Abstract: Disclosed are Niobium Nitride film forming compositions, methods of synthesizing the same, and methods of forming Niobium Nitride films on one or more substrates via vapor deposition processes using the Niobium Nitride film forming precursors.

Abstract: Disclosed is a method for phosphorus absorption by hydration and fluorine recovery for a fume exiting a kiln in a kiln process for the production of phosphoric acid, comprising the following steps: a fume containing P2O5 and fluorine exiting a kiln is introduced into a hydration tower, the fume performs heat and mass transfer with the spraying liquid, with most of the phosphoric acid produced being absorbed into the spraying liquid; the phosphoric acid solution falling from the spraying finally enters the acid solution circulating and spraying system; the fume discharged from a fume outlet then passes through a phosphoric acid mist capturing tower and a mist removing and separating tower successively, such that the phosphoric acid mist entrained in the fume exiting the hydration tower is further captured.

Abstract: A method for concentration of phosphate compounds comprises dissolving (205) of sludge ash in hydrochloric acid. Insoluble residues are separated (210), thereby forming a first leach solution. A mole ratio of phosphorus to a sum of ferric iron and aluminum in the first leach solution is controlled (215) to be larger than 1. A base is added (220) to the first leach solution in an amount causing precipitation of phosphate compounds. The precipitated phosphate compounds are removed (225) from the first leach solution. Sulphuric acid is added (240) to the first leach solution, causing precipitation of sulphate compounds. The precipitated sulphate compounds are separated (245) from the first leach solution. At least a part of the leach solution is recycled (248) as the hydrochloric acid used for the dissolving of sludge ash. Further methods for processing the precipitated phosphate compounds are presented as well as arrangements for performing the methods.

Abstract: A mixed-metallic phosphate compound is disclosed, which contains as the main metal copper in the divalent oxidation state in a proportion of at least 90.0 at-% and one or more doping metals in a total proportion of the doping metals of at least 0.01 to at most 10.0 at-%, wherein the doping metals are selected from the group consisting of the elements of the first and second main groups and the eighth subgroup of the elements of the periodic table, Al, Sn, Si, Bi, Cr, Mo, Mn, and the lanthanides. The stated metal proportions relate to the total amount of the metals in the mixed-metallic phosphate compound. The mixed-metallic compound has a phosphate content expressed as P2O5 in the range of 10 to 60 wt-%. Also disclosed is a method for producing the mixed-metallic phosphate compound and the use thereof.

Abstract: A composition and a method for producing mesoporous carbon materials with a chiral or achiral organization. In the method, a polymerizable inorganic monomer is reacted in the presence of nanocrystalline cellulose to give a material of inorganic solid with cellulose nanocrystallites organized in a chiral nematic organization. The cellulose can be carbonized through thermal treatment under inert atmosphere (e.g., nitrogen or argon) and the silica may subsequently be removed using aqueous solutions of sodium hydroxide (NaOH) or hydrogen fluoride (HF) to give the stable mesoporous carbon materials that retain the chiral nematic structure of the cellulose. These materials may be obtained as free-standing films with very high surface area. Through control of the reaction conditions the pore-size distribution may be varied from predominantly microporous to predominantly mesoporous materials.

Abstract: A method for manufacturing a nanocarbon material includes the steps of: a) supplying an acetylene-based flammable gas into a torch nozzle at a flow rate such that an ignition at the torch nozzle produces a reducing flame in a cooling zone in a chamber; and b) supplying a cooling medium to a nebulizer disposed upstream of the cooling zone to produce nebulized droplets of the cooling medium such that the nebulized droplets come into contact with the reducing flame in the cooling zone to thereby cause carbon nanoparticles to be entrained in the nebulized droplets.

Abstract: Systems and methods for synthesizing continuous graphene sheets are provided. The systems and methods include passing a catalyst substrate through a heated chemical vapor deposition chamber and exposing the substrate to a reaction gas mixture of hydrogen and hydrocarbon at a preselected location within the chamber. The reaction gas mixture can include hydrogen having a partial pressure of between about 0 Torr and 20 Torr, hydrocarbon having a partial pressure of between about 20 mTorr and about 10 Torr, and one or more buffer gases. The buffer gases can include argon or other noble gases to maintain atmospheric pressure within the chemical deposition chamber. The resulting graphene can be made with continuous mono and multilayers (up to six layers) and have single crystalline hexagonal grains with a preselected nucleation density and domain size for a range of applications.

