Patents Issued in October 15, 2019
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Patent number: 10442941Abstract: A heat stable radiation curable epoxy resin composition for preparing an ink composition including: (a) at least one divinylarene dioxide compound; (b) at least one photoinitiator compound; (c) at least one pigment; and (d) at least one optional additive wherein the at least one photoinitiator compound is a triarylsulfonium salt; wherein the at least one pigment is (i) a cyan pigment, or (ii) a magenta pigment; a process for preparing the above heat stable radiation curable epoxy resin composition; and a cured inkjet ink product prepared by curing the above heat stable radiation curable epoxy resin composition.Type: GrantFiled: March 17, 2016Date of Patent: October 15, 2019Assignee: Blue Cube IP LLCInventors: Hamed Lakrout, Katherine Clement, Maurice J. Marks
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Patent number: 10442942Abstract: A radiation-curable ink jet composition contains at least one monomer A represented by general formula (I): CH2?CR1—COOR2—O—CH?CH—R3, wherein R1 represents a hydrogen atom or a methyl group, R2 represents a divalent organic moiety having a carbon number of 2 to 20, and R3 represents a hydrogen atom or a monovalent organic moiety having a carbon number of 1 to 11. The composition also contains a cyclic, linear, or branched monomer B containing a (meth)acryloyloxy or (meth)acryloyl group in which the total number of nitrogen atoms and oxygen atoms other than the oxygen atoms contained in the (meth)acryloyloxy or (meth)acryloyl group is at least 2, and at least one monomer C represented by the following general formula (II): wherein n represents an integer of 2 to 6. The total content of monomer A is 10% by mass or more relative to the total mass of the ink jet composition.Type: GrantFiled: June 28, 2017Date of Patent: October 15, 2019Assignee: Seiko Epson CorporationInventors: Keitaro Nakano, Toshiyuki Yoda
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Patent number: 10442943Abstract: An ink composition for printing by the continuous deflected ink jet technique, liquid at room temperature, including a method for marking or printing on a substrate, support or object using said ink composition, and a substrate, support, or object provided with a marking obtained by drying, and/or absorption of said ink composition, in which the ink composition includes a solvent including one or several organic solvent compounds, and optionally water; a binder comprising at least one binding resin; at least one plasticizer of said binding resin; at least one dye which belongs to the family of anthraquinone dyes; and optionally, at least one or several other dyes and/or pigments which do not belong to the family of anthraquinone dyes.Type: GrantFiled: June 25, 2015Date of Patent: October 15, 2019Assignee: MARKEM-IMAJE HOLDINGInventors: Mickaelle Insulaire, Gregory Guillot-Patrique
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Patent number: 10442944Abstract: Provided is a novel photoinitiator in the form of a hybrid nanoparticle constructed of a semiconductor and metallic regions, and uses thereof.Type: GrantFiled: June 29, 2016Date of Patent: October 15, 2019Assignee: Yissum Research Development Company of the Hebrew University of Jerusalem Ltd.Inventors: Uri Banin, Hermona Soreq, Shlomo Magdassi, Nir Waiskopf, Yuval Ben-Shahar, Amol Ashok Pawar, Shira Halivni
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Patent number: 10442945Abstract: A conductive ink includes a conductive nano-metal and a graphene dispersion liquid. The graphene dispersion liquid includes a graphene. A lateral size of the graphene is between approximately 0.1 micron and approximately 1 micron. The graphene has a weight percentage with respect to the conductive ink ranging from approximately 0.2 wt % to approximately 0.5 wt %.Type: GrantFiled: December 13, 2017Date of Patent: October 15, 2019Assignees: BOE TECHNOLOGY GROUP CO., LTD., Hefei Xinsheng Optoelectronics Technology Co., Ltd.Inventors: Xujie Zhang, Ming Hu, Ming Zhang, Xiaodong Xie, Kongshuo Zhu, Yu Zhu
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Patent number: 10442946Abstract: The present application describes a composition and method thereof to make low cost environment friendly and highly safe conducive ink by using micro-sized silver particles, water, edible level thickener, water-based solvent, water-based resin and surfactant. The conductive ink may be written by various kinds of writing devices like gel pen, ball pen etc. on various substrates like paper, plastic, metal, etc. form a conductive trace. As additional features of the present application, the composition comprises erasable conductive ink, which is fast curing and conductive immediately upon application, having multiple applications for educational purpose to help students have a better understanding of how electronic work and even design their own electronics conveniently.Type: GrantFiled: February 22, 2018Date of Patent: October 15, 2019Assignee: Nano and Advanced Materials Institute LimitedInventors: Yuechen Wang, Tao Xu, Li Fu
