Treating Starch Patents (Class 127/71)
  • Patent number: 7045003
    Abstract: The invention relates to a process for producing a pregelatinized starch having good gel-formation properties, in which a) a suspension of starch and water is prepared, b) the suspension prepared in a) is applied to a hot roller of a roller dryer, and c) the pregelatinized starch obtained by process step b) s isolated. According to the invention a potato starch having an amylose content of at least 30% by weight is used.
    Type: Grant
    Filed: December 19, 2002
    Date of Patent: May 16, 2006
    Assignee: Bayer Cropscience GmbH
    Inventors: Rudolf Klingler, Karl-Georg Busch
  • Patent number: 7041369
    Abstract: The present invention relates to starch compositions which contain starch and additives. The starch has a weight average molecular weight ranging from about 1,000 to about 2,000,000. The additives can be plasticizers or diluents. The composition containing the starch and the additive is formed by means of passing the composition through a die to produce fibers, foams or films. These compositions have an extensional viscosity in the range from about 50 to about 20,000 pascal seconds. The starch compositions preferably contain a polymer that is substantially compatible with starch and has a weight-average molecular weight of at least 500,000.
    Type: Grant
    Filed: November 27, 2000
    Date of Patent: May 9, 2006
    Assignee: The Procter & Gamble Company
    Inventors: Larry Neil Mackey, Michael David James, Gregory Charles Gordon, John Gerhard Michael, Paul Dennis Trokhan, Valerie Ann Bailey
  • Patent number: 7001939
    Abstract: Wheat starch of the present invention is obtained from endosperm of a seed of wheat which is modified to lack starch granule protein-1 (SGP-1). The wheat starch has an apparent amylose content of about 35% or more. Wheat flour of the present invention is obtained from endosperm of a seed of wheat which is modified to lack SGP-1. Wheat of the present invention is modified to lack SGP-1. The wheat flour and the wheat comprise wheat starch which has an apparent amylose content of about 35% or more.
    Type: Grant
    Filed: April 24, 2001
    Date of Patent: February 21, 2006
    Assignee: National Institute of Agrobiological Sciences
    Inventor: Makoto Yamamori
  • Patent number: 6936109
    Abstract: A method produces starch or starch-containing products from starch-containing plant raw materials. The method is distinguished by the inclusion of an electric pulse method.
    Type: Grant
    Filed: December 3, 2003
    Date of Patent: August 30, 2005
    Assignee: Suedzucker AG Mannheim/Ochsenfurt
    Inventors: Dietmar Grüll, Robert Wittenberger, Michel Marnik Wastyn
  • Patent number: 6929815
    Abstract: The invention relates to a process for increasing the content of ?-amylase-resistant starch (RS content) of a polysaccharide wherein the polysaccharide used is, under a water deficit, incubated, then cooled, if appropriate dried and a polysaccharide having an RS content increased compared with the polysaccharide used is obtained.
    Type: Grant
    Filed: December 9, 2000
    Date of Patent: August 16, 2005
    Assignee: Celanese Ventures GmbH
    Inventors: Holger Bengs, Gisela Jacobasch, Detlef Schmiedl
  • Patent number: 6896915
    Abstract: The present invention relates to a method for glazing a food comprising applying a solution of a glaze base containing a converted starch to the food and drying the food; a process for preparing the starch; the starch prepared therefrom; and a glaze comprising the glaze bases thereof.
    Type: Grant
    Filed: November 13, 2001
    Date of Patent: May 24, 2005
    Assignee: National Starch and Chemical Investment Holding Corporation
    Inventors: Yong-Cheng Shi, Chung-Wai Chiu, David P. Huang, Danuta Janik
  • Patent number: 6890571
    Abstract: This patent pertains to a slowly digestible starch prepared by debranching low amylose starches, particularly by isoamylase. Such slowly digestible starches are useful in edible products, including nutritional supplements.
    Type: Grant
    Filed: May 14, 2002
    Date of Patent: May 10, 2005
    Assignee: National Starch and Chemical Investment Holding Corporation
    Inventors: Yong-Cheng Shi, Xiaoyuan Cui, Anne M. Birkett, Michael G. Thatcher
  • Patent number: 6864063
    Abstract: The invention relates to the use of modified starch obtainable by treating amylose containing starch in aqueous medium with an enzyme from the group of the ?-1,4-?-1,4-glucosyl transferases (EC 2.4.1.25) or an enzyme the activity of which corresponds to that of enzymes from the group just mentioned, as an agent for forming a thermoreversible gel. The invention also relates to products in the form of a thermoreversible gel having as gel-forming substance a modified starch as defined. The invention further relates to the use of a modified starch as defined in the form of an aqueous solution.