Abstract: Disclosed is a method of producing graphene, which includes bringing a metal catalyst into contact with hydrogen gas (Step a), bringing the metal catalyst in Step a into contact with at least one selected from among a hydrocarbon gas, nitrogen gas, and an inert gas (Step b), and forming graphene on the metal catalyst by bringing the metal catalyst in Step b into contact with hydrogen gas and a hydrocarbon gas (Step c), whereby the number of layers of graphene can be variously controlled as needed, regardless of the initial surface roughness of a metal catalyst layer, and also, the time required to form graphene can be shortened, thus reducing processing costs.

Abstract: A controlled preparation of octachlorotrisilane and higher polychlorosilane such as DCTS and DCPS from monomeric chlorosilane, proceeds by exposing the chlorosilane to a nonthermal plasma and recycling chlorosilane that has not been converted to octachlorotrisilane into the plasma.

Abstract: Precipitated silica specifically useful in the paper industry and in particular in paper-coating applications for inject printing, is characterized by an uptake of DOP oil lower than 260 ml/100 g, a pore volume (Vd25) of greater than 0.8 ml/g formed by pores having a diameter of less than 25 nm, a CTAB specific surface area of greater than 280 m2/g.

Abstract: The invention pertains to methods of producing aluminum trioxide in the form of powders or agglomerations with particles having a porous honeycomb structure, which can be used as catalyst substrates, adsorbents and filters for the chemical, food, and pharmaceutical industry. The method of production of aluminum oxide in the form of powders or agglomerations with particles having a porous honeycomb structure involves the treatment of the aluminum salt with a solution of an alkaline reagent, washing of the sediment and thermal treatment thereof. The technical result of the invention is the production of aluminum oxide in the form of separate particles with given structure and properties, specifically, with particle porosity of 60-80% and a porous structure represented by extensive parallel channels with near hexagonal packing, with dimension of the channels at the diameter of 0.3 to 1.0 micron and length up to 50 microns.

Abstract: A wastewater sewage system is disclosed. The sewage system includes a flow control valve that controls the flow of wastewater through the sewage system such that the sewage pipes in the sewage system are substantially full.

Abstract: Provided are methods of petroleum sequestration, which use electrospun microtubes capable of sequestering the petroleum from the water, and method of depleting and optionally degrading petroleum from water using floating devices which comprise the electrospun microtube attached to a floating carrier.

Abstract: A water-processing filter having a high dimensional accuracy and an improved filterability (such as a capability to remove turbidity components) is provided. The water-processing filter comprises (A) a hollow cylindrical filter which comprises (a1) a granular activated carbon having a median particle size of 30 to 80 ?m and (a2) a fibrillated fibrous binder. The cylindrical filter (A) has an upstream outer surface having an arithmetical mean deviation of a waviness profile adjusted to not more than 30 ?m and an arithmetical mean deviation of a primary profile adjusted to 35 to 45 ?m. The cylindrical filter (A) may have a downstream inner surface having an arithmetical mean deviation of a waviness profile of not more than 30 ?m and an arithmetical mean deviation of a primary profile of 35 to 45 ?m. The cylindrical filter (A) may have a grounded outer surface.

Abstract: A water filter cartridge is reduced in fluctuation in filtration flow rate or in filtration performance due to activated carbon, and can exhibit stable performance even at the time of large scale production; and a water purifier is equipped with the water filter cartridge. A water filter cartridge having particulate activated carbon filled in a case for accommodating a filtering material in which the ratio of the total mass of particulate activated carbon having a particle size of 0.3 to 4.0 mm relative to the total mass of activated carbon is 97% by mass or more, and, in a particle size distribution which represents the relationship of the mass ratio of activated carbon relative to the particle size of activated carbon, a peak at which the mass ratio is 31% by mass or more does not appear in a particle size range of from 0.3 to 4.0 mm.

Abstract: A treatment solution supply method of supplying a treatment solution to a substrate, the method includes the steps of: applying a DC voltage to the treatment solution; detecting a potential difference between two points in the treatment solution in a state where the DC voltage is applied to the treatment solution; and increasing the DC voltage when the detected potential difference is less than a predetermined reference value.

Abstract: A system and method for treating flowing water systems with a plasma discharge to remove or control growth of microbiological species. Components of the water system are protected from being damaged by excess energy from the electrohydraulic treatment. Ozone gas generated by a high voltage generator that powers the plasma discharge is recycled to further treat the water. A gas infusion system may be used to create fine bubbles of ozone, air, or other gases in the water being treated to aid in plasma generation, particularly when the conductivity of the water is high. An electrode mounting assembly maintains a high voltage electrode and ground electrode at a fixed distance from each other to optimize plasma generation. An open support structure for the high voltage generator circuit physically separates spark gap electrodes and resists metal deposits that may disrupt discharge of a high voltage pulse to create the plasma.