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Patent number: 10442947Abstract: Colored fine-particle dispersion for ink-jet printing. The colored fine-particle dispersion is produced by subjecting dispersion including pigment, polymerizable monomer, polymerizable surfactant, and water to emulsion polymerization, including dispersing a mixed solution including the pigment, the polymerizable surfactant, the water, and an organic solvent to prepare a dispersion 1; removing the organic solvent from the dispersion 1 to prepare a dispersion 2; and subjecting the dispersion 2 and the polymerizable monomer to emulsion polymerization to obtain the colored fine-particle dispersion. The process for producing the ink includes mixing the obtained colored fine-particle dispersion and an organic solvent B. The colored fine-particle dispersion includes colored fine-particles with average particle size of 10 to 300 nm.Type: GrantFiled: July 1, 2015Date of Patent: October 15, 2019Assignee: KAO CORPORATIONInventor: Yuuta Matsumoto
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Patent number: 10442948Abstract: Provided is a near infrared absorbing fine particle dispersion liquid, which can be applied to offset printing, including: a solvent of one or more kinds selected from vegetable oils and vegetable oil-derived compounds; near infrared absorbing fine particles of one or more kinds selected from 10 mass % more and 25 mass % or less of a composite tungsten oxide expressed by MxWyOz, and/or a tungsten oxide having a Magneli phase expressed by a general formula WyOz; and a dispersant soluble in the solvent and having a fatty acid in its structure, wherein a viscosity is 180 mPa/S or less.Type: GrantFiled: January 27, 2016Date of Patent: October 15, 2019Assignee: SUMITOMO METAL MINING CO., LTD.Inventors: Mika Okada, Hideaki Fukuyama
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Patent number: 10442949Abstract: A composition for an electric wire coating material that has excellent damage resistance, low-temperature flexibility, tear resistance, and thermal stability, and an insulated electric wire in which this composition is used. The composition for an electric wire coating material containing polyvinyl chloride contains a plasticizer in an amount of 15 to 30 parts by mass and one or more ethylene-based copolymers selected from ethylene-vinyl ester copolymers and ethylene-?,?-unsaturated carboxylic acid ester copolymers in an amount of 0.1 to 10 parts by mass, with respect to 100 parts by mass of the polyvinyl chloride. An insulated electric wire is obtained by coating an outer circumference of a conductor with an insulating coating layer, with this composition for an electric wire coating material used in an electric wire coating material.Type: GrantFiled: September 23, 2016Date of Patent: October 15, 2019Assignees: AUTONETWORKS TECHNOLOGIES, LTD., SUMITOMO WIRING SYSTEMS, LTD., SUMITOMO ELECTRIC INDUSTRIES, LTD.Inventors: Toyoki Furukawa, Hiroaki Kojima
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Patent number: 10442950Abstract: A film is formed on a sliding surface of a component. The film contains fluororesin. The film includes a surface structure in which convex portions are joined with each other like a mesh. Each of the convex portions is formed by particles of fluororesin having aggregated.Type: GrantFiled: May 9, 2018Date of Patent: October 15, 2019Assignee: CANON KABUSHIKI KAISHAInventors: Hirotomo Tamiya, Nobuyuki Kume
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Patent number: 10442951Abstract: The present invention provides an economical route to environmentally friendly polymeric coatings with a high content of raw materials from renewable resources. These polymeric coatings offer performance characteristics that are competitive with conventional coating systems. The unique polymers on which this invention is based are copolymers of triglyceride oils, such as soybean oil, linseed oil, or another natural oil, with a vinyl compound, such as an acrylate or methacrylate, or a vinyl aromatic monomer. The present invention more specifically discloses a water dispersible, self-crosslinkable prepolymer composition which is comprised of a triglyceride oil having appended thereto (1) hydroxyl groups, (2) epoxy groups, (3) moieties which contain at least one aldehyde group or at least one ketone group, and (4) moieties which contain at least one vinyl and/or substituted vinyl group. In one embodiment of this invention the moiety which contains at least one vinyl group is derived from maleic anhydride.Type: GrantFiled: November 28, 2016Date of Patent: October 15, 2019Assignee: Lubrizol Advanced Materials, Inc.Inventor: Anthony D. Pajerski
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Patent number: 10442952Abstract: The present invention comprises a composition and method of use for providing durable dirt pickup resistance to architectural coatings. Such compositions comprise a coating base and a post-modified crosslinkable fluoropolymer additive, such that the coatings additive is allowed to migrate to the coating surface and further cure once applied to a substrate. The compositions of the present invention provide durability to coating compositions, while also providing surface effects such as increased water and oil contact angles, enhanced dirt pickup resistance, and enhanced cleanability to the coating films.Type: GrantFiled: April 27, 2016Date of Patent: October 15, 2019Assignee: THE CHEMOURS COMPANY FC, LLCInventors: Anilkumar Raghavanpillai, Brad M. Rosen, James J. Hughes, Vincent Franco, John Russell Crompton, Jr., Kai Qi, Michael Henry Ober
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Patent number: 10442953Abstract: An aqueous-based coating composition suitable as a container coating comprising: (A) a resinous phase comprising (i) an at least partially neutralized acid functional polymer containing reactive functional groups, (ii) a phenolic compound and an aldehyde or the reaction product thereof, (iii) a hydroxy-terminated polybutadiene; the resinous phase dispersed in (B) aqueous medium.Type: GrantFiled: October 25, 2013Date of Patent: October 15, 2019Assignee: PPG Industries Ohio, Inc.Inventors: Christopher L. Most, Robert McVay