    Type: Grant
    Filed: April 3, 2002
    Date of Patent: March 8, 2005
    Assignee: Cooperatieve Verkoop-en Productievereniging van Aardappelmeel en Derivaten AVEBE B.A.
    Inventors: Gerrit Jan Willem Euverink, Doede Jacob Binnema
  • Patent number: 6844022
    Abstract: The present invention is in the technical field of physicochemical starch modification and relates to a process for producing thermochemically modified starch, the thin-boiling starches which are obtainable by the inventive process and thermally reversible gel-forming dextrins, and to their use, in particular as gelatin substitute or fat substitute.
    Type: Grant
    Filed: February 14, 2001
    Date of Patent: January 18, 2005
    Assignee: Bayer CropScience GmbH
    Inventors: Rudolf Klingler, Karl-Georg Busch
  • Patent number: 6770148
    Abstract: The present invention provides a peritoneal dialysis solution that contains heat stable osmotic agents such as D-glucitols, gluconic acids and alkylglycosides produced the reduction, oxidation or glycosylation of icodextrins respectively. As a result, osmotic agents that are stable under autoclaving or heat sterilization conditions are provided which reduces the amount of bioincompatible materials in the sterilized peritoneal dialysis solutions. Methods of preparing the D-glucitols, gluconic acids and alkylglycosides are disclosed.
    Type: Grant
    Filed: December 4, 1998
    Date of Patent: August 3, 2004
    Assignee: Baxter International Inc.
    Inventors: Annamaria Naggi, Enrico Petrella, Giangiacomo Torri, Benito Casu
  • Patent number: 6755915
    Abstract: A method for the preparation of starch particles in a two-phase system comprises at least the following steps: a) a preparation of a first phase comprising a dispersion of starch in water; b) preparation of a dispersion or emulsion of the first phase in a second liquid phase, with the proviso that the second phase is not water; c) cross-linking of the starch present in the first phase; d) separating the starch particles thus formed. According to a first aspect of the invention the second phase consists of a hydrophobic liquid and step b) consists in forming an oil-in-water emulsion, which is then inverted to a water-in-oil emulsion. According to a second aspect of the invention, the second phase consists of a water-miscible non-solvent for starch. Starch particles of very small particles size can be produced in a controlled manner by means of this method.
    Type: Grant
    Filed: October 1, 2001
    Date of Patent: June 29, 2004
    Assignee: Ecosynthetix Inc.
    Inventors: Jeroen Johannes Gerardus Van Soest, Frank Hubertus Maria Stappers, Renée Josie Gide Van Schijndel, Kornelis Fester Gottlieb, Herman Feil
  • Patent number: 6746542
    Abstract: A process for modifying starch by heating starch in an aqueous medium to temperatures above the gelatinization temperature of said starch comprises effecting said modifying of said starch in the presence of (a) a polymeric cationizer selected from the group consisting of the polymers containing vinylamine units and having molar masses of up to 1 million, the polyethyleneimines, the polydiallyldimethylammonium chlorides, the condensates of dimethylamine with epichlorohydrin or dichloroalkanes, the condensates of dichloroethane and ammonia, and the mixtures thereof, and (b) polymeric papermaking drainage aids selected from the group consisting of the water-soluble crosslinked polyamidoamines with or without an ethyleneimine graft, the polymers containing acrylamide and/or methacrylamide units and having molar masses of more than 1 million, the polymers containing vinylamine units and having molar masses of more then 1 million, and the mixtures thereof.
    Type: Grant
    Filed: September 27, 2001
    Date of Patent: June 8, 2004
    Assignee: BASF Aktiengesellschaft
    Inventors: Primoz Lorencak, Andreas Stange, Kurt Diehl, Norbert Mahr
  • Patent number: 6676984
    Abstract: Modified starch materials having a number average molecular weight of at least 10,000 for nutritional products provide a relatively slow release of metabolizable carbohydrates, giving a source of carbohydrate energy over a longer period of time than can be obtained from glucose and other carbohydrates such as lactose, fructose, or sucrose. Such modified starch material possess altered processing and pasting profile characteristics.
    Type: Grant
    Filed: October 8, 1998
    Date of Patent: January 13, 2004
    Assignee: Iowa State University Research Foundation, Inc.
    Inventors: Rickey L. Sharp, John F. Robyt, Murray L. Kaplan
  • Patent number: 6670470
    Abstract: The present invention relates to a process for the preparation of a stable, chlorine free modified starch which is useful in paper coating and sizing. In the process, starch is degraded by catalyzed hydrogen peroxide oxydation, and stabilized by acetyl esterification, combined with crosslinking of the starch.
