Patents Issued in April 3, 2018
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Patent number: 9932480Abstract: A process of forming a multi-layered pigment includes the steps of: providing a metal core material; dispersing the metal core material in a first solvent and organic binder mixture; depositing a high refractive index material onto the metal core material; drying the deposited high refractive index and metal core material wherein the high refractive index layer is uniform and crack-free.Type: GrantFiled: July 3, 2014Date of Patent: April 3, 2018Assignees: Toyota Motor Engineering & Manufacturing North America, Inc., Toyota Jidosha Kabushiki KaishaInventors: Khoa Vo, Songtao Wu, Debasish Banerjee, Masahiko Ishii
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Patent number: 9932481Abstract: Actuatable microstructures and methods of making the same are disclosed. An example a sheet includes a first side including an elastomeric material and a second side opposite the first side. The sheet defines sealed channels. In response to a pressure differential across the elastomeric material, the elastomeric material is to be in a deformed position relative to the sealed channels to define microstructures.Type: GrantFiled: April 21, 2015Date of Patent: April 3, 2018Assignee: The Boeing CompanyInventor: Weidong Song
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Patent number: 9932482Abstract: The present disclosure describes a strategy to create self-healing, slippery liquid-infused porous surfaces (SLIPS). Roughened (e.g., porous) surfaces can be utilized to lock in place a lubricating fluid, referred to herein as Liquid B to repel a wide range of materials, referred to herein as Object A (Solid A or Liquid A). SLIPS outperforms other conventional surfaces in its capability to repel various simple and complex liquids (water, hydrocarbons, crude oil and blood), maintain low-contact-angle hysteresis (<2.5°), quickly restore liquid-repellency after physical damage (within 0.1-1 s), resist ice, microorganisms and insects adhesion, and function at high pressure (up to at least 690 atm). Some exemplary application where SLIPS will be useful include energy-efficient fluid handling and transportation, optical sensing, medicine, and as self-cleaning, and anti-fouling materials operating in extreme environments.Type: GrantFiled: April 20, 2016Date of Patent: April 3, 2018Assignee: President and Fellows of Harvard CollegeInventors: Joanna Aizenberg, Michael Aizenberg, Sung Hoon Kang, Philseok Kim, Tak Sing Wong
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Patent number: 9932483Abstract: The present invention relates to a solventborne primer surfacer which comprises at least one additive preparable by reacting at least one alpha,omega-hydroxy-functionalized oligoester which possesses an OH number of 30 to 160 mg KOH/g, a theoretical carbon-carbon double bond content of 1 to 2.5 mmol/g, a number-average molecular weight of 1000 to 3000 g/mol, and a weight-average molecular weight of 2800 to 10 000 g/mol, and at least one alkoxysilane which possesses an OH-reactive functional group, the sum of the weight percentage fractions of all additives of the invention being 0.5 to 10 wt %, based on the total amount of the solventborne primer surfacer. The present invention further relates to a process for producing multicoat paint systems, and to multicoat paint systems producible by means of said process. The invention further relates to the use of the additive identified above in solventborne primer surfacers for improving adhesion.Type: GrantFiled: December 17, 2014Date of Patent: April 3, 2018Assignee: BASF Coatings GmbHInventors: Audree Andersen, Cathrin Corten, Manuela Niemeier, Frederik Foelling, Simone Hesener, Nicole Freitag, Stefanie Boshe-Plois
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Patent number: 9932484Abstract: A self-healing, scratch resistant slippery surface that is manufactured by wicking a chemically-inert, high-density liquid coating over a roughened solid surface featuring micro and nanoscale topographies is described. Such a slippery surface shows anti-wetting properties, as well as exhibits significant reduction of adhesion of a broad range of biological materials, including particles in suspension or solution. Specifically, the slippery surfaces can be applied to medical devices and equipment to effectively repel biological materials such as blood, and prevent, reduce, or delay coagulation and surface-mediated clot formation. Moreover, the slippery surfaces can be used to prevent fouling by microorganisms such as bacteria.Type: GrantFiled: January 19, 2012Date of Patent: April 3, 2018Assignee: President and Fellows of Harvard CollegeInventors: Joanna Aizenberg, Benjamin Hatton, Donald Ingber, Michael Super, Tak Sing Wong
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Patent number: 9932485Abstract: A film, coating, appliqué and method to eliminate paint removal via hazardous methods and maintain effective corrosion inhibition via employment of a re-useable coating. Embodiments of the invention generally relate to a multilayer film having a first layer constructed of at least one electro-active polymer, a second layer constructed of at least one flexible electrically-conductive solid, and a third layer constructed of at least one inert polymer.Type: GrantFiled: January 20, 2016Date of Patent: April 3, 2018Assignee: The United States of America as Represented by the Secretary of the NavyInventors: Peter Zarras, John Stenger-Smith, William Lai