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Patent number: 10442954Abstract: Linear polyfunctional polyglycidyl amine oligomeric and/or polymeric structures exhibiting at least two primary amines are described, which provide crosslinking capabilities for latex paint compositions. These crosslinkers not only exhibit latent crosslinking properties but also improve scrub resistance when compared with existing latex formulations. Once the latex is coated onto a substrate, the volatile base evaporates and the groups react to form a crosslinked coating with improved scrub resistant properties.Type: GrantFiled: September 14, 2017Date of Patent: October 15, 2019Inventor: Jiali Cai
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Patent number: 10442955Abstract: Low VOC, unsaturated alkyd resins are obtained by reacting (A) to (E): (A) optionally from 0 to 30% w/w naturally occurring Rosin, comprising from 40 to 80 w/w parts per hundred of Rosin of an unsaturated mono carboxylic acid with at least one C15-25cyclohydrocarbo moiety capable of a Diels Alder or Ene reaction (preferred monoacids being abietic acid, palustric acid, levopimaric acid, sandaracopimaric acid, and/or anhydrides thereof); (B) from 25 to 80% w/w of a linear C12-60hydrocarbo carboxylic acid with at least one (preferably at least two conjugated) C?C bonds (=unsaturated fatty acid); (C) optionally from 1 to 30% w/w of an ethylenically unsaturated C5-6hydrocarbo dicarboxylic acid and/or anhydride thereof, being reactive as a dienophile and/or enophile with A and/or B (preferred for C are itaconic acid, citraconic acid and/or anhydrides thereof); (D) from 1 to 40% w/w of at least one polyol; (E) optionally at least one monomer other than A to D—the total of A to E being 100%.Type: GrantFiled: January 17, 2018Date of Patent: October 15, 2019Assignee: DSM IP ASSETS B.V.Inventors: Johannes Wilhelmus Maria Hendriks, Adrianus Jozephus Hendricus Lansbergen
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Patent number: 10442956Abstract: The present disclosure relates to a two-component composition containing a polymer polyol, a dial chain extender, an aldimine of formula (I), optionally additional polyols and diphenylmethandiisocyanates in the two components. The composition is particularly suitable as a manually applicable solvent-free liquid film for coating and/or sealing floors and roofs. It also has a long open time, cures quickly and without complications in a wide temperature and humidity range, has a high level of strength and is weather resistant.Type: GrantFiled: September 12, 2016Date of Patent: October 15, 2019Assignee: SIKA TECHNOLOGY AGInventors: Hans Häberle, Urs Burckhardt, Ursula Stadelmann
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Patent number: 10442958Abstract: An anisotropic conductive film contains conductive particles and spacers. The spacers are arranged at a central part of the film in a width direction. The central part of the film in the width direction represents 20 to 80% of the overall width of the film. The height of the spacers in the thickness direction of the anisotropic conductive film is larger than 5 ?m and less than 75 ?m. Such an anisotropic conductive film has a layered structure having a first insulating adhesion layer and a second insulating adhesion layer, wherein the conductive particles are dispersed in the first insulating adhesion layer, and the spacers are regularly arranged on a surface of the first insulating adhesion layer on a side of the second insulating adhesion layer.Type: GrantFiled: January 29, 2015Date of Patent: October 15, 2019Assignee: DEXERIALS CORPORATIONInventors: Yuta Araki, Tomoyuki Ishimatsu
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Patent number: 10442959Abstract: Peelable polymeric film, in particular, peelable polymeric film which comprises a polymeric substrate layer and a coating layer of adhesive, and which is of particular use in the manufacture of electronic devices is described. The adhesive layer is derived from an aqueous composition which comprises an aliphatic polyurethane and is switchable.Type: GrantFiled: April 29, 2016Date of Patent: October 15, 2019Assignee: DUPONT TEIJIN FILMS U.S. LIMITED PARTNERSHIPInventors: Julian N. Robinson, Jackie H. Symonds, Duncan Mackerron, Stephen W. Sankey, Jamie Evans, Rachel Clare Little
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Patent number: 10442960Abstract: The present application relates to an adhesive film, an organic electronic device comprising same, and a lighting apparatus and a display device comprising same. The present application enables an organic electronic device to show excellent moisture-blocking properties and have flexibility as well as excellent and reliable durability at high temperature and high humidity.Type: GrantFiled: June 9, 2016Date of Patent: October 15, 2019Assignee: LG CHEM, LTD.Inventors: Kyung Yul Bae, Yoon Gyung Cho, Hyun Jee Yoo, Se Woo Yang
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Patent number: 10442961Abstract: Provided are a composition which has good elastomer solubility, is thus capable of increasing a concentration of solid contents, and is capable of forming a film having excellent drying properties, surface morphology, and heat resistance, a process for producing a sheet, a sheet, a laminate, and a laminate with a device wafer. This composition includes an elastomer having a 5% thermal mass reduction temperature of 375° C. or higher when heated at an elevation rate of 20° C./min from 25° C., a solvent represented by the following General Formula (1) and having a boiling point of 160° C. or higher, and a solvent having a boiling point of lower than 120° C. In General Formula (1), R1 to R6 each independently represent a hydrogen atom or an aliphatic hydrocarbon group.Type: GrantFiled: March 24, 2017Date of Patent: October 15, 2019Assignee: FUJIFILM CorporationInventors: Yoshitaka Kamochi, Ichiro Koyama, Yu Iwai, Atsushi Nakamura, Mitsuru Sawano