    Type: Grant
    Filed: March 10, 2000
    Date of Patent: December 30, 2003
    Assignee: Raisio Chemicals Ltd.
    Inventors: Hannu Ketola, Peggy Hagberg
  • Patent number: 6664389
    Abstract: Highly resistant granular starches may be produced which have unique and useful properties, including high enzyme resistance, dietary fiber, a unique molecular weight distribution, a high melting temperature and a high heat of gelatinization (Delta H) indicative of excellent processing tolerance. These starches may be prepared for example by heating a high amylose starch having at least 40% by weight amylose content and at a percent moisture and temperature insufficient to destroy the granular nature of the starch, and digesting the amorphous regions using alpha-amylase or a chemical reagent.
    Type: Grant
    Filed: September 27, 2000
    Date of Patent: December 16, 2003
    Assignee: National Starch and Chemical Investment Holding Coporation
    Inventors: Yong-Cheng Shi, Roger Jeffcoat
  • Patent number: 6648978
    Abstract: An improved corn wet milling process is disclosed in which a first stream comprising water, starch, and protein (e.g., gluten) is generated by separating fiber from wet milled de-germed corn particles (e.g. fiber separation step). Membrane filtration (e.g. starch-protein stream thickening) is performed on the first stream, producing a first retentate and a first aqueous permeate. The first retentate (e.g. thickened starch-protein stream) is separated into a second stream and a third stream (e.g. primary starch separation step). The second stream comprises water and a majority of the starch present in the first retentate, and the third stream comprises water and a majority of the protein (e.g., gluten) present in the first retentate. This process provides an economical means of recovering a higher percentage of the available cornstarch for inclusion in high value products.
    Type: Grant
    Filed: October 15, 2001
    Date of Patent: November 18, 2003
    Assignee: A. E. Staley Manufacturing Co.
    Inventors: Gin C. Liaw, Munir Cheryan, Roy O. Elmore
  • Patent number: 6623943
    Abstract: The present invention relates to a process for preparing resistant starch, the resistant starch obtainable from this process and use thereof.
    Type: Grant
    Filed: March 9, 2000
    Date of Patent: September 23, 2003
    Assignee: Bayer Corporation GmbH
    Inventors: Detlef Schmiedel, Bärbel Johanna König, Gisela Jacobasch
  • Patent number: 6617447
    Abstract: The present invention relates to a method of starch production using continuous oxidation. This method allows for the starting material to contain variable amounts of non-starch products, which is common in large-scale processes. This method produces consistently oxidized starch products that exhibit a reduced tendency to form amylose crystals. Using this continuous reactor with multiple stages, it is possible to produce oxidized starch at any given viscosity.
    Type: Grant
    Filed: November 8, 2001
    Date of Patent: September 9, 2003
    Assignee: Archer-Daniels-Midland Company
    Inventors: Tanja Gnad, James McClain
  • Patent number: 6613152
    Abstract: The invention relates to a process for preparing a starch dextrin wherein a starch comprising at least 95 wt. %, based on dry substance of the starch, of amylopectin or a derivative of said starch is dextrinized. The invention further relates to a dextrin obtainable by said process and to the use thereof as an adhesive.
    Type: Grant
    Filed: January 29, 2001
    Date of Patent: September 2, 2003
    Assignee: Cooperatieve Verkoop-en Productievereniging van Aardappelmeel en Derivaten Avebe B.A.
    Inventors: Augustinus Arnoldus M. Maas, Johanuddes Cornelis P. Hopman, Ronald Peter W. Kesselmans
  • Publication number: 20030051726
    Abstract: A process for the oxidation of starch to obtain carbonyl-substituted starch using V, Cr, Mn, Fe, Co or Cu, wherein Fe and/or Cu are preferred as catalyst. The oxidation of the starch proceeds in quasi-dry form by spraying the dry starch with solutions containing hydrogen peroxide and/or the catalyst and mixing the moistened powder. Oxidized starch containing up to approx. 10 carbonyl groups per 100 glucose units is obtainable.
    Type: Application
    Filed: September 19, 2002
    Publication date: March 20, 2003
    Inventors: Stefan Leininger, Thomas Haas, Dietmar Bischoff, Rudolf Vanheertum, Armin Ecker
  • Publication number: 20030029444
    Abstract: The subject of the present invention is a process for preparing pregelatinized high amylose starch, comprising the steps consisting of:
    Type: Application
    Filed: March 25, 2002
    Publication date: February 13, 2003
    Inventors: Domenico Carbone, Claude Quettier, Giovanni Semino, Ernesto Fossati
  • Patent number: 6485575
    Abstract: A method of producing starch-emulsifier compositions by heating a starch in the presence of an emulsifier to form a complex with unique properties. The product can be further treated to obtain greater than about 20% short chain amylose. Starch-emulsifier compositions (e.g., powders, gels, pastes) produced by this method and food products containing the starch-emulsifier composition are also described.
