmatron coupled to the fluid input channel, the plasmatron operative to affix nitrogen to liquid received from the fluid input channel resulting in treated liquid. The system further comprises a liquid chamber connected to the plasmatron for storing treated liquid and a treated fluid output channel connected to the liquid chamber.

Abstract: Disclosed is a process for making a water-soluble granule enriched in humic acid. Disclosed also is a water-soluble granule enriched in humic acid. Such a granule is useful as an organic aid to crop growth, particularly in applications where solubility is desirable or necessary.

Abstract: The present application discloses an improved electrically controlled propellant wherein the electrically controlled propellant comprises at least one compound selected from the group comprising organosilanes, siloxanes, and poly(dimethylsiloxane)s.

Abstract: A process for the production of jet and other heavy fuels from alcohols and mixture of alcohols is disclosed. The process may include contacting in a reaction zone at least one C2 to C11 alcohol with a solid catalyst having activity for the simultaneous dehydration of the alcohols to form olefins, isomerization of the olefins to form internal olefins, and oligomerization of the olefins produced in situ via the dehydration reaction to form an effluent comprising mono-olefinic hydrocarbons. Preferably, the alcohol feed is a mixture of alcohols, such as C2 to C7 alcohols or C4 and C6 alcohols, enabling the production of a mixture of branched hydrocarbons that may be used directly as a jet fuel without blending.

Abstract: Disclosed is a process and apparatus for switching oligomerization feed between a first oligomerization zone that includes a uni-dimensional small pore zeolite to make more diesel and a second oligomerization zone that includes SPA catalyst for making more gasoline. The diesel can be recycled to make more propylene. The process and apparatus will provide refiners with flexibility to produce the most valuable product commensurate with fluctuating market conditions.

Abstract: An alkylation process utilizing less than 10 vol % of a halometallate based ionic liquid catalyst is described. By decreasing the catalyst volume fraction, the level of subsequent undesirable reactions may be minimized. The total residence time is typically in the range of about 1 min to about 30 min. The alkylate typically has a research octane number of at least about 93, and the olefin conversion is typically at least about 96%.

Abstract: Alkylation processes are described. The processes utilize ionic liquid catalysts having a kinematic viscosity range of about 50 cSt to about 100 cSt at 25° C. Catalysts within this range produce alkylate having higher octane than catalysts outside this range, especially at higher process temperatures which are preferable from an operating cost standpoint. The alkylate can have one or more of a research octane number of at least about 93, a selectivity of C8 of at least about 65%, and a mole ratio of trimethylpentane to dimethylhexane of greater than about 7:1.

Abstract: A process includes hydrogenating, in a reaction zone, a highly unsaturated hydrocarbon received from a hydrocarbon stream to yield a product having an unsaturated hydrocarbon, the hydrogenating step occurring in the presence of a hydrogenation catalyst which has a selectivity for conversion of the highly unsaturated hydrocarbon to the unsaturated hydrocarbon of about 90 mol % or greater based on the moles of the highly unsaturated hydrocarbon which are converted to the product, the hydrogenating step occurring in a reaction zone under conditions which include a flow index (IF) in a range of about 0.09 to about 35, wherein the IF is defined as: I F = F × [ CO ] V , wherein F is the flow rate of the hydrocarbon stream into the reaction zone in units of kg/h, [CO] is the concentration of carbon monoxide in the hydrocarbon stream in units of mol %, and V is the volume of the reaction zone in units of ft3.

Abstract: Fluidizable catalysts for oxygen-free oxidative dehydrogenation of alkanes to corresponding olefins. The catalysts contain 10-20% (by weight per total catalyst weight) of one or more vanadium oxides as the catalytic material, which are mounted upon an alumina support that is modified with zirconia at alumina/zirconia ratios of 5:1 up to 1:2. Various methods of preparing and characterizing the fluidizable catalysts are also provided.

Abstract: Disclosed is a process and system to convert acyclic C5 feedstock to non-aromatic, cyclic C5 hydrocarbon. A furnace and reactor tubes comprising a catalyst compound are disclosed. A process involving contacting acyclic C5 feedstock with catalyst composition and obtaining cyclic C5 hydrocarbon is also disclosed.

Abstract: One or more processes for recovering entrained ionic liquid from a hydrocarbon phase containing droplets of ionic liquid are described. The processes includes contacting the hydrocarbon phase containing the droplets of ionic liquid with a retaining material in a separation zone. The droplets of ionic liquid are retained by the retaining material. The ionic liquid may be recovered from the retaining material with a solvent or desorbent. The retaining material may be regenerated and the ionic liquid may be reactivated. The retaining material may be used in a wash vessel to retain or remove contaminant solids within the reactor or other vessels.