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Patent number: 9932486Abstract: The invention is comprised of a coalescent and non-ionic surfactant blend additive for use in water-based architectural coating formulations. The dual-function blend is produced by reacting 2,2,4-trimethyl-1,3-pentanediol monoisobutyrate with ethylene oxide in the presence of a basic catalyst and separating the desired ethoxylated coalescent and non-ionic surfactant blend from the reaction product.Type: GrantFiled: October 5, 2016Date of Patent: April 3, 2018Assignee: Eastman Chemical CompanyInventors: Jennifer Lynn Cogar, Damon Ray Billodeaux, Jerome Leonard Stavinoha, Jr., Michelle Nicole Tuttle
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Patent number: 9932487Abstract: The present invention relates to a thermosensitive recording material comprising paper, an undercoat layer disposed on the paper, and a thermosensitive recording layer disposed on the undercoat layer, wherein the undercoat layer comprises a binder and first and second hollow sphere polymer particles, wherein the first hollow sphere polymer particles have a diameter in the range of from 1.2 ?m to 1.8 ?m; the second hollow sphere polymer particles have a diameter in the range of from 0.25 ?m to 1.0 ?m; the number ratio of the second to the first hollow sphere polymer particles is in the range of from 1:1 to 20:1; the diameter of the second hollow sphere polymer particles is in the range of from 15 to 65% of the diameter of the first hollow sphere polymer particles; the dry bulk density of the first hollow sphere polymer particles is in the range of 0.25 to 0.5 g/mL; and the dry bulk density of the second hollow sphere polymer particles is in the range of 0.30 to 0.90 g/mL.Type: GrantFiled: December 1, 2016Date of Patent: April 3, 2018Assignees: Rohm and Haas Company, Dow Global Technologies LLCInventors: Brian R. Einsla, Valeriy V. Ginzburg, Lanfang Li, John A. Roper, III, Rebecca Smith, Jian Yang
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Patent number: 9932488Abstract: A resin composition including from 30 to 99 wt % of a cellulose-based resin represented by the following formula (1) and from 70 to 1 wt % of a fumaric acid ester polymer containing 30 mol % or more of a fumaric acid diester residue unit represented by the following formula (2); an optical compensation film using the same; and a production method of the optical compensation film. (wherein R1 to R3 represent a substituent having a carbon number of 1 to 12, and R4 and R5 represent an alkyl group having a carbon number of 1 to 12).Type: GrantFiled: June 4, 2014Date of Patent: April 3, 2018Assignee: TOSOH CORPORATIONInventors: Masayasu Ito, Shinsuke Toyomasu, Takahiro Kitagawa
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Patent number: 9932489Abstract: The invention relates to improved non-efflorescing cement-free and water-dispersible powder building material compositions comprising a homopolymer or copolymer as binder, useful for the preparation of wet formulations of plasters grouts, waterproofing coatings or mortars for the construction and the civil engineering industry. The binder is obtained by spray-drying or lyophilization of a dispersion containing a polymer and a protective colloid. These compositions also comprise a deprotection agent and a specific adsorbent filler. The invention also refers to the methods of preparation of these dry compositions and wet formulations, the application of these latter onto the surface of buildings or civil engineering works, the so obtained coatings as well as the so coated elements. The hardened products obtained therefrom are remarkably water-resistant, non efflorescent and easy to obtain.Type: GrantFiled: July 13, 2011Date of Patent: April 3, 2018Assignee: PAREXGROUP SAInventors: Veronique Dantin, Gerard Leplay, Paulo Goncalo, Carlos Nones, Pedro Paredes
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Patent number: 9932491Abstract: A method for preparing an emulsion for a cationic electrodeposition coating composition at an emulsification field, wherein the method includes synthesizing a base resin for a cationic electrodeposition coating composition, removing the base resin in a liquid state from a reaction vessel and then changing the resin into a solid state, and optionally, adjusting a size of the resin into an predetermined size, and emulsifying the resin at the emulsification field by adding water and an optional solvent, a neutralizing agent, a curing agent or additives, wherein the base resin is an aminated resin and has a softening point of 20-90° C., and wherein the adjusted shortest size of the base resin is 40 cm or less. Furthermore, the present application relates to a method for transporting a resin for cationic electrodeposition coating composition.Type: GrantFiled: March 24, 2015Date of Patent: April 3, 2018Assignee: NIPPON PAINT AUTOMOTIVE COATINGS CO., LTD.Inventors: Takeshi Hara, Nobuhiro Miyamae, Makoto Andou, Masahiko Harada, Noriyuki Nakazawa