    Type: Grant
    Filed: October 23, 2001
    Date of Patent: November 26, 2002
    Assignee: Opta Food Ingredients, Inc.
    Inventor: Chienkuo Ronnie Yuan
  • Publication number: 20020152931
    Abstract: A method of producing starch-emulsifier compositions by heating a starch in the presence of an emulsifier to form a complex with unique properties. The product can be further treated to obtain greater than about 20% short chain amylose. Starch-emulsifier compositions (e.g., powders, gels, pastes) produced by this method and food products containing the starch-emulsifier composition are also described.
    Type: Application
    Filed: October 23, 2001
    Publication date: October 24, 2002
    Applicant: Opta Food Ingredients, Inc.
    Inventor: Chienkuo Ronnie Yuan
  • Patent number: 6469161
    Abstract: A chemical fluidification process for a starchy material, which is carried out in a reactor suitable for continuous operation and with a humidity of the reaction mix (starch included) of less thank 25%, which consists in subjecting a starchy material to the hydrolyzing action of a chemical agent. The dwell time of the starchy material in the fluidification reactor is more than 5 minutes and less than 30 minutes. The temperature at the core of said reactor is more than 60° C. and less than 100° C. approximately, a conversion process comprising said chemical fluidification, and starchy materials obtainable by such processes.
    Type: Grant
    Filed: September 10, 1998
    Date of Patent: October 22, 2002
    Inventors: Patrick Fuertes, Anne Lambin
  • Patent number: 6468355
    Abstract: The invention discloses a boiling-stable granular resistant starch product which may comprise over 60% resistant starch as determined by the TDF method. The starch is made by subjecting a starch source to acid hydrolysis, followed by a hydrothermal treatment which is preferably heat-moisture treatment. The boiling-stable granular resistant starch product may be used in fromulating low-fat, high-fiber food products, as a tabletting aid, and as an inhibitor of excessive ice crystal formation in frozen products.
    Type: Grant
    Filed: May 25, 2000
    Date of Patent: October 22, 2002
    Assignee: The Penn State Research Foundation
    Inventors: Donald B. Thompson, Jorge Brumovsky
  • Patent number: 6451121
    Abstract: Thermally-inhibited starches and flours which are functionally equivalent to chemically-crosslinked starches are prepared by a process which comprises the steps of dehydrating a granular starch or flour to anhydrous or substantially anhydrous (<1% moisture) and heat treating the dehydrated starch or flour for a time and at a temperature sufficient to inhibit the starch, (e.g., 120-180° C. for up to 20 hours). Preferably the pH of the starch is adjusted to neutral or greater (e.g., pH 8-9.5) prior to the dehydration. The dehydration may be a thermal dehydration carried out simultaneously with the heat treatment or a non-thermal dehydration carried out by extraction with a solvent (e.g., ethanol) or by freeze drying.
    Type: Grant
    Filed: March 2, 2001
    Date of Patent: September 17, 2002
    Assignee: National Starch and Chemical Investment Holding Corporation
    Inventors: Chung-Wai Chiu, Eleanor Schiermeyer, David J. Thomas, Manish B. Shah, Douglas J. Hanchett, Roger Jeffcoat
  • Patent number: 6447615
    Abstract: The present invention is directed to sago fluidity starch and the use thereof. Such fluidity starches exhibit exceptionally fast gelling properties, high gel strengths, and exceptional elasticity. These properties allow for significantly reduced processing times, including reduced hold times. Further, the higher gel strength allows for reduced starch levels without loss of final product gel strength integrity or texture.
    Type: Grant
    Filed: August 10, 1999
    Date of Patent: September 10, 2002
    Assignee: National Starch and Chemical Investment Holding Corporation
    Inventors: Douglas J. Hanchett, Tunyawat Kasemsuwan, Joseph Light, Ai-Tsing Tan
  • Publication number: 20020117168
    Abstract: Processes for the elimination of deposit formation during starch processing are provided. The processes include one or more of raising the pH of ethylated starch solutions to a pH above 7; adding uncooked oxidized starch to cooked ethylated starch; adjusting the conductivity of uncooked ethylated starch granules; and/or silicone treatment of vessel surfaces.
    Type: Application
    Filed: May 18, 2001
    Publication date: August 29, 2002
    Inventor: James J. Foster
  • Patent number: 6379467
    Abstract: Disclosed is a method for preparing a modified starch hydrolysate that has a relatively reduced tendency to become sticky as compared with the unmodified starch hydrolysate. The method includes the step of compacting a starch hydrolysate, preferably via roller compaction. Also disclosed is a modified starch hydrolysate. The compacted starch hydrolysates may be transported readily, and is useful in numerous applications, including poultry feed applications.