Abstract: Provided is a process for making 2-chloro-1,1,1,2-tetrafluoropropane. The process has the step of hydrofluorinating 2-chloro-3,3,3-trifluoropropene in the presence of a catalyst selected from the group consisting of SbCl3, SbCl5, SbF5, TiCl4, SnCl4, Cr2O3, and fluorinated Cr2O3.

Abstract: The preparation of high-quality oxo process alcohols from inconstant raw material sources is the technically demanding problem which is addressed by a process for continuously preparing an alcohol mixture, in which an input mixture which contains an olefin and has a composition that changes over time is subjected to an oligomerization to obtain an oligomerizate and at least a portion of the olefin oligomers present in the oligomerizate are hydroformylated with carbon monoxide and hydrogen in a hydroformylation in the presence of a homogeneous catalyst system to give aldehydes, at least some of which are converted to the alcohol mixture by subsequent hydrogenation. The process provides a constant plasticizer quality to be produced over a long production period and, optionally, a higher throughput with the same product quality.

Abstract: Disclosed are a highly efficient neopentyl glycol preparation method and a device therefor. The method includes adding a hydroxypivaldehyde solution and hydrogen to a hydrogenation reactor that includes a hydrogenation catalyst. The hydroxypivaldehyde solution includes 6 to 30% by weight of hydroxypivaldehyde, 35 to 70% by weight of neopentyl glycol, 10 to 30% by weight of alcohol, and 10 to 30% by weight of water. The neopentyl glycol preparation method does not require separate heating in a section of a feed vessel to an inlet of a hydrogenation reactor unlike conventional technologies to save energy, and, at the same time, by-products with a high boiling point are not generated in the section to prevent poisoning of a hydrogenation catalyst in a reactor due to the by-products with a high boiling point and increase a hydrogenation yield, and a device therefor can be provided.

Abstract: A method of synthesizing fuel from an aqueous solution includes pumping the aqueous solution, containing dissolved inorganic carbon, from a body of water into a carbon extraction unit. The method further includes extracting the dissolved inorganic carbon from the aqueous solution to create CO2 by changing a pH of the aqueous solution in the carbon extraction unit. The CO2 derived in the carbon extraction unit is received by a fuel synthesis unit, and the CO2 is converted into fuel including at least one of a hydrocarbon, an ether, or an alcohol using the fuel synthesis unit.

Abstract: Allyl alcohol production processes are generally described herein. One or more of the processes generally include contacting a propylene oxide stream with an isomerization catalyst under isomerization conditions sufficient to form an isomerization product stream including allyl alcohol, wherein the propylene oxide stream includes a total impurity concentration of at least 100 ppm. One or more of the processes generally includes purging at least a portion of a stream from one or more separation unit(s).

Abstract: A system for, and method of, recovering salt from fluid stream in a recycle loop of a flash separator has a desanding hydrocyclone located in the hot recycle loop of the flash separator; a first solids fluidization device located at the bottom end of the flash separator's brine column; a second desanding hydrocyclone arranged to receive a salt slurry stream created by the first solids fluidization device; and an accumulator located downstream of the second desanding hydrocyclone and having a second solids fluidization device located at its bottom end. Each solids fluidization device causes a motive fluid to exit the device in a swirling motion to fluidize the salt components contained in the resident fluid. The overflow from the second desanding hydrocyclone is the motive fluid for the brine column and a produced water, condensate water, or seawater stream is the motive fluid for the accumulator.

Abstract: A method of producing fatty alcohols comprises: introducing a fatty alcohol feedstock stream to a distillation column; forming a light outlet stream and a heavy outlet stream; condensing at least a portion of the light outlet stream to form a reflux stream; returning the reflux stream to a reflux inlet of the distillation column at a reflux ratio of greater than or equal to 2; and recovering a fatty alcohol product stream from an outlet of the distillation column, wherein the fatty alcohol product stream comprises a first mass percentage of the first fatty alcohol species (M), and a second mass percentage of the second fatty alcohol species (M2), and wherein a fatty alcohol mass ratio (M1/M2) of the fatty alcohol product stream is the first mass percentage divided by the second mass percentage, and wherein the fatty alcohol mass ratio is greater than or equal to 2.0.