Abstract: The present disclosure relates to a spacer structure that is configured to be disposed between a pair of electrodes in a capacitive deionization apparatus so as to provide a space for flowing a fluid therethrough. The spacer structure includes a copolymer prepared by copolymerizing a mixture of a polyurethane backbone including a carboxyl group or a sulfonic acid group, an ion conductive monomer including a carboxyl group and a cation exchange group, and a second polymer including a functional group that reacts with the carboxyl group or sulfonic acid group and forms a cross-linking bond with the polyurethane backbone.

Abstract: A method for fabricating a porous carbon material possessing a hierarchical porosity, the method comprising subjecting a precursor composition to a curing step followed by a carbonization step, the precursor composition comprising: (i) a templating component comprised of a block copolymer, (ii) a phenolic component, (iii) a dione component in which carbonyl groups are adjacent, and (iv) an acidic component, wherein said carbonization step comprises heating the precursor composition at a carbonizing temperature for sufficient time to convert the precursor composition to a carbon material possessing a hierarchical porosity comprised of mesopores and macropores. Also described are the resulting hierarchical porous carbon material, a capacitive deionization device in which the porous carbon material is incorporated, as well as methods for desalinating water by use of said capacitive deionization device.

Abstract: Methods and systems for preventing biofouling of membranes utilized in water treatment processes (i.e., water treatment membranes) are described. Methods include X-ray excitation of luminescent materials capable of emitting in the violet to UV range (e.g., from about 180 nm to about 440 nm). X-rays are directed at water treatment modules to contact the luminescent materials within the modules and excite internal violet/UV to prevent biofouling of membranes. The methods can be utilized in conjunction with existing processing equipment and can prevent biofouling of water treatment membranes in high volume treatment processes in an environmentally friendly fashion.

Abstract: A method and system for injecting a pulsed radio frequency signal into a fluid-containing system in order to create and propagate an electromagnetic field throughout the fluid-containing system. The electromagnetic field may be used to prevent the formation and build-up of scale in the fluid-containing system and/or to prevent the proliferation of bacteria within the fluid-containing system. The method and system may also be used to inject a pulsed radio frequency signal at a number of points in a fluid-containing system, or to inject a pulsed radio frequency signal to a number of independent fluid-containing systems.

Abstract: The invention provides a liquid composition when used for maintenance of a body of water, the liquid composition comprising a solution of magnesium and potassium salts, at least one of which is a halide salt. Preferably, the liquid composition comprises Mg2+ from the magnesium salt in an amount of from about 6000 ppm to about 15 000 ppm; K+ from the potassium salt in an amount from about 40 000 ppm to about 120 000 ppm and hypohalite from the halide in an amount from about 100 000 ppm to about 400 000 ppm.

Abstract: Methods for the use of peracid compositions having decreased hydrogen peroxide concentration and a UV-blocking agent for various water treatments, including oil- and gas-field operations, and/or other aseptic treatments are disclosed. In numerous aspects, peracetic acid is the preferred peracid and is treated with a peroxide-reducing agent to substantially reduce the hydrogen peroxide content. Methods for using the treated peracid compositions for treatment of drilling fluids, frac fluids, flow back waters and disposal waters are also disclosed for improving water condition, reducing oxidizing damage associated with hydrogen peroxide and/or reducing bacteria infestation.

Abstract: The invention provides a system for treatment of wastewater. A pumping system pumps wastewater from a source basin to a recipient basin, while a conduit allows gravitational flow of water from a source basin to a recipient basin when the pumping system is inactive. A controller activates the pumping system to pump wastewater from the source basin to a recipient basin when a wastewater level in the source basin is at a first predetermined height or when a rate of gravitational flow wastewater from the source basin to the recipient basin is below a first predetermined flow rate. The controller also turns off the pumping system when the water level in the source basin is at a source basin minimal level and the water level in the recipient basin is at a recipient basin maximal level. The invention also provides a method for operating a wastewater treatment of the invention, and a pumping system for use in the system of the invention.

Abstract: A ballasted sequencing batch reactor system for treating wastewater including one or more sequencing batch reactors. A weighting agent impregnation subsystem is configured to mix biological flocs and weighting agent to form weighted biological flocs. A weighting agent recovery subsystem is configured to recover weighting agent from the weighted biological flocs and reintroduce the recovered weighting agent to the weighting agent impregnation subsystem.

