Organic Product Patents (Class 117/5)
  • Patent number: 5772754
    Abstract: An electron beam of more than 1.times.10.sup.19 e/cm.sup.2 .multidot.sec is irradiated to metastable metal oxide particles such as .theta.-Al.sub.2 O.sub.3 particles or the like disposed on an amorphous carbon film. A phase transformation or the like of the metastable metal oxide particles is occurred by the electron beam irradiation. Thus, stable metal oxide ultrafine particles such as an .alpha.-Al.sub.2 O.sub.3 ultrafine particle 2 whose diameter is more tiny than the metastable metal oxide particles used, and a metal ultrafine particle composed of an oxide such as Al ultrafine particles are produced.
    Type: Grant
    Filed: February 7, 1996
    Date of Patent: June 30, 1998
    Assignees: Research Development Corporation of Japan, Shun-ichiro Tanaka
    Inventors: Shun-ichiro Tanaka, Bing She Xu
  • Patent number: 5746823
    Abstract: A method for forming an optical device includes the steps of providing a first plate having a first face defining a recess, filling the recess with a material which can be crystallized, and covering the first face and the recess with a second plate having a second face, so that the second face is in contact with the first face and the material in the recess is completely enclosed by the first and second plates. The material in the recess is thereby protected from chemical and mechanical damage, as well as evaporation. In addition, the plates can be transparent, allowing the material in the recess to be visually monitored. A grown crystalline film packed in the cell can be used as a non-liner and/or electro-optical device.
    Type: Grant
    Filed: September 8, 1995
    Date of Patent: May 5, 1998
    Assignee: University of Puerto Rico
    Inventor: Alexander Leyderman
  • Patent number: 5593494
    Abstract: Process for controlling the density of oxygen precipitate nucleation centers in single crystal silicon. In the process, the single crystal silicon is annealed at a temperature of at least about 350.degree. C. to cause the formation of oxygen precipitate nucleation centers in the single crystal silicon. During the annealing step, the single crystal silicon is heated (or cooled) to achieve a first temperature, T.sub.1, which is between about 350.degree. C. and about 500.degree. C. The temperature is then increased from T.sub.1 to a second temperature, T.sub.2, which is between about 500.degree. C. and about 750.degree. C. with the average rate of temperature increase from T.sub.1 to T.sub.2 being less than about 25.degree. C. per minute. The annealing is terminated at a point in time when the oxygen precipitate nucleation centers are capable of being dissolved by heat-treating the silicon at a temperature not in excess of about 1150.degree. C.
    Type: Grant
    Filed: March 14, 1995
    Date of Patent: January 14, 1997
    Assignee: MEMC Electronic Materials, Inc.
    Inventor: Robert Falster
  • Patent number: 5385116
    Abstract: A method for producing a crystal film of an organic compound from a molten liquid or solution of the organic compound on a substrate or between a pair of substrates, the substrate or at least one of the pair of substrates having on a part of the surface thereof a three-dimensional geometrical structure capable of controlling the direction of the crystal growth of the organic compound, and the other part of the surface thereof than the part having a three-dimensional geometrical structure being smooth. The resulting crystal film comprises a sufficiently large single crystal for application to a practical element with its orientation controlled in an arbitrarily selected direction.
    Type: Grant
    Filed: March 23, 1993
    Date of Patent: January 31, 1995
    Assignee: Sumitomo Electric Industries, Ltd.
    Inventors: Yasuhiro Hattori, Akira Mizoguchi, Michiru Kubata
  • Patent number: 5360477
    Abstract: A process for fabricating diamond from a starting powder material containing carbon as the principal component, and said process comprising bringing said powder material under high pressure, wherein, said powder material containing carbon as the principal component is a powder material containing C.sub.60 and/or carbon microtubules as the principal component, andsaid powder material is brought under high pressure by applying a gradient pressure to the material, while the portion of the powder material to which maximum pressure is applied is irradiated by a laser beam optionally through a diamond window material. An apparatus for fabricating diamond is also described.
    Type: Grant
    Filed: March 2, 1993
    Date of Patent: November 1, 1994
    Assignee: Semiconductor Energy Laboratory Co., Ltd.
    Inventors: Tohru Inoue, Masaya Kadono, Akiharu Miyanaga