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Patent number: 10442962Abstract: The present invention is related to adhesive compositions comprising about 50 to about 80 wt % of a polymer blend of at least two different propylene-based polymers, wherein the polymer blend has a melt viscosity of about 100 to about 6,000 cP and adhesive compositions comprising about 30 to about 60 wt % of a polymer blend of at least two different propylene-based polymers, wherein the polymer blend has a melt viscosity of about 6,000 cP to about 60,000 cP. When subjected to Temperature Rising Elution Fractionation, the polymer blend exhibits a first fraction that is soluble at ?15° C. in xylene, the first fraction having an isotactic (mm) triad tacticity of about 70 mol % to about 90 mol %; and a second fraction that is insoluble or less soluble than the first fraction at ?15° C. in xylene, the second fraction having an isotactic (mm) triad tacticity of about 85 mol % to about 98 mol %.Type: GrantFiled: October 6, 2014Date of Patent: October 15, 2019Assignee: ExxonMobil Chemical Patents Inc.Inventors: Jurgen J. M. Schroeyers, Jennifer J. Austin, Shawn W. Mowry, James N. Coffey
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Patent number: 10442963Abstract: A hydrophobic binder/adhesive, for treating a substrate, may include about 60% to 98.9% by weight bulk polymer selected from one or more monomers associated with styrene, vinyl acetate, acrylic acid ester, methacrylic acid esters, ethylene, or butadiene; about 0.1% to about 10.0%, by weight of one or more hydrophobic monomers selected from stearyl methacrylate or laurel acrylate; and about 1% to about 30%, by weight of one or more protective colloids associated with a hard resin polymer. The hydrophobic binder/adhesive may increase resistance to wetting of the substrate when expose to moisture, and increases durability of the substrate.Type: GrantFiled: December 21, 2016Date of Patent: October 15, 2019Assignee: McTron Technologies, LLCInventors: Kenneth Loren Snyder, Jr., Larry Milton McDaniel
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Patent number: 10442964Abstract: Multi-component synthetic resin adhesive composition for the fixing sector, especially for adhesively bonding an anchoring element in a hole (for example, a drilled hole) or crevice, comprising fillers, which comprises a biogenic liquid diluting agent (for example a vegetable oil, such as especially castor oil, or a polyol); use of the synthetic resin adhesive composition for embedding anchoring means in mortar in holes or crevices; process or method for embedding anchoring elements in mortar and holes or crevices, in which the synthetic resin adhesive composition is used; and use of biogenic fillers in producing such a synthetic resin adhesive composition.Type: GrantFiled: March 21, 2014Date of Patent: October 15, 2019Assignee: fischerwerke GmbH & Co. KGInventors: Jurgen Grun, Martin Vogel, Christian Schlenk, Christian Weinelt
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Patent number: 10442965Abstract: The present invention contemplates a method for enclosing a panel edge comprising forming a panel structure having at least one edge, applying a reformable epoxy resin material onto the at least one edge, and contacting the reformable epoxy resin material within about 10 minutes, or even about 5 minutes of applying the reformable epoxy resin material such that the reformable epoxy resin material is below its glass transition temperature and dry to the touch upon contact.Type: GrantFiled: October 20, 2017Date of Patent: October 15, 2019Assignee: Zephyros, Inc.Inventors: Sylvain E. Gleyal, Laurent Meistermann
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Patent number: 10442966Abstract: New adhesives and methods for preparing them are disclosed that include polylactic acid irradiated with gamma radiation, such as by a Co60 source. Irradiation times are used that improve the characteristics of the adhesive materials. Generally, the dose of radiation is from about 5 kGy to about 200 kGy of gamma irradiation. The adhesives generally have melting temperatures in the range of at least about 140 to about 148° C. such that they can be conveniently used in conventional glue guns and other glue equipment. The disclosed adhesives can provide bond strengths in the range of about 1,600 psi or more to about 2,500 psi or more. The disclosed adhesives can include a crosslinking agents. They can be used to join a wide range of substrates including wood, metal, plastic, ceramic, glass or combinations of substrates. They can be conveniently prepared by heating a polylactic acid (polylactic acid) preparation and mixing the molten polylactic acid with one or more crosslinkers when present.Type: GrantFiled: November 15, 2013Date of Patent: October 15, 2019Assignee: Purdue Research FoundationInventors: Rusi Taleyarkhan, Alexander Charles Bakken, Kevin F. Fisher, Alexander R. Hagen, Neal P. Kostry