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Patent number: 9932492Abstract: Disclosed is an oxidatively drying alkyd resin composition and a method for preparing said composition. Said composition is obtained by admixing an aqueous silica sol into a substantially 100% alkyd resin being in a liquid state either at ambient temperature or at an elevated temperature. Said silica sol is added in an amount of 0.1-10% by weight calculated as 100% silica on 100% alkyd resin. The use of a said composition is in a further aspect disclosed.Type: GrantFiled: December 20, 2012Date of Patent: April 3, 2018Assignees: PERSTORP AB, DYRUP A/SInventors: Kent Sorensen, David Lof
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Patent number: 9932493Abstract: Disclosed are one-component compositions that include: (1) an isocyanate-functional urethane acrylate and (2) a polyisocyanate containing allophanate and/or uretdione groups, wherein the one-component composition has a viscosity of less than or equal to about 800 mPa·s and an isocyanate content of greater than about 5% by weight, based on the weight of the one-component composition. Also disclosed are circuit boards and electronic components that are coated with such compositions.Type: GrantFiled: January 10, 2014Date of Patent: April 3, 2018Assignee: Allnex Netherlands B.V.Inventors: Abdullah Ekin, Michael J Dvorchak
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Patent number: 9932494Abstract: Disclosed are a resin composition and a molded product obtained using the same. By using the resin composition according to the present invention, a molded product having excellent tensile strength, tensile modulus, electromagnetic shielding effects, anti-static effects, and the like may be provided.Type: GrantFiled: August 28, 2014Date of Patent: April 3, 2018Assignee: LG CHEM, LTD.Inventors: Yeon Sik Choi, Su Min Lee, Chang Hun Yun, Gi Dae Choi
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Patent number: 9932495Abstract: Coating compositions that provide hydrophilic and self-cleaning properties upon exposure to an electromagnetic spectrum are disclosed. Coatings can include lignin-coumarate derivatives and/or lignin-azobenzene derivatives. When exposed to the electromagnetic spectrum, these compounds isomerize to cis-configuration which are hydrophilic in nature as compared to when these compounds are in their hydrophobic trans-state.Type: GrantFiled: April 23, 2015Date of Patent: April 3, 2018Assignee: Empire Technology Development LLCInventor: Sivaraman Raghu
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Patent number: 9932496Abstract: Disclosed are various embodiments relating to a liquefied wood coating that can be applied to virtually any surface. The liquefied wood coating contains a micronized wood powder, a non-elastomeric resin with high adhesion properties, and an elastomeric resin for flexibility. Once dried, the wood coating accepts stain, polyurethane, and other types of coatings to provide a real wood finish.Type: GrantFiled: January 21, 2015Date of Patent: April 3, 2018Assignee: ADVANCED WOOD PAINT, LLCInventor: Christopher R. Boest
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Patent number: 9932497Abstract: A polishing liquid comprising an abrasive grain, an additive, and water, wherein the abrasive grain includes a hydroxide of a tetravalent metal element, produces absorbance of 1.00 or more and less than 1.50 for light having a wavelength of 400 nm in an aqueous dispersion having a content of the abrasive grain adjusted to 1.0 mass %, and produces a liquid phase having a content of a non-volatile component of 300 ppm or more when centrifuging an aqueous dispersion having a content of the abrasive grain adjusted to 1.0 mass % for 50 minutes at a centrifugal acceleration of 1.59×105 G.Type: GrantFiled: March 26, 2013Date of Patent: April 3, 2018Assignee: HITACHI CHEMICAL COMPANY, LTD.Inventors: Tomohiro Iwano, Hisataka Minami, Toshiaki Akutsu, Koji Fujisaki
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Patent number: 9932498Abstract: A method to create a roll of double sided tape with at least one longitudinal or el-tab along the circumference of the entire roll of double sided tape. These rolls having the el-tab already within the roll can be placed directly into specialized cutting machines.Type: GrantFiled: September 11, 2012Date of Patent: April 3, 2018Assignee: TABBED TAPE-STRIP CORP.Inventor: Joseph P. McGee