Abstract: A method or process for treating wastewater containing high organics, silica, boron, hardness, and suspended and dissolved solids. The method includes degasifying the wastewater for the removal of dissolved gases and thereafter chemically softening the wastewater. After the chemical softening step, the wastewater is directed through a media filter or membrane which removes additional solids and precipitants. Thereafter the wastewater is directed through a sodium ion exchange that further softens the wastewater. The effluent from the ion exchange is directed through a cartridge filter and the effluent from the cartridge filter is directed through one or more reverse osmosis units. At a selected phase of the process, prior to the wastewater reaching the reverse osmosis unit or units, the pH of the wastewater is raised and maintained such that the pH of the wastewater reaching a reverse osmosis unit is at a pH greater than 10.5.

Abstract: The synthetic amorphous silica powder of the present invention is characterized in that it comprises a synthetic amorphous silica powder obtained by applying a spheroidizing treatment to a silica powder, and by subsequently cleaning and drying it so that the synthetic amorphous silica powder has an average particle diameter D50 of 10 to 2,000 ?m; wherein the synthetic amorphous silica powder has: a quotient of 1.00 to 1.35 obtained by dividing a BET specific surface area of the powder by a theoretical specific surface area calculated from the average particle diameter D50; a real density of 2.10 to 2.20 g/cm3; an intra-particulate porosity of 0 to 0.05; a circularity of 0.75 to 1.00; and an unmolten ratio of 0.00 to 0.25.

Abstract: A method for producing, without a mold, a shaped glass article having a predefined geometry is provided. The method includes providing a starting glass, supporting the starting glass, heating a portion of the starting glass so that in the portion a predetermined spatial viscosity distribution of the starting glass is obtained from 109 to 104 dPa·s and so that at points where the starting glass is supported a predetermined spatial viscosity distribution of the starting glass does not fall below 1013 dPa·s, and deforming the heated starting glass by action of an external force until the predefined geometry of the glass article is obtained.

Abstract: A method of manufacturing an optical fiber of the invention includes: preparing a direction changer; drawing the bare optical fiber from an optical fiber preform; providing a coated layer on a periphery of the bare optical fiber; obtaining an optical fiber by curing the coated layer; changing a direction of the bare optical fiber at a position between a bare-optical-fiber formation position and a coated-layer provision position; and measuring the outer diameter of the coated layer; and adjusting the length of the bare optical fiber from a drawing unit to a coating unit by controlling a position of the direction changer based on a measurement value of the outer diameter, the drawing unit forming the bare optical fiber, the coating unit providing the coated layer on the periphery of the bare optical fiber.

Abstract: An inorganic fiber containing silica and magnesia as the major fiber components which further includes intended synergistic amounts of calcia and, an additional alkali metal oxide other than magnesia, such as lithium oxide, to improve the thermal performance and manufacturability of the fiber. The inorganic fiber is easier to manufacture, has a better fiber quality, exhibits good thermal performance at a use temperature of 1260° C. and greater, retains mechanical integrity after exposure to the use temperature, and exhibits low biopersistence in physiological fluids. Also provided are methods of preparing the inorganic fiber and of thermally insulating articles using thermal insulation prepared from the inorganic fibers.

Abstract: Embodiments are directed to glass frits containing phosphors that can be used in LED lighting devices and for methods associated therewith for making the phosphor containing glass frit and their use in glass articles, for example, LED devices.

Abstract: A colored lacquered substrate made of glass or glass-ceramic includes a mineral coating based on alkaline silicate, which achieves the required performance in terms of color and of change in color during tempering, and in terms of adhesion and of mechanical strength at low temperatures without requiring a high-temperature baking step.

Abstract: A coated article is provided, having a coating supported by a glass substrate where the coating includes at least one color and/or reflectivity-adjusting absorber layer. The absorber layer(s) allows color tuning, and reduces the glass side reflection of the coated article and/or allows sheet resistance of the coating to be reduced without degrading glass side reflection. In certain example embodiments the absorber layer is provided between first and second dielectric layers which may be of substantially the same material and/or composition. In certain example embodiments, the coated article is capable of achieving desirable transmission, together with desired color, low reflectivity, and low selectivity, when having only one infrared (IR) reflecting layer of silver and/or gold. Coated articles according to certain example embodiments of this invention may be used in the context of insulating glass (IG) window units, monolithic windows, or the like.