Abstract: A composition containing a novel vinyl-group-containing compound. This composition contains a vinyl-group-containing compound represented by general formula (1). In the formula: W1 and W2 represent a group represented by general formula (2) (where a ring (Z) is an aromatic hydrocarbon ring, X is a single bond or —S—, R1 is a single bond or a C1-4 alkylene group, R2 is a specific substituent group such as a monovalent hydrocarbon, and m is an integer equal to 0 or higher), a group represented by general formula (4) (where the ring (Z), X, R1, R2, and m are as previously stated), a hydroxyl group, or a (meth)acryloyloxy group; rings (Y1, Y2) are aromatic hydrocarbon rings; R represents a single bond or a specific divalent group; R3a and R3b represent a cyano group, a halogen atom, or a monovalent hydrocarbon group; and n1 and n2 are integers of 0-4.

Abstract: The present invention belongs to the field of pharmaceutical technology, more specifically relates to optically pure benzyl-4-chlorophenyl-C-glucoside derivatives represented by formulae (II) and (III), a process for preparing these compounds and intermediates thereof, a pharmaceutical formulation and a pharmaceutical composition containing these compounds, and the use of the optically pure benzyl-4-chlorophenyl-C-glucoside derivative as a sodium glucose co-transporter (SGLT) inhibitor in manufacture of a medicament for treating and/or preventing diabetes mellitus (including insulin-dependent diabetes mellitus and non-insulin-dependent diabetes mellitus) or diabetes-associated diseases (including insulin resistance disease and obesity)

Abstract: In one aspect, the present invention encompasses integrated processes for the conversion of epoxides to acrylic acid derivatives and polyesters. In certain embodiments, the methods of the present invention comprise the steps of: providing a feedstock stream comprising an epoxide and carbon monoxide; contacting the feedstock stream with a metal carbonyl in a first reaction zone to effect conversion of at least a portion of the provided epoxide to a beta lactone; directing the effluent from the first reaction zone to a second reaction zone where the beta lactone is subjected to conditions that convert it to a compound selected from the group consisting of: an alpha beta unsaturated acid, an alpha beta unsaturated ester, an alpha beta unsaturated amide, and an optionally substituted polypropiolactone polymer; and isolating a final product comprising the alpha-beta unsaturated carboxylic acid, the alpha-beta unsaturated ester, the alpha-beta unsaturated amide or the polypropiolactone.

Abstract: The present invention relates to catalytic conversion of ketoacids, including methods for increasing the molecular weight of ketoacids. The method can include providing in a reactor a raw material having at least one ketoacid. The raw material is then subjected to one or more C—C-coupling reaction(s) in the presence of an ion exchange resin catalyst to produce at least one ketocid dimer. The method can include providing in a reactor a feedstock having the at least one ketoacid dimer and subjecting the feedstock to one or more C—C-coupling reaction(s) at a temperature of at least 200° C.

Abstract: The first subject matter of the invention is the (3R) epimer of octahydro-7,7-dimethyl-8-methylene-1H-3a,6-methanoazulen-3-yl acetate [(octahydro-7,7-dimethyl-8-methylene-[3R,3aR,6R,8aR]-1H-3a,6-methanoazulen-3-yl acetate) or (R)-norzizaenylacetate] of formula I (I). The subject matter of the invention is also compositions comprising (R)norzizaenyl acetate and also a novel synthesis process and the use of said ester.

Abstract: Provided is a process for preparing 4-phenyl-1-butyric acid, comprising: reacting 4-phenyl-1-butanol with sodium chlorite, a nitroxyl radical catalyst and sodium hypochlorite in an organic solvent and a phosphate buffer; and quenching the reaction with sodium sulfite to produce 4-phenyl-1-butyric. Also provided is 4-phenyl-1-butyric acid prepared by such a process.

Abstract: The present invention relates to a process for preparing ethylenediamine (EDA), where the process comprises the steps a) to c). In step a), formaldehyde is reacted with hydrocyanic acid (HCN) to form formaldehyde cyanohydrin (FACH), where the hydrocyanic acid is completely free or largely free of sulfur dioxide (SO2). The FACH prepared in this way is reacted with ammonia (NH3) to form aminoacetonitrile (AAN) in step b), whereupon a hydrogenation of AAN in the presence of a catalyst to form EDA is carried out in step c).

Abstract: The present invention relates to a method for the purification of cadaverine from an aqueous cadaverine salt composition comprising one or more involatile impurities, the method comprising: (1) mixing the aqueous cadaverine salt composition with one or more bases selected from the group consisting of Ca(OH)2, Mg(OH)2, CaO and MgO to provide an aqueous cadaverine composition; and (2) distilling or evaporating the aqueous cadaverine composition to produce purified cadaverine; wherein one or more solvents are added to the evaporation/distillation system before the evaporation/distillation stops, and the one or more solvents comprise at least one or more high boiling point (HBP) solvents.