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Patent number: 10442967Abstract: There is provided an article having at least a first surface having: a binder resin layer comprising an actinic radiation reactive polyurethane dispersion, where the binder resin layer has a first major surface opposite a second major surface; and a plurality of microspheres partially embedded and adhered to the first major surface of the binder resin layer. There is also provided a thermoset article derived from such thermoformable articles.Type: GrantFiled: August 12, 2016Date of Patent: October 15, 2019Assignee: 3M Innovative Properties CompanyInventors: Christopher B. Walker, Jr., Abdullahi A. Mohamud, Mary M. Caruso Dailey, Benjamin G. Sonnek
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Patent number: 10442968Abstract: Provided is a latent heat transfer material that is micro-encapsulated, said material exhibiting superior mechanical strength and heat resistance. A production method for the latent heat transfer material that is micro-encapsulated in a hard shell comprises: 1) a step in which a perforate hollow silica particle is manufactured; 2) a step in which the phase change material is sealed inside the perforate hollow silica particle by inserting the perforate hollow silica particle in a molten solution of the phase change material and repeatedly subjecting the same to vibrations such as ultrasound oscillations; 3) a step in which the perforate hollow silica particle having the phase change material sealed within is washed in a saturated aqueous solution of the phase change material; and 4) a step in which perhydropolysilazane is used to coat the outer shell of the perforate hollow silica particle with silica.Type: GrantFiled: August 25, 2014Date of Patent: October 15, 2019Assignee: National University Corporation Kobe UniversityInventors: Hiroshi Suzuki, Yoshiyuki Komoda, Ruri Hidema
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Patent number: 10442969Abstract: One or more embodiments of the present invention provide (i) a novel heat storage material composition, (ii) a heat storage material containing the heat storage material composition, and (iii) a transport container including the heat storage material. A heat storage material composition in accordance with one or more embodiments of the present invention may contain sodium sulfate 10-hydrate, sodium bromide, and sodium chloride, and have a melting point and a solidifying point within a range of 0° C. to 10° C.Type: GrantFiled: September 20, 2018Date of Patent: October 15, 2019Assignee: KANEKA CORPORATIONInventor: Toru Ueda
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Patent number: 10442970Abstract: A solid ice melting composition is composed of pelletized salt, the pelletized salt having a plurality of salt particles pressed together, inter-particle spaces between the salt particles inside the pelletized salt, and a deicing liquid in the inter-particle spaces. The composition is produced by pelletizing a plurality of salt particles to form pelletized salt, and introducing deicing liquid into inter-particles spaces between the salt particles in the pelletized salt by infusing the deicing liquid into the pelletized salt. The solid ice melting composition is easy to handle and spread, is longer lasting and is effective at temperatures down to about ?30° C. or lower.Type: GrantFiled: February 16, 2018Date of Patent: October 15, 2019Assignee: 9533109 Canada Inc.Inventor: Peter Burley Neal
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Patent number: 10442971Abstract: A drilling mud composition including Aloe vera particles with a largest dimension of 75-600 ?m, an aqueous base fluid, and a viscosifier, where the Aloe vera particles are present in the drilling mud composition at a concentration of less than 150 ppm, relative to the total weight of the drilling mud composition. A process for fracking a geological formation, whereby the drilling mud composition is injected into the geological formation through a well bore at a pressure of at least 5,000 psi to fracture the geological formation.Type: GrantFiled: January 29, 2018Date of Patent: October 15, 2019Assignee: King Fahd University of Petroleum and MineralsInventor: Mohammed Enamul Hossain
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Patent number: 10442972Abstract: A drilling fluid composition including a viscosifier, treated date pit particles which are i) de-oiled and ii) treated with a base or both a base and an acid, and an aqueous base fluid, wherein the treated date pit particles are present in an amount of 0.01-5 wt %, relative to a total weight of the drilling fluid composition. A method of making the drilling fluid composition by de-oiling date pit particles, treating with a base or a base and an acid in a freeze/thaw process, and adding the freeze/thaw mixture to the viscosifier and the aqueous base fluid. A process for drilling a subterranean geological formation with the drilling fluid composition.Type: GrantFiled: January 29, 2018Date of Patent: October 15, 2019Assignee: King Fahd University of Petroleum and MineralsInventors: Jimoh K. Adewole, Musa O. Najimu