Abstract: The glass containers described herein have at least two performance attributes selected from resistance to delamination, improved strength, and increased damage resistance. In one embodiment, a glass container may include a body having an inner surface, an outer surface and a wall thickness extending between the outer surface and the inner surface. A compressively stressed layer may extend from the outer surface of the body into the wall thickness. The compressively stressed layer may have a surface compressive stress greater than or equal to 150 MPa. A lubricous coating may be positioned around at least a portion of the outer surface of the body. The outer surface of the body with the lubricous coating may have a coefficient of friction less than or equal to 0.7.

Abstract: The present disclosure relates to no fiber calcined gypsum and methods of making the same using a multi-stage (typically two-stage) calcination process. The first stage is a high temperature calcination and nucleation stage. The second stage is a lower temperature calcination and crystal growth stage which produces product slurry containing calcined gypsum particles having large, acicular calcined gypsum crystal morphology for use in making gypsum fiberboard.

Abstract: The present invention relates to a novel multifunctional material for workability of geopolymeric system and its process thereof. The viscous characteristics in geopolymeric system are responsible for observed negligible workability of geopolymeric cement concrete system and which limits its broad application spectrum. The novel multifunctional material of the present invention prepared by digestion of siliceous agricultural waste i.e. Rice husk with aqueous alkaline materials involving simultaneous and synergistic chemical reactions among the various constituents of rice husk, aqueous alkaline compounds and optionally adding Cetyl trimethyl ammonium bromide (CTAB) to obtain in-situ synthesis of desired nano-sized multi functional agents lignin, hemicelluloses, cellulose, sodium silicate necessary for addressing the issue of workability and also improving the engineering properties of geopolymeric system for broad application spectrum.

Abstract: Compositions and methods for terminating water flow in a subterranean formation are described. The compositions include a calcium aluminate cement, a Portland cement, a non-aqueous carrier fluid, and a polyphosphate. The cement compositions, upon making contact with water, form a viscous gel that sets into a hardened mass with extraordinary compressive strengths in a short period of time.

Abstract: A hard material which, when used as a material of a sintered material, makes it possible to obtain a sintered material with excellent abrasion resistance, a sintered material, a cutting tool including the sintered material, a method for manufacturing the hard material and a method for manufacturing the sintered material are provided. The hard material contains aluminum, nitrogen, and at least one element selected from the group consisting of titanium, chromium, and silicon, and has a cubic rock salt structure.

Abstract: The subject matter disclosed herein relates generally to light-curable ceramic slurries, and more specifically, to hybrid binders for light-curable ceramic slurries. A light-curable ceramic slurry includes a hybrid binder having an organic resin component and a multi-functional reactive siloxane component that is miscible with the organic resin component. The slurry also includes a photoinitiator having a corresponding photoactivation wavelength range and ceramic particles. The slurry is cured via exposure to light in the photoactivation wavelength range of the photoinitiator such that both the organic resin component and the multi-functional reactive siloxane component of the hybrid binder polymerize.

Abstract: A fertilizer derived from an organic source and a method of making are provided. The fertilizer of the present invention advantageously has a Nitrogen content greater than 4%. The method of making the fertilizer also produces potable water.

Abstract: The disclosed invention relates to soil and water treatment compounds, specifically to an acidifying composition used to treat soil or irrigation water used for growing plants. Disclosed is an acidifying composition that includes an organic acid. The acidifying composition is used to control and manage conditions in irrigation water and soil to prevent sodic deterioration of soil structure. Treatment of soil and/or irrigation water with the disclosed acidifying composition leads to improved soil quality and improved quality of plants grown in the soil treated with the acidifying composition.

Abstract: Treated biochar and methods for treating biochar are provided. The method for treating the biochar includes forcing, assisting or accelerating the movement of an infiltrant into the pores of the biochar, whereby the treatment affects properties of the biochar that provide for a more reliable and predictable biochar for use in various applications, including, but not limited to, agricultural applications.

Abstract: This disclosure provides a composting system and method. The system comprises: (a) a container configured to contain a composition and comprising (i) insulated walls, (ii) an air intake and (iii) a vent; and (b) a composition contained in the container. The composition comprises aerobic microorganisms, a carbon source and a nutrient source sufficient to support growth of the aerobic microorganisms. The container is sufficiently insulated so that heat generated by aerobic respiration is sufficiently retained in the container to maintain a heat gradient in the container. The container is dimensioned to generate a stack effect that moves air into the air intake, through the composition and out the vent. The moving air provides oxygen to support growth of aerobic microorganisms, making the stack effect self-sustaining as long as a carbon source and nutrients last. The insulation can maintain temperatures in the composting cell sufficient to kill pathogenic microorganisms.