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Patent number: 9932499Abstract: The present invention relates to a polymerizable composition, comprising a polymerizable monomer of formula (I), a copolymerizable UV-initiator, at least one copolymerizable (meth)acrylic monomer: R1—(OCH2CH2)n-L-OC(O)—CR2?CH2??Formula (I) wherein R1 is hydrogen or a C1-C6 alkyl group, n is an integer from 1 to 100, L is a single bond or a divalent linking group, preferably a single bond or a C1-6 alkylene group, and R2 is hydrogen or a CH3 group; and optionally (d) at least one copolymerizable non-acrylate monomer; wherein the amount of the polymerizable monomer of formula (I) is between 2.5 and 40% by weight of the total of all polymerizable monomers (a), (b), (c) and (d). The invention also relates to a random copolymer obtained by reacting the polymerizable composition, a crosslinked product of the random copolymer and an adhesive composite material comprising the random copolymer or the crosslinked product on a substrate.Type: GrantFiled: November 26, 2014Date of Patent: April 3, 2018Assignee: ICAP-SIRA S.p.A.Inventors: Giorgio Zanzottera, Robert Henry Mayan
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Patent number: 9932500Abstract: According to one embodiment, an adhesive tape includes a film and an adhesive layer. The film includes polytetrafluoroethylene and a carbon filler. The adhesive layer is provided on a surface of the film, and includes a silicone pressure-sensitive adhesive.Type: GrantFiled: June 23, 2017Date of Patent: April 3, 2018Assignee: Chukoh Chemical Industries, Ltd.Inventors: Kentaro Tanaka, Masayuki Sueishi
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Patent number: 9932501Abstract: The present invention is related to an adhesive composition comprising a 50-95 wt % polymer blend and a tackifier. The blend has a first and second propylene-based polymer, both different homopolymers of propylene or a copolymer of propylene and ethylene or a C4 to C10 alpha-olefin. The blend has a melt viscosity, measured at 190° C., of 1,000 to 30,000 cP and a crystallization temperature of greater than 60° C. The tackifier has a softening point of 85° C. to 105° C., an aromaticity of 5 mol % to 15 mol % aromatic protons, and a Cloud Point of 45° C. to 75° C.Type: GrantFiled: December 16, 2015Date of Patent: April 3, 2018Assignee: ExxonMobil Chemical Patents Inc.Inventors: Ranjan Tripathy, Jean-Roch Schauder
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Patent number: 9932502Abstract: A hot melt adhesive composition is provided which contains at least one silane group-containing thermoplastic poly-?-olefin which is solid at 25° C. and at least one paraffin wax. The hot melt adhesive composition has only low adhesion to uncoated aluminum tool surfaces, wherein at the same time they have high final strengths and thermal stabilities comparable to conventional adhesives, as well as good resistance to environmental influences. The hot melt adhesive is suitable as a laminating adhesive for laminating films made of thermoplastic olefins, which have sufficient stability for subsequent deep-draw lamination.Type: GrantFiled: May 12, 2015Date of Patent: April 3, 2018Assignee: SIKA TECHNOLOGY AGInventors: Doreen Janke, Kai Paschkowski
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Patent number: 9932503Abstract: An adhesive composition comprising an aromatic epoxy resin, an epoxy resin rubber adduct, an amine curing agent; and optionally one or more of an oil absorbent, a corrosion inhibitor and a urone accelerator, wherein the adhesive composition is curable at 150° C. in no more than 210 seconds.Type: GrantFiled: June 30, 2015Date of Patent: April 3, 2018Assignee: Hexcel Composites LimitedInventors: Chris Harrington, Vaida Burton
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Patent number: 9932504Abstract: Provided is an aqueous emulsion composition which has excellent chemical stability (stability with respect to impurities) and excellent mechanical stability. Disclosed is an aqueous emulsion composition which contains: (A) a polymer that contains a fluoroalkyl group; and (B) a surfactant that contains (B1) an amidoamine surfactant having an amide group and an amino group, and (B2) a nonionic surfactant. It is preferable that the surfactant does not contain a monool having an unsaturated triple bond or an alkylene oxide addition product of a polyol.Type: GrantFiled: March 19, 2013Date of Patent: April 3, 2018Assignee: DAIKIN INDUSTRIES, LTD.Inventors: Rumi Kawabe, Ryousuke Hara, Masahiro Miyahara, Masaki Fukumori, Kouji Kubota, Kensuke Mohara, Takashi Enomoto
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Patent number: 9932505Abstract: An environmentally friendly hydrocarbon refrigerant mixture may be used as a substitute for existing refrigerant in a refrigerant system. The hydrocarbon refrigerant mixture offers greater operating efficiency and effectively replaces chlorofluorocarbon refrigerants. The refrigerant mixture for the refrigeration system includes from about 85% to about 89% by weight propane and from about 11% to about 15% by weight propene.Type: GrantFiled: October 27, 2016Date of Patent: April 3, 2018Assignee: GLANT, LLCInventors: Gary Michael Lindgren, Frank Galante
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Patent number: 9932506Abstract: An environmentally friendly hydrocarbon refrigerant mixture may be used as a substitute for existing refrigerant in a refrigerant system. The hydrocarbon refrigerant mixture offers greater operating efficiency and effectively replaces chlorofluorocarbon refrigerants. The refrigerant mixture for the refrigeration system includes from about 85% to about 89% by weight propane and from about 11% to about 15% by weight propene.Type: GrantFiled: October 27, 2016Date of Patent: April 3, 2018Assignee: GLANT, LLCInventors: Gary Michael Lindgren, Frank Galante
