Abstract: The invention relates to a method for manufacturing or modifying an endodontic instrument made from an NiTi alloy, comprising a heat-treatment. The invention further relates to an endodontic instrument, preferably obtained by the method, having superior properties with regard to cyclic fatigue resilience.

Abstract: An induction heating apparatus of a plate-like member for arranging a plate-like member having a three-dimensional structure so that it is interposed between a pair of plate-like coils and inductively heating the plate-like member, the pair of plate-like coils having a three-dimensional structure that corresponds to the plate-like member and being arranged to be opposed to each other. The plate-like member arranged between the pair of plate-like coils includes a plurality of surfaces in a predetermined cross section perpendicular to a current that flows through the plate-like coil pair, and each of the coils of the plate-like coil pair is divided into a plurality of turns along the direction in which the current flows for at least each of the plurality of surfaces of the plate-like member.

Abstract: Embodiments of the present disclosure generally relate to protective coatings on substrates and methods for depositing the protective coatings. In one or more embodiments, a method of forming a protective coating on a substrate includes depositing a chromium oxide layer containing amorphous chromium oxide on a surface of the substrate during a first vapor deposition process and heating the substrate containing the chromium oxide layer comprising the amorphous chromium oxide to convert at least a portion of the amorphous chromium oxide to crystalline chromium oxide during a first annealing process. The method also includes depositing an aluminum oxide layer containing amorphous aluminum oxide on the chromium oxide layer during a second vapor deposition process and heating the substrate containing the aluminum oxide layer disposed on the chromium oxide layer to convert at least a portion of the amorphous aluminum oxide to crystalline aluminum oxide during a second annealing process.

Abstract: A method for manufacturing a press-molded article may include molding a blank material which is a steel plate into a press-molded article by sandwiching the blank material between a first molding surface and a second molding surface of a die, and press-molding the blank material into a predetermined shape. The method for manufacturing a press-molded article may include irradiating a predetermined portion of the press-molded article with infrared light after removing the press-molded article from the die.

Abstract: A method of processing a metal alloy includes heating to a temperature in a working temperature range from a recrystallization temperature of the metal alloy to a temperature less than an incipient melting temperature of the metal alloy, and working the alloy. At least a surface region is heated to a temperature in the working temperature range. The surface region is maintained within the working temperature range for a period of time to recrystallize the surface region of the metal alloy, and the alloy is cooled so as to minimize grain growth. In embodiments including superaustenitic and austenitic stainless steel alloys, process temperatures and times are selected to avoid precipitation of deleterious intermetallic sigma-phase. A hot worked superaustenitic stainless steel alloy having equiaxed grains throughout the alloy is also disclosed.

Abstract: Disposable cutting blades and method for producing disposable cutting blades with profiled cross sections for a device for chipping wood. The method includes heating a primary material of a hardenable material in a soft-annealed state having a worked surface to a temperature above room temperature, but below a conversion temperature Ac1, rolling the primary material to form a profile blank with at least one precisely gaged guide path in a base body in cross section and with an increased thickness of at least one edge region, a metal-removing working of at least one edge region in a longitudinal direction of the profile blank to form a cutting edge and to form scratching edges in a spaced manner directed perpendicularly to the cutting edge, and continuously hardening the edge regions of the cutting blade.

Abstract: Disclosed herein is a partial heat treatment method using a double metal layer, in which a surface of a workpiece is hardened by heat treatment, including the steps of: primarily plating the surface of the workpiece with a first metal layer; secondarily plating the surface of the first metal layer with a second metal layer; partially stripping the first metal layer and the second metal layer to expose a part of the surface of the workpiece; heat-treating the workpiece to harden the exposed surface of the workpiece; and removing the first metal layer and the second metal layer remaining on the surface of the workpiece.

Abstract: The invention relates to a method for producing a metal structural component, in particular a vehicle structural component, in which a steel part is hot formed and is hardened at least over sections by contact with a tool surface, in which the steel part is during the hardening cooled in at least two partial regions at different cooling rates, so that the partial regions after the hardening differ in their microstructure, wherein the cooling rates differing from one another