Abstract: A method of producing a propellant material element, such as an electrically-operated propellant material, includes extruding a propellant material through a heated nozzle. The nozzle may be heated to a temperature that is above the boiling point of a solvent that is part of the propellant material, yet is below a decomposition temperature of the propellant material. This allows some of the solvent to be driven off during the extruding process, while still preventing initiation of an energy-creating reaction within the material. The heating of the material in the extruding process, and especially the heating of the nozzle that the material is extruded through, may be controlled to remove an amount of solvent that results in the extruded material having desirable properties.

Abstract: Fuel cell arrangement having an improved efficiency. The arrangement comprises one or more fuel cell units 110 and a methanation unit 200 and a control unit 300. The fuel cell unit comprises a water inlet 111, a hydrogen outlet 112 and an oxygen outlet 113. The methanation unit comprises a catalyst 222, a hydrogen inlet 213, a carbon oxide inlet 214 having a first controllable valve 215 and a methane outlet 216, wherein the hydrogen outlet of the first fuel cell unit is coupled to the hydrogen inlet of the methanation unit, and the methanation unit is adapted to convert hydrogen and carbon oxide into methane, wherein the control unit is adapted to control the first controllable valve so as to obtain an optimum converting process to convert hydrogen and carbon oxide into methane.

Abstract: A process for producing propylene or butene is disclosed, comprising passing a stream comprising 10-70 wt % of diisopropyl ether or 30-95 wt % of di-sec butyl ether over an acid catalyst at a temperature of 180-300° C. and a pressure of 0.01-3 bar g. Also disclosed is a process for producing either isopropanol or 2-butanol, comprising contacting water and a propylene- or butene-containing feedstock in a hydration reaction zone with a hydration catalyst to produce a stream comprising either isopropanol and a by-product stream or 2-butanol and a by-product stream, passing said by-product stream over an acid catalyst at a temperature of 180-300° C. and a pressure of 0.01-3 bar g to produce either propylene or butene, and then recycling said propylene or butene to the hydration reaction zone.

Abstract: A process utilizing an ionic liquid is described. The process includes contacting a hydrocarbon feed with an ionic liquid component, the ionic liquid component comprising a mixture of a first ionic liquid and a viscosity modifier, wherein a viscosity of the ionic liquid component is at least about 10% less than a viscosity of the first ionic liquid.

Abstract: Processes and apparatuses for producing a C8 aromatic isomer product are provided. The apparatus comprises an isomerization unit to provide an isomerized stream. An isomerate stripper column is in communication with the isomerization unit to provide an isomerate stripper overhead stream comprising C6? hydrocarbons in an isomerate overhead line and an isomerate stripper bottoms stream in an isomerate bottoms line. A dividing wall naphthene splitter column is in communication with the isomerate bottoms line to provide an overhead naphthene splitter stream comprising the C8 naphthenes and C7 aromatic hydrocarbons in a naphthene splitter overhead line and a naphthene splitter sidedraw stream comprising C8 aromatic isomers in a naphthene splitter sidedraw line. An extractive distillation column is in communication with the naphthene splitter overhead line to provide a recycle feedstream comprising the C8 naphthenes in a recycle line and an extract stream comprising the C7 aromatic hydrocarbons in an extract line.

Abstract: This invention provides a method for producing 2,3,3,3-tetrafluoropropene or 2-chloro-1,1,1,2-tetrafluoropropane, which is a precursor of 2,3,3,3-tetrafluoropropene, in two or three reaction steps, using at least one chlorine-containing compound selected from the group consisting of 1,1,1,2,3-pentachloropropane, 2,3-dichloro-1,1,1-trifluoropropane, and 1,1,2,3-tetrachloropropene as a starting material, the reaction products of at least two of the steps being supplied to the same distillation apparatus to subject the products to a separation operation simultaneously. With this method, 2,3,3,3-tetrafluoropropene or 2-chloro-1,1,1,2-tetrafluoropropane, which is a precursor of 2,3,3,3-tetrafluoropropene, can be efficiently produced with reduced energy and equipment costs in an economically advantageous manner.

Abstract: A process is provided for the chlorination of ethane using chlorine as the chlorinating agent to produce vinylidene (1,1-dichloroethylene), hydrogen chloride and ethylene.