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Patent number: 10442973Abstract: The invention relates to the field of petroleum drilling fluids, and discloses a super-amphiphobic strongly self-cleaning high-performance water-based drilling fluid comprising polymeric super-amphiphobic agent and a drilling method. The polymeric super-amphiphobic agent comprises structural units A derived from acrylamide, structural units B derived from methyl methacrylate, structural units C derived from butyl acrylate, structural units D derived from a compound represented by the following formula (1), structural units E derived from a silane coupler, and nano-titania; wherein the nano-titania is bonded to the polymeric super-amphiphobic agent via the structural unit E, and the silane coupler is a silane coupler having double bonds; R is a C3-C8 perfluoroalkyl group. A water-based drilling fluid additive prepared from the polymeric super-amphiphobic agent in the present invention has excellent wettability, inhibition, lubrication, reservoir protection, and rheology and fluid loss properties.Type: GrantFiled: April 23, 2019Date of Patent: October 15, 2019Assignee: CHINA UNIVERSITY OF PETROLEUM (BEIJING)Inventors: Guancheng Jiang, Xiaoxiao Ni, Lili Yang, Yinbo He, Xiaohu Quan, Zhong Li, Xiaoyong Wang, Yongbin Guo, Fabin Xu, Zhengqiang Deng, Xi Wang, Deli Gao, Kai Wang, Xuwu Luo, Chunyao Peng
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Patent number: 10442974Abstract: In some instances, a fluid loss control enhancement additive may synergistically work with lost circulation materials (“LCM”) to arrest lost circulation in wellbores where LCMs alone have been ineffective. For example, a method may involve treating a wellbore penetrating a subterranean formation with a pill comprising an aqueous base fluid and a lost circulation material; observing fluid loss from the wellbore to the subterranean formation while treating the wellbore with the pill; and adding salt, a swellable polymer, and fibers to the pill.Type: GrantFiled: January 14, 2014Date of Patent: October 15, 2019Assignee: Halliburton Energy Services, Inc.Inventors: Donald Lee Whitfill, Sharath Savari, Matthew L. Miller, Dale E. Jamison, Robert J. Murphy
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Patent number: 10442975Abstract: In an embodiment, the cement compositions comprise: (i) hydraulic cement, wherein the hydraulic cement has a ratio of CaO to SiO2 in the range of 2.0 to 4.0; and (ii) a water-soluble metaphosphate in a concentration of at least 2.5% bwoc. In another embodiment, the cement compositions comprise: (i) hydraulic cement, wherein the hydraulic cement has a ratio of CaO to SiO2 of less than 2.0; and (ii) a water-soluble metaphosphate; wherein any alkali nitrate is in a concentration of less than 2% bwoc; and wherein any alkali hydroxide, alkali carbonate, or alkali citrate is in a concentration of less than 0.2% bwoc. Methods of cementing in a well comprising forming either of such cement compositions and introducing it into the well are provided.Type: GrantFiled: March 3, 2015Date of Patent: October 15, 2019Assignee: Halliburton Energy Services, Inc.Inventors: Rahul Chandrakant Patil, Sandip Prabhakar Patil, Sohini Bose, Ashok K. Santra, Balasundaram Balaraman
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Patent number: 10442976Abstract: An oil-soluble coated particle flow modifier, a preparation method thereof, and a use thereof in fractured-vuggy carbonate reservoirs mining. The oil-soluble coated particle flow modifier is of a core-shell structure, which has a core layer of a coated core and a shell layer of a coating agent, wherein the coated core is made of a plugging material, and the coating agent consists of petroleum resin and hollow beads. Based on the total weight of the coated particle flow modifier, the content of the petroleum resin, the hollow beads, the cotton linters, and the coated cores is 10-40 wt %, 9-40 wt %, 1-10 wt %, and 35-80 wt %, respectively. A preparation method of the coated particle flow modifier and a use of the coated particle flow modifier in fractured-vuggy carbonate reservoirs mining to improve oil recovery is also provided.Type: GrantFiled: February 14, 2019Date of Patent: October 15, 2019Assignees: China University of Geosciences (Beijing), China University of Petroleum (East China)Inventors: Qing You, Caili Dai, Long He, Jichao Fang, Baolei Jiao, Liang Li, Guang Zhao, Yifei Liu, Yan Zhang, Pan Wang
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Patent number: 10442977Abstract: A cleanup fluid for reducing a viscosity of a residual viscous material in fractures of a hydrocarbon-bearing formation. The cleanup fluid includes an exothermic reaction component operable to generate heat, where the heat is operable to reduce a viscosity of the residual viscous material to create a reduced viscosity material, the reduced viscosity material operable to flow from the fractures.Type: GrantFiled: February 22, 2019Date of Patent: October 15, 2019Assignee: SAUDI ARABIAN OIL COMPANYInventors: Ayman R. Al-Nakhli, Hazim H. Abass, Ahmad S. Al-Otaibi
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Patent number: 10442978Abstract: A cleanup fluid for reducing a viscosity of a residual viscous material in fractures of a hydrocarbon-bearing formation. The cleanup fluid includes an exothermic reaction component operable to generate heat, where the heat is operable to reduce a viscosity of the residual viscous material to create a reduced viscosity material, the reduced viscosity material operable to flow from the fractures.Type: GrantFiled: February 22, 2019Date of Patent: October 15, 2019Assignee: SAUDI ARABIAN OIL COMPANYInventors: Ayman R. Al-Nakhli, Hazim H. Abass, Ahmad S. Al-Otaibi