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Patent number: 9932507Abstract: The present invention relates to a composition comprising HFO-1234yf, or trans-HFO-1234ze, or a mixture thereof; HFC-32; and HFC-152a, HFO-1243zf, or a mixture thereof, wherein said composition is selected from the group consisting of: (I) a first composition, wherein said HFO-1234yf or trans-HFO-1234ze or a mixture thereof is at least 56 weight percent of said first composition; (II) a second composition, wherein said HFC-32 is at most 29 weight percent of said second composition; (III) a third composition, wherein said HFC-152a is at least 56 weight percent said third composition; (IV) a fourth composition, wherein said HFC-32 is at least 56 weight percent of said fourth composition; (V) a fifth composition comprising trans-HFO-1234ze, HFC-32, and HFC-152a, HFO-1243zf, or a mixture thereof; and (VI) a sixth composition, wherein said HFO-1243zf or mixture thereof with HFC-152a is at most 20 weight percent of said sixth composition.Type: GrantFiled: May 31, 2017Date of Patent: April 3, 2018Assignee: THE CHEMOURS COMPANY FC, LLCInventors: Barbara Haviland Minor, Joachim Gerstel
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Patent number: 9932508Abstract: A silicone composition that contains an organopolysiloxane having at least two aliphatic unsaturated hydrocarbon groups per molecule, a filler containing an aluminum powder and a zinc oxide powder, an organohydrogenpolysiloxane having two or more SiH groups per molecule, and a platinum group metal catalyst, in which when a storage and loss elastic modulus G? of the silicone composition is measured by means a viscoelasticity measurement apparatus capable of measuring shear modulus, the silicone composition can provide a cured product wherein G? after 3,000 seconds from the start of holding is 10,000 Pa or less, G? after 7,200 seconds from the start of holding is 100,000 Pa or less, and G? exceeds G? after 800 seconds or more from the start of holding. As a result, there is provided a silicone composition excellent in crushability, spreadability, and heat conductivity, and further provided a method for manufacturing a heat-conductive silicone composition.Type: GrantFiled: June 13, 2014Date of Patent: April 3, 2018Assignee: SHIN-ETSU CHEMICAL CO., LTD.Inventors: Keita Kitazawa, Kunihiro Yamada
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Patent number: 9932509Abstract: The present invention relates to the use of a double salt of Ca(NO3)2 and KNO3 for the manufacture of a melt, in particular a nitrate-based heat transfer fluid (HTF) and/or thermal energy storage fluid, for example in solar energy applications, such as in solar electrical power plant systems using a parabolic through, a central receiver or a linear Fresnel, which have both a low melting temperature and a high decomposition temperature, as well as to methods for the manufacture thereof. Using said double salt, a melt could be manufactured comprising at least NaNO3, KNO3 and Ca(NO3)2, preferably, an eutectic ternary melt comprising Ca(NO3)2, NaNO3 and KNO3 in a weight ratio of about 42:15:43 with an operating temperature of about 131° C. to about 560° C.Type: GrantFiled: September 17, 2013Date of Patent: April 3, 2018Assignee: YARA INTERNATIONAL ASAInventors: Torstein Obrestad, Amund Myrstad, Tore Frogner
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Patent number: 9932510Abstract: A treatment fluid comprising: a base fluid; a plurality of a first type of fiber, wherein the first type of fiber is degradable; a plurality of a second type of fiber; and a third lost-circulation material, wherein the first type of fibers, the second type of fibers, and the third lost-circulation material inhibit or prevent some or all of the treatment fluid from penetrating into a subterranean formation from a wellbore, wherein the wellbore penetrates the subterranean formation.Type: GrantFiled: June 10, 2014Date of Patent: April 3, 2018Assignee: Halliburton Energy Services, Inc.Inventors: Jonathan P. Walker, Donald L. Whitfill, Sharath Savari
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Patent number: 9932511Abstract: Compositions useful as wellbore fluids are generally disclosed. In some embodiments, the compositions include polymerizable olefinic surfactant compositions, which, under certain conditions, can polymerize via free-radical polymerization to form surfactant polymers. In some embodiments, the compositions are introduced to an oil well as part of the drilling or extraction process, e.g., to assist in flushing hydrocarbon material out of subterranean formations.Type: GrantFiled: July 13, 2015Date of Patent: April 3, 2018Assignee: Elevance Renewable Sciences, Inc.Inventors: Ryan Littich, Charles Coburn
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Patent number: 9932512Abstract: The present application provides a composition containing a maleic anhydride copolymer, a polyaziridine crosslinker, optionally an additional crosslinking agent such as an amine crosslinker, and optionally a gel time control agent. Methods of using the composition to treat a subterranean formation are also provided.Type: GrantFiled: August 22, 2017Date of Patent: April 3, 2018Assignee: Saudi Arabian Oil CompanyInventors: Matthew Gary Hilfiger, B. Raghava Reddy