    Type: Grant
    Filed: June 15, 2000
    Date of Patent: April 30, 2002
    Assignee: Grain Processing Corporation
    Inventors: E. Daniel Hubbard, Robert L. Olson, Thomas A. Wiesner, Terry V. Andren, Frank Gute
  • Patent number: 6352733
    Abstract: An enzyme resistant starch type III which has a melting point or endothermic peak of at least about 140° C. as determined by differential scanning calorimetry (DSC) is produced in yields of at least about 25% by weight, based upon the weight of the original starch ingredient. A gelatinization stage, nucleation/propagation stage, and preferably a heat-treatment stage are used to produce reduced calorie starch-based compositions which contain the enzyme resistant starch type III. The enzyme resistant starch is produced using crystal nucleation and propagation temperatures which avoid substantial production of lower melting amylopectin crystals, lower melting amylose crystals, and lower melting amylose-lipid complexes. The nucleating temperature used is above the melting point of amylopectin crystals. The propagating temperature used is above the melting point of any amylose-lipid complexes but below the melting point of the enzyme resistant starch.
    Type: Grant
    Filed: October 6, 1999
    Date of Patent: March 5, 2002
    Assignee: Kraft Foods Holdings, Inc.
    Inventors: Lynn Haynes, Norbert Gimmler, John P. Locke, III, Mee-Ra Kweon, Louise Slade, Harry Levine
  • Patent number: 6348264
    Abstract: A process for producing solid forms comprising the steps of: (1) forming an aqueous composition comprising the low DE starch hydrolysate of the invention; (2) drying said aqueous composition to result in a substantially dry low DE starch hydrolysate composition; (3) shaping said dry low DE starch hydrolysate composition to result in a solid form. A process for producing a coated solid form, comprising the steps of forming an aqueous composition comprising the low DE starch hydrolysate of the present invention and applying to the solid form said aqueous composition in order to form a coated solid form.
    Type: Grant
    Filed: May 9, 2000
    Date of Patent: February 19, 2002
    Assignee: Roquette Freres
    Inventors: Ibrahim Abou-Nemeh, Michael A. Tripodi
  • Patent number: 6322632
    Abstract: The present invention fulfills, in an efficient, cost effective manner, the need for a starch which has a reduced tendency to form amylose crystals after cooking by providing a method using high levels of caustic materials during a reaction of oxidant with uncooked starch granules.
    Type: Grant
    Filed: February 18, 2000
    Date of Patent: November 27, 2001
    Assignee: Archer-Daniels-Midland Corporation
    Inventor: James A. McClain
  • Patent number: 6306218
    Abstract: A method of producing starch-emulsifier compositions by heating a starch in the presence of an emulsifier to form a complex with unique properties. The product can be further treated to obtain greater than about 20% short chain amylose. Starch-emulsifier compositions (e.g., powders, gels, pastes) produced by this method and food products containing the starch-emulsifier composition are also described.
    Type: Grant
    Filed: January 20, 2000
    Date of Patent: October 23, 2001
    Assignee: Opta Food Ingredients, Inc.
    Inventor: Chienkuo Ronnie Yuan
  • Publication number: 20010017133
    Abstract: Thermally-inhibited starches and flours which are functionally equivalent to chemically-crosslinked starches are prepared by a process which comprises the steps of dehydrating a granular starch or flour to anhydrous or substantially anhydrous (<1% moisture) and heat treating the dehydrated starch or flour for a time and at a temperature sufficient to inhibit the starch, (e.g., 120-180° C. for up to 20 hours). Preferably the pH of the starch is adjusted to neutral or greater (e.g., pH 8-9.5) prior to the dehydration. The dehydration may be a thermal dehydration carried out simultaneously with the heat treatment or a non-thermal dehydration carried out by extraction with a solvent (e.g., ethanol) or by freeze drying.
    Type: Application
    Filed: March 2, 2001
    Publication date: August 30, 2001
    Inventors: Chung-Wai Chiu, Eleanor Schiermeyer, David J. Thomas, Manish B. Shah, Douglas J. Hanchett, Roger Jeffcoat
  • Patent number: 6261376
    Abstract: Thermally-inhibited, pregelatinized non-granular starches and flours are prepared by pregelatinizing the starch or flour and thermally inhibiting the starch or flour by dehydrating the starch or flour to anhydrous or substantially anhydrous and then heat treating the dehydrated starch. The pregelatinization may be carried out prior to or after the thermal inhibition using known methods which disrupt the granular structure such by drum drying or jet cooking and spray-drying. Preferably the starch or flour is adjusted to a pH above 7.0 prior to the thermal inhibition. The starch may be dehydrated by heating the starch in a suitable heating apparatus, by extracting the water from the starch using a solvent such as ethanol, or by freeze drying the starch. Preferably the starch or flour is treated with a solvent to remove proteins and/or lipids and thus prevent off flavors.