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Patent number: 10442979Abstract: Injection fluid tuning is provided. In one possible implementation, injection fluid can be tuned by accessing both surface properties of rock found in a hydrocarbon reservoir of interest and a chemical composition of oil found in the reservoir of interest. An ion effect on wettability of a contact surface of the rock can be acquired and then used to formulate a tuned ion solution based on the ion effect on wettability of the contact surface of the rock. In another possible implementation, an electrolyte solution has an ionic composition and an ionic concentration configured to enhance recovery of oil from a reservoir. The electrolyte solution includes a content of direct contact ions including monovalent ions with a static polarizability larger than a preset limit sufficient to influence a contact surface of a rock in the reservoir to reach a desired wettability.Type: GrantFiled: June 8, 2015Date of Patent: October 15, 2019Assignees: SCHLUMBERGER TECHNOLOGY CORPORATION, UNIVERSITY OF STRATHCLYDEInventors: Wael Abdallah, Mikhail Stukan, Reza Taherian, Maxim Fedorov
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Patent number: 10442980Abstract: Emulsions of mobility control polymers can be used to increase recovery of crude oil from a subterranean hydrocarbon-containing formation. A flooding fluid comprising the polymer emulsions are injected into a well that is in contact with the subterranean hydrocarbon-containing formation. The polymers can be temporarily cross-linked and have protected shear degradation and improved injectivity into the well; the shear resistance can be measured in terms of viscosity loss due to shear, and the improved injectivity can be measured in terms of the flooding fluid's filter ratio, flow rate, and viscosity.Type: GrantFiled: July 29, 2014Date of Patent: October 15, 2019Assignee: Ecolab USA Inc.Inventors: Xiaojin Harry Li, Peter E. Reed, William J. Andrews
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Patent number: 10442981Abstract: The present invention is related to the obtaining and use of zwitterionic geminal liquids based on hydroxypropyl betaine, as wettability modifiers of rocks such as limestone, dolomite, sandstone, quartz or heterogeneous lithologies, in the presence of brines with high content of divalent ions as calcium, magnesium, barium and strontium, at high temperature and high pressure conditions during the application of enhanced oil recovery processes. The zwitterionic geminal liquids based hydroxypropyl betaine of the present invention have also the property of acting as inhibitors/dispersing of asphaltenes, both at extraction and production operations of petroleum industry, thus allowing to increase the level of crude oil production. An additional advantage presented by zwitterionic geminal liquid based on hydroxypropyl betaine which can be dissolved in distilled water, brine, aliphatic hydrocarbons or other polar and nonpolar solvents.Type: GrantFiled: November 17, 2015Date of Patent: October 15, 2019Assignee: INSTITUTO MEXICANO DEL PETRÓLEOInventors: Violeta Yázmin Mena Cervantes, Raúl Hernández Altamirano, Luis Silvestre Zamudio Rivera, Alejandro Ramírez Estrada, Jorge Francisco Ramírez Pérez, José Manuel Martínez Magadan, Rodolfo Cisneros Devora
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Patent number: 10442982Abstract: To deliver surfactants or tracers to underground oil fields, inorganic encapsulated surfactant nanoparticles or microparticles that are stable for several weeks under high temperature and high salt conditions can be used.Type: GrantFiled: May 20, 2016Date of Patent: October 15, 2019Assignee: MASSACHUSETTS INSTITUTE OF TECHNOLOGYInventors: Angela M. Belcher, Nurxat Nuraje, Yu Lei, Hiroshi Atsumi, Xunpei Liu
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Patent number: 10442983Abstract: The present application relates to methods and systems for mitigating condensate banking. In some embodiments, the methods and systems involve altering the wettability of a rock formation in the vicinity of a wellbore for a gas condensate reservoir.Type: GrantFiled: July 18, 2018Date of Patent: October 15, 2019Assignee: Saudi Arabian Oil CompanyInventors: Mohammed Sayed, Feng Liang, Hooisweng Ow, Jason Cox
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Patent number: 10442984Abstract: Methods and compositions for treating subterranean formations, and more specifically, to smart fracturing fluids. In one or more embodiments, the methods comprise providing a fracturing fluid that comprises a base fluid and an additive having a high dielectric constant; and introducing the fracturing fluid into least a portion of a subterranean formation. In one or more embodiments, the compositions comprise a base fluid and an additive having a high dielectric constant.Type: GrantFiled: December 3, 2014Date of Patent: October 15, 2019Assignee: Halliburton Energy Services, Inc.Inventors: Raed Rahal, Michael Bittar
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Patent number: 10442985Abstract: A dry polymer powder for use in enhanced petroleum recovery without being prehydrated before being added to water or brine to be introduced into a wellhead. The dry polymer powder consisting of at least one of a polyacrylamide, a copolymer of acrylamide and acrylic acid, a functionalized derivatives thereof, a galactomannan, or cellulosic polymer or derivatives thereof, and the polymer can be crosslinked or not crosslinked, provided that if they are homo- or co-polymers of acrylic acid, they are not crosslinked. The dry polymer powder is sized between two size limits, namely at least about 85 wt % of particles of a size smaller than about 40-mesh, and at least 75 wt % of particles of a size greater than 200-mesh, which size range ensures that the dry polymer powder will efficiently hydrate in the water or brine within about one minute without forming fisheyes.Type: GrantFiled: June 16, 2017Date of Patent: October 15, 2019Assignee: CHEMEOR, INC.Inventors: Yongchun Tang, Allen Thomas Lyssy, Yaser Asgari, Carl Wilhelm Aften, Hongxin Tang
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Patent number: 10442986Abstract: Systems and methods for treating subterranean formations including quantifying additive concentrations. Certain of those methods include; introducing a fluid including an aqueous base fluid and a friction reducer into a wellbore penetrating of a subterranean formation at a pressure sufficient to create or enhance one or more fractures within the subterranean formation; recovering a portion of the fluid from the wellbore; adding a reactive agent to a sample of the portion of the fluid that has been recovered from the wellbore, where the reactive agent reacts with the friction reducer to form a photo-detectable compound in the sample; measuring a light absorbance of the sample at a selected wavelength of light; and using the measured absorbance and a calibration curve for the selected wavelength of light to determine the concentration of the friction reducer in the fluid that has been recovered from the wellbore.Type: GrantFiled: May 31, 2016Date of Patent: October 15, 2019Assignee: Multi-Chem Group, LLCInventors: Kai He, Liang Xu, Paul Lord
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Patent number: 10442987Abstract: A fluorescent member includes: a plurality of fluorescent particles; an inorganic binder; and a plurality of pores. An upper surface of the fluorescent member is a light extraction surface of the fluorescent member. The plurality of pores are localized in a vicinity of at least one of the plurality of fluorescent particles in a cross section that is parallel to the upper surface of the fluorescent member and extends through the fluorescent particles and the pores.Type: GrantFiled: August 30, 2018Date of Patent: October 15, 2019Assignee: NICHIA CORPORATIONInventors: Toru Takasone, Masahiko Sano, Hiroyuki Inoue, Shoichi Yamada, Takafumi Sugiyama
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Patent number: 10442988Abstract: The method for preparing water-dispersible core-shell quantum dots stabilized with a layer of hydrophilic surface ligands includes making a core of PbS nanocrystals, and obtaining the shell of CdS layer and the surface ligands of dithiocarbamates obtained by reacting amino acids with carbon disulphide, while maintaining the photoluminescence. The emulsion formed of an aqueous solution of amino acid and carbon disulphide includes adding a solution of PbS/CdS in chloroform (CHCl3). Then, the contents are stirred vigorously for at least 20 hours, then the phases are separated. The upper, aqueous phase, being a solution of PbS/CdS/DTC-amino acid residue, is subjected to purification. The present invention is also colloid and a method for preparing colloid.Type: GrantFiled: November 19, 2015Date of Patent: October 15, 2019Assignee: UNIWERSYTET WROCLAWSKIInventors: Jakub Cichos, Miroslaw Karbowiak
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Patent number: 10442989Abstract: A scintillation crystal can include Ln(1-y)REyX3, wherein Ln represents a rare earth element, RE represents a different rare earth element, y has a value in a range of 0 to 1, and X represents a halogen. In an embodiment, RE is Ce, and the scintillation crystal is doped with Sr, Ba, or a mixture thereof at a concentration of at least approximately 0.0002 wt. %. In another embodiment, the scintillation crystal can have unexpectedly improved linearity and unexpectedly improved energy resolution properties. In a further embodiment, a radiation detection system can include the scintillation crystal, a photosensor, and an electronics device. Such a radiation detection system can be useful in a variety of radiation imaging applications.Type: GrantFiled: July 24, 2018Date of Patent: October 15, 2019Assignee: SAINT-GOBAIN CERAMICS & PLASTICS, INC.Inventors: Peter R. Menge, Vladimir Ouspenski
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Patent number: 10442990Abstract: A liquid-crystal medium having a component A which is one or more compounds of the formula IA and corresponding, novel mesogenic compounds and the preparation thereof. These liquid-crystal media, are used in components for high-frequency technology, and to components of this type which contain the media. The components are suitable, in particular, for phase shifters in the microwave and millimeter wave region, for microwave and millimeter wave array antennae and very particularly for so-called tunable “reflectarrays”.Type: GrantFiled: February 27, 2012Date of Patent: October 15, 2019Assignee: Merck Patent GmbHInventors: Christian Jasper, Elvira Montenegro, Detlef Pauluth, Volker Reiffenrath, Atsutaka Manabe
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Patent number: 10442991Abstract: Shown is a liquid crystal composition satisfying at least one of characteristics such as high maximum temperature, low minimum temperature, small viscosity, suitable optical anisotropy, large dielectric anisotropy and small frequency dependence, or has a suitable balance regarding at least two of the characteristics, and an AM device including the composition. The liquid crystal composition contains a specific compound having large positive dielectric anisotropy as a first component, and a specific compound having small viscosity as a second component, and may contain a specific compound having high maximum temperature or small viscosity as a third component, a specific compound having positive dielectric anisotropy as a fourth component or a specific compound having negative dielectric anisotropy as a fifth component.Type: GrantFiled: April 5, 2017Date of Patent: October 15, 2019Assignees: JNC CORPORATION, JNC PETROCHEMICAL CORPORATIONInventors: Naoko Matsuda, Masayuki Saito