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Patent number: 9932513Abstract: Treatment fluids employing stabilized heteropolysaccharide-based gels in brines are used as part of gravel packing and combined gravel packing-fracturing operations; a method includes providing a treatment fluid which includes an aqueous brine base, a heteropolysaccharide including one selected from the group consisting of diutan, scleroglucan, and succinoglycan, and a protein present in an amount sufficient to stabilize the heteropolysaccharide and hence minimizing the salting out phenomenon, the method including placing the treatment fluid in a subterranean formation.Type: GrantFiled: January 23, 2013Date of Patent: April 3, 2018Assignee: Haliburton Energy Services, Inc.Inventors: Prerana Umesh Suryawanshi, Lalit Pandurang Salgaonkar, Achala Vasudev Danait
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Patent number: 9932514Abstract: An aqueous slurry composition for use in industries such as petroleum and pipeline industries, such as for use as a fracturing fluid. The aqueous slurry composition includes a particulate, an aqueous liquid and a chemical compound that renders the particulate surface hydrophobic. The slurry is produced by rendering the surface of the particulate hydrophobic during or prior to making the slurry.Type: GrantFiled: April 24, 2015Date of Patent: April 3, 2018Inventors: Kewei Zhang, Shang Ying Liu, Chuanzhong Wang, Weibing Lu
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Patent number: 9932515Abstract: A fracturing fluid comprising: a base fluid, wherein the base fluid comprises water; proppant; and an additive, wherein the additive: (i) is a cross-linkable polymer, wherein the polymer is a polysaccharide comprising a backbone and pendant functional groups, wherein the polysaccharide is derivatized by substituting one or more of the pendant functional groups with furan; (ii) is a viscosifying agent; and (iii) is a curable resin for consolidating the proppant. A method of fracturing a subterranean formation comprising: introducing the fracturing fluid into the subterranean formation; and creating or enhancing one or more fractures in the subterranean formation.Type: GrantFiled: April 2, 2014Date of Patent: April 3, 2018Assignee: Halliburton Energy Services, Inc.Inventors: Dipti Singh, Jeremy Holtsclaw, Aaron G. Russell
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Patent number: 9932516Abstract: In a slick-water fracturing operation, a composition is used to prevent the interaction between a polymer in a water-based fracturing fluid and naturally-occurring metal ions. The composition includes a metal-complexing agent, such as a chelating agent. The chelating agent can also be biodegradable and is citric acid in embodiments. The metal-complexing agent can be coated with one or two coatings to create a time-released form. The time-released form prevents loss of the agent prior to delivery at the shale.Type: GrantFiled: September 4, 2015Date of Patent: April 3, 2018Assignee: Flex-Chem Holding Company, LLCInventor: Andrew Bryce Conway
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Patent number: 9932517Abstract: The present invention relates to the field of oil-field chemical reagents, and discloses a polymer, a preparation method of the polymer, and a viscosified acid fluid. The polymer contains structural units represented by formula (1), structural units represented by formula (2), and structural units represented by formula (3), wherein, R1-R6 and R11-R13 are H or C1-C4 linear or branched alkyl respectively and independently, R7 is C1-C4 linear or branched alkylene, R8-R10 are C1-C5 linear or branched alkyl respectively and independently, R14 is C1-C4 linear or branched alkyl, and n=0-4.Type: GrantFiled: August 8, 2017Date of Patent: April 3, 2018Assignees: China University of Petroleum (East China), Research Institute of Petroleum Exploration & DevelopmentInventors: Caili Dai, Mingwei Zhao, He Liu, Yining Wu, YOngpeng Sun, Guang Zhao, Zhongliang Xu
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Patent number: 9932518Abstract: A method for increasing the permeability of a geologic formation by fracturing includes the step of pumping a solution of a borohydride into a well bore. The solution may also include a basic material such as sodium hydroxide. This step may be followed by pumping a second acidic solution into the well bore.Type: GrantFiled: May 13, 2014Date of Patent: April 3, 2018Assignee: Montgomery Chemicals LLCInventor: James George Clements