    Type: Grant
    Filed: November 10, 1999
    Date of Patent: July 17, 2001
    Assignee: National Starch and Chemical Investment Holding Corporation
    Inventors: Roger Jeffcoat, Chung-Wai Chiu, Manish B. Shah, David J. Thomas, Douglas J. Hanchett
  • Patent number: 6231675
    Abstract: Thermally-inhibited starches and flours which are functionally equivalent to chemically-crosslinked starches are prepared by a process which comprises the steps of dehydrating a granular starch or flour to anhydrous or substantially anhydrous (<1% moisture) and heat treating the dehydrated starch or flour for a time and at a temperature sufficient to inhibit the starch, (e.g., 120-180° C. for up to 20 hours). Preferably the pH of the starch is adjusted to neutral or greater (e.g., pH 8-9.5) prior to the dehydration. The dehydration may be a thermal dehydration carried out simultaneously with the heat treatment or a non-thermal dehydration carried out by extraction with a solvent (e.g., ethanol) or by freeze drying.
    Type: Grant
    Filed: June 7, 1999
    Date of Patent: May 15, 2001
    Assignee: National Starch and Chemical Investment Holding Corporation
    Inventors: Chung-Wai Chiu, Eleanor Schiermeyer, David J. Thomas, Manish B. Shah, Douglas J. Hanchett, Roger Jeffcoat
  • Patent number: 6190462
    Abstract: The present invention provides in a method of treating starch, comprising the steps of (1) contacting starch with water to form a slurry and (2) mechanically removing said water from said starch slurry; the improvement comprising incorporating a dewatering composition comprising a dioctyl sulfosuccinate salt and a water miscible polyol into said starch slurry in an amount effective to decrease the water content of the resulting starch cake upon conclusion of the mechanical dewatering step.
    Type: Grant
    Filed: July 2, 1999
    Date of Patent: February 20, 2001
    Assignee: Penford Corporation
    Inventors: Flave E. Markland, David A. Dunn
  • Patent number: 6147175
    Abstract: The invention relates to the field of biological chemistry, and to polysaccharides in particular. Specifically, it concerns biological products obtained as a result of the polymerization and crosslinking in an alkaline medium of a gel, comprised of wheat or spelt wheat flour, in the presence of a dual-function crosslinking reagent. The invention further relates to a process for obtaining said biological products, consisting in forming an aqueous dispersion of flour, rendering this dispersion alkaline by adding an alkaline metal hydroxide, performing polymerization and crosslinking in the presence of a dual-function crosslinking reagent, and drying the resultant gel to obtain a vitreous, lightly colored product with a solid substance content of between 75% and 85% which is then ground into hard particles of a predetermined size. The application of the invention is abrasive particles.
    Type: Grant
    Filed: November 19, 1998
    Date of Patent: November 14, 2000
    Assignee: Syndicat Interprofessionnel Biodecap
    Inventors: Jean-Paul Bonhoure, Jacques Doumeizel, Denis Thery
  • Patent number: 6136097
    Abstract: A process is disclosed for producing thermoplastic starch based on renewable raw materials and, if required, for further processing it into a granulate. A low viscosity starch is modified under a low shearing stress during the extrusion process and leaves the extruder with an increased viscosity in the form of a strip, threads or in other geometrical shapes. The advantages of the invention mainly lie in the improved quality of the starch products, the preservation of the mechanical parts of the extruder installation and the increase of the nominal output of the extruder.
    Type: Grant
    Filed: February 5, 1996
    Date of Patent: October 24, 2000
    Assignee: Biotec Biologische Naturverpackungen GmbH & Co., Forschungs- und Entwichlungs KG
    Inventors: Jurgen Lorcks, Winfried Pommeranz, Kurt Klenke, Harald Schmidt, Joachim Heuer
  • Patent number: 6068705
    Abstract: A process for producing a low DE starch hydrolysate, involves fractionating a starch hydrolysate comprising a DE greater than about 18 using a nanofiltration membrane, having a molecular weight cut-off of less than about 4,000 daltons, under nanofiltration conditions effective to result in a low DE starch hydrolysate comprising a DE of less than about 25. A process for producing a low DE starch hydrolysate blend involves combining the product produced by the process of the present invention with At least one other substance in a predetermined blending ratio to result in a low DE starch hydrolysate blend. A process for hydrogenating a low DE starch hydrolysate produced by the process of the present invention to result in an hydrogenated low DE starch hydrolysate. A process for producing a substantially thermal and shelf-life stable emulsion comprising forming a mixture of the low DE starch hydrolysate of the invention with an effective concentration of at least one ingredient to result in an emulsion.
    Type: Grant
    Filed: December 28, 1998
    Date of Patent: May 30, 2000
    Assignee: Roquette Freres
    Inventors: Dan Tang, Liuming Zhou, Robert Gerhardt, Ibrahim Abou-Nemeh, Carl Jaundoo, Tom Parady
  • Patent number: 6056816
    Abstract: Novel starch-silicate adhesive compositions are disclosed which are of particular advantage in the manufacture of corrugated board. By the controlled combination of starch, alkali silicate and, optionally, caustic soda and borax it has been found possible to produce useable adhesives having much higher levels of solids content than conventional starch-based adhesives, thereby allowing for lowered energy costs in use of the adhesive formulation to manufacture boxboard, as well as improved product quality. The formulation of starch-silicate adhesives according to the invention allows viscosity, rheological characteristics--in particular gelation temperature--and the speed of "green-bond" formation to be controlled and adapted to the requirements of modern high-speed corrugating equipment.
    Type: Grant
    Filed: May 4, 1998
    Date of Patent: May 2, 2000
    Inventors: Rodger Graham Hagens, Michael McDonald, William Millard
  • Patent number: 6013299
    Abstract: An enzyme resistant starch type III which has a melting point or endothermic peak of at least about 140.degree. C. as determined by differential scanning calorimetry (DSC) is produced in yields of at least about 25% by weight, based upon the weight of the original starch ingredient. A gelatinization stage, nucleation/propagation stage, and preferably a heat-treatment stage are used to produce reduced calorie starch-based compositions which contain the enzyme resistant starch type III. The enzyme resistant starch is produced using crystal nucleation and propagation temperatures which avoid substantial production of lower melting amylopectin crystals, lower melting amylose crystals, and lower melting amylose-lipid complexes. The nucleating temperature used is above the melting point of amylopectin crystals. The propagating temperature used is above the melting point of any amylose-lipid complexes but below the melting point of the enzyme resistant starch.
    Type: Grant
    Filed: November 4, 1997
    Date of Patent: January 11, 2000
    Assignee: Nabisco Techology Company
    Inventors: Lynn Haynes, Norbert Gimmler, John P. Locke, III, Mee-Ra Kweon, Louise Slade, Harry Levine
  • Patent number: 6010574
    Abstract: Thermally-inhibited, pregelatinized non-granular starches and flours are prepared by pregelatinizing the starch or flour and thermally inhibiting the starch or flour by dehydrating the starch or flour to anhydrous or substantially anhydrous and then heat treating the dehydrated starch. The pregelatinization may be carried out prior to or after the thermal inhibition using known methods which disrupt the granular structure such by drum drying or jet cooking and spray-drying. Preferably the starch or flour is adjusted to a pH above 7.0 prior to the thermal inhibition. The starch may be dehydrated by heating the starch in a suitable heating apparatus, by extracting the water from the starch using a solvent such as ethanol, or by freeze drying the starch. Preferably the starch or flour is treated with a solvent to remove proteins and/or lipids and thus prevent off flavors.
    Type: Grant
    Filed: October 28, 1997
    Date of Patent: January 4, 2000
    Assignee: National Starch and Chemical Investment Holding Corporation
    Inventors: Roger Jeffcoat, Chung-Wai Chiu, Manish B. Shah, David J. Thomas, Douglas J. Hanchett
  • Patent number: 5989350
    Abstract: Heat-modified starch having a Brabender viscosity in aqueous dispersion at 6% by weight of between 750-900 B.U, after 5 min at 95.degree. C. The starch is heat treated with a monoglyceride.
    Type: Grant
    Filed: July 27, 1998
    Date of Patent: November 23, 1999
    Assignee: Nestec S.A.
    Inventors: Monica Fischer, Pierre Wursch, Eric Plante
  • Patent number: 5964950
    Abstract: A method and apparatus for cooking a starch solution and then dispensing that cooked starch solution to a commercial laundry washer provides a vessel with an interior surrounded by a wall for holding a volume of liquid, a water supply inlet for supplying water to the vessel interior, an opening for adding dry starch to the vessel interior, and a steam supply inlet for adding steam to the vessel interior so that the volume of liquid within the vessel can be heated. A level controller controls the level of fluid within the vessel in between the minimum and maximum levels. A recirculation flow line has an inlet and outlet that each communicate with the vessel interior. A gear pump mounted in the recirculation flow line pumps fluid from the inlet to the outlet in a recirculating fashion, the pump having a geared portion that breaks up starch lumps flowing in the recirculation flow line.
    Type: Grant
    Filed: December 10, 1997
    Date of Patent: October 12, 1999
    Inventor: David W. Boling
  • Patent number: 5959102
    Abstract: The present invention is directed to purifying starch granules from starch-bearing crops, preferably maize, which include treating starch granules with a thermally tolerant, broad pH range proteolytic enzyme that is specific for surface-associated proteins. Also disclosed are purified starch granules which are substantially free of surface-associated proteins. Uses of the isolated starch granules are disclosed.
    Type: Grant
    Filed: June 30, 1997
    Date of Patent: September 28, 1999
    Assignee: Rutgers University
    Inventors: Bruce Wasserman, Chen Mu-Forster
  • Patent number: 5954883
    Abstract: The present invention is directed to a waxy maize starch derived from a single plant which is heterozygous for the recessive sugary-2 allele. Such starch has excellent low temperature and freeze-thaw stability, a relatively high peak viscosity, a relatively high pasting temperature, and intact granules. The starch is useful in a wide variety of food, pharmaceutical, and industrial applications.
    Type: Grant
    Filed: October 8, 1996
    Date of Patent: September 21, 1999
    Assignee: National Starch and Chemical Investment Holding Corporation
    Inventors: Barry J. Nagle, Joseph L. Emling, William R. Mason, Roger Jeffcoat
  • Patent number: 5932017
    Abstract: Thermally-inhibited starches and flours which are functionally equivalent to chemically-crosslinked starches are prepared by a process which comprises the steps of dehydrating a granular starch or flour to anhydrous or substantially anhydrous (<1% moisture) and heat treating the dehydrated starch or flour for a time and at a temperature sufficient to inhibit the starch, (e.g., 120-180.degree. C. for up to 20 hours). Preferably the pH of the starch is adjusted to neutral or greater (e.g., pH 8-9.5) prior to the dehydration. The dehydration may be a thermal dehydration carried out simultaneously with the heat treatment or a non-thermal dehydration carried out by extraction with a solvent (e.g., ethanol) or by freeze drying.
    Type: Grant
    Filed: January 29, 1996
    Date of Patent: August 3, 1999
    Assignee: National Starch and Chemical Investment Holding Corporation
    Inventors: Chung-Wai Chiu, Eleanor Schiermeyer, David J. Thomas, Manish B. Shah, Douglas J. Hanchett, Roger Jeffcoat
  • Patent number: 5929231
    Abstract: The subject of the invention is a method for preparing fine-granuled starch from kernels of oats or rice. In the method, the kernels are ground and the starch is separated from the starch containing fraction obtained by the milling. An essential feature of the invention is that a suspension of the said fraction or of starch separated from it is treated with a surface-active agent or a lipolytic enzyme for disintegrating compound granules or aggregates of starch granules. Except the particle size, also functional properties of starch are affected. Disintegration of compound granules is enhanced by alkaline conditions and by mixing of the suspension. The fine-granuled starch obtained can be applied in foods and, for instance, for biodegradable plastics and for surface treatment agents. The invention can be included as a part of an integrated fractionation process, in which, in addition to starch, an oil fraction, an enriched fibre fraction, and a surplus fraction suitable for feed, are obtained.
    Type: Grant
    Filed: January 17, 1997
    Date of Patent: July 27, 1999
    Assignee: Exavena Oy
    Inventors: Yrjo Malkki, Olavi Myllymaki, Risto Tuomela
  • Patent number: 5928707
    Abstract: A food product is prepared by mixing (i) a native starch having, by weight, an amylose content of from about 10% to 30%, (ii) a lipid emulsifier which complexes amylose and (iii) water to obtain a dispersion, heating the dispersion first at a temperature below a gelatinization temperature of the amylose for a time for complexing the amylose and emulsifier and then at a temperature to gelatinize the starch and obtain a heated dispersion of intact swollen starch granules and the heated dispersion is cooled to obtain a food product having intact swollen starch granules. The native starch is employed in an amount of between 5% and 30% by weight based upon water weight and the emulsifier is employed in an amount of between 5% and 15% by weight based upon amylose content weight. The food product has a complex viscosity at 0.4 Hz of between 200 Pa.s. and 700 Pa.s.
    Type: Grant
    Filed: June 17, 1997
    Date of Patent: July 27, 1999
    Assignee: Nestec S.A.
    Inventors: Birgitt Mahr, Hans Uwe Trueck