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Patent number: 9932519Abstract: A method for forming particles having a ridge portion includes inducing flow of a slurry of particles and a reactant through one or more orifices, detaching an amount of the slurry from the slurry flow following exit from the one or more orifices, the detached amount forming a slurry body, forming the slurry body into a particle shape, contacting the particle shaped slurry body with a coagulation solution to form a stabilized particle having the ridge portion, and drying and/or sintering the particle having the ridge portion.Type: GrantFiled: November 19, 2015Date of Patent: April 3, 2018Assignee: Schlumberger Technology CorporationInventors: Jiangshui Huang, Jose Alberto Ortega Andrade, Bernhard Rudolf Lungwitz
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Patent number: 9932520Abstract: Composition and methods using the compositions are disclosed, where the compositions include heterocyclic aromatic amines, substituted heterocyclic aromatic amines, poly vinyl heterocyclic aromatic amines, co-polymers of vinyl heterocyclic aromatic amine and non amine polymerizable monomers (ethylenically unsaturated mononers and diene monomers), or mixtures or combinations thereof reacted with sulfonic acids, alkyl sulfonic acids, sulfosuccinates, sulfamic acids, sulfuric acids or partially neutralized amine or other alkali sulfonate and/or reacted with alpha hydroxyl carboxcylic acids which form coatings that alter self-aggregating properties and/or aggregation propensities of the particles and surfaces. Furthermore, the coating can be used to improve filtration of fluids through particulate matter and it is found that the coating will increase hydrocarbon liquid and gas flow through or over treated particulates and surfaces.Type: GrantFiled: May 24, 2016Date of Patent: April 3, 2018Assignee: Sumisaujana TCM Chemicals Sdn. Bhd.Inventors: Raynard Veldman, Arthur Thomas Gilmer, Mohammad Zaki Hasra Shafie, Norazlam Norbi
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Patent number: 9932521Abstract: A self-suspending proppant comprises a proppant particle substrate carrying a coating of an anionic hydrogel-forming polymer. The detrimental effect of calcium and other divalent ions on the ability of the proppant to swell when contacted with water is reduced by including a calcium binding agent in the proppant.Type: GrantFiled: February 26, 2015Date of Patent: April 3, 2018Assignee: SELF-SUSPENDING PROPPANT, LLCInventors: David S. Soane, Robert P. Mahoney, Marie K. Herring, Kevin P. Kincaid, Rosa Casado Portilla
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Patent number: 9932522Abstract: To provide an electrochromic compound, represented by the following general formula (I), where Ar1 is a pyridinium ring having a structure represented by the following general formula (IIa), (IIb), or (IIc), where Ar2 is a monovalent heterocyclic ring which may have a substituent, but Ar2 is not a pyridinium ring; R1 to R8 are each independently a monovalent group which may have a functional group, where the monovalent group may have a substituent; A is a monovalent group which may have a functional group, where the monovalent group may have a substituent; and B? is a monovalent anion.Type: GrantFiled: June 17, 2015Date of Patent: April 3, 2018Assignee: Ricoh Company, Ltd.Inventors: Daisuke Goto, Toshiya Sagisaka, Shigenobu Hirano, Satoshi Yamamoto, Mamiko Inoue, Tohru Yashiro, Hiroyuki Takahashi, Koh Fujimura, Tamotsu Horiuchi, Keiichiroh Yutani, Yoshihisa Naijo, Yoshinori Okada, Kazuaki Tsuji, Sukchan Kim, Keigo Takauji
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Patent number: 9932524Abstract: The present invention is directed to processing feedstock materials for recovery, recycling and/or reuse of the constituent components of the feedstock materials, and includes adding feedstock materials at a constant temperature to a thermal reactor, heating the feedstock materials at a temperature of 1,100° F. or higher in an anaerobic environment within the thermal reactor to produce cracked and gasified hydrocarbons and residual material, removing cracked and gasified hydrocarbons released from the feedstock materials from the thermal reactor, further processing the residual material to recover one or more constituent component of the feedstock materials, and oxidizing the cracked and gasified hydrocarbons removed from the thermal reactor having five or less carbon atoms in their molecular structure in order to produce heat to obtain the temperature of 1,100° F. or higher for the thermal reactor.Type: GrantFiled: February 2, 2015Date of Patent: April 3, 2018Assignee: MODERN RECOVERY SYSTEMS, INC.Inventors: Douglas D. Griffin, II, Joachim P. Roesler
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Patent number: 9932525Abstract: The present invention provides new techniques related to magnetically controllable and/or steerable froth for use in separation processes of mineral-bearing ore and bitumen. Apparatus is provided featuring a processor configured to contain a fluidic medium having a material-of-interest and also having a surfactant with magnetic properties so as to cause the formation of a froth layer that contains at least some of the material-of-interest and is magnetically responsive; and a magnetic field generator configured to generate a magnetic field and provide non-mechanical mixing and steering/driving of the froth layer in the processor. The material-of-interest may be mineral-bearing ore particles or bitumen. The processor includes a flotation tank, a primary separation vessel (PSV), or a pipe, including a tailings pipeline.Type: GrantFiled: February 28, 2013Date of Patent: April 3, 2018Assignee: CiDRA CORPORATE SERVICES, INC.Inventor: Alan D. Kersey
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Patent number: 9932526Abstract: The present invention relates to methods of treating heavy crude oil on the surface or in situ. The methods of the present invention include: (a) mixing the heavy crude oil with a solvent; (b) subjecting the mixture to ultrasonic vibrations; and (c) subjecting mixture treated with ultrasonic vibrations to microwave energy.Type: GrantFiled: August 7, 2014Date of Patent: April 3, 2018Inventor: Bruce Rout
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Patent number: 9932527Abstract: The invention is directed to a process that combines the solvent deasphalting with resin hydrotreatment so as to reduce the costs associated with performing each of the steps separately. The integrated process of the invention permits higher product yields coupled with lower energy and transportation costs.Type: GrantFiled: July 29, 2012Date of Patent: April 3, 2018Assignee: AMEC Foster Wheeler USA CorporationInventors: Daniel B. Gillis, Robert Clarke, Joseph Woodson
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Patent number: 9932528Abstract: A system for desalting a crude oil stream includes vessel that has an interior piping structure that releases wash water into a crude oil flow within the vessel. The piping structure, which may have more than one level, has a plurality of spray nozzles for dispersing or releasing the wash water into the flowing crude oil stream. The spray nozzles may be located on a same side or opposite sides of the piping structure. Where multiple levels are used, the number of spray nozzles on each level may be the same as or different than the number of spray nozzles on other levels. The pressure drop through each spray nozzle is no greater than 300 psi and the nozzles deliver a dilution water droplet no larger than 300 microns in diameter. A mixing valve, static mixer, or both can be placed downstream of the vessel.Type: GrantFiled: November 28, 2016Date of Patent: April 3, 2018Assignee: Cameron Solutions, Inc.Inventors: Gary W. Sams, Joseph Min-Hsiun Lee
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Patent number: 9932529Abstract: The invention discloses a rubber process oil and a process for manufacturing rubber process oils which are non-carcinogenic in nature. The process comprises of selectively producing Hildebrand solubility components enriched vacuum residue by selective distillation of reduced crude oil (RCO) to obtain minimum of 10 vol % boiling components in the range 490° C. to 50° C., which leads to higher solubility of rubber process oil with an aniline point of less than 70° C. and with extremely low concentration of selective polycyclic aromatics which makes the 15 product non-carcinogenic.Type: GrantFiled: February 2, 2013Date of Patent: April 3, 2018Assignee: INDIAN OIL CORPORATION LTD.Inventors: Naduhatty Selai Raman, Palvannan Mohanasundaram, Pattathilchira Varghese Joseph, Pankaj Bhatnagar, Deepak Saxena, Anil Yadav, Vivekanand Kagdiyal, Brijesh Kumar, Rajan Thomas Mookken, Santanam Rajagopal, Ravinder Kumar Malhotra
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Patent number: 9932530Abstract: A method for refining used motor oil using two or more hydrotreating reactors arranged in series. The used motor oil may be vacuum distilled to produce an unrefined gasoil. The unrefined gasoil may then be hydrotreated in a first hydrotreating reactor with hydrogen operated at a temperature ranging from approximately 245° C. to approximately 260° C. to produce a hydrotreated gasoil. The hydrogen may comprise a mixture of fresh hydrogen and recycled hydrogen recovered from the last of the two or more hydrotreating reactors. The hydrotreated gasoil may then be hydrotreated in one or more additional hydrotreating reactors operated at temperatures ranging from approximately 260° C. to approximately 330° C. to produce a refined gasoil. The first hydrotreating reactor may remove a substantial portion of metallic impurities from the unrefined impurities, while the one or more additional hydrotreating reactors remove a substantial portion of heteroatom impurities from the unrefined gasoil.Type: GrantFiled: June 17, 2014Date of Patent: April 3, 2018Assignee: Air Products and Chemicals, Inc.Inventors: Diwakar Garg, Timothy D. Lebrecht
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Patent number: 9932531Abstract: Systems, processes, and catalysts are disclosed for obtaining fuel and fuel blends containing selected ratios of open-chain and closed-chain fuel-range hydrocarbons suitable for production of alternate fuels including gasolines, jet fuels, and diesel fuels. Fuel-range hydrocarbons may be derived from ethylene-containing feedstocks and ethanol-containing feedstocks.Type: GrantFiled: April 24, 2017Date of Patent: April 3, 2018Assignee: Battelle Memorial InstituteInventors: Michael A. Lilga, Richard T. Hallen, Karl O. Albrecht, Alan R. Cooper, John G. Frye, Karthikeyan Kallupalayam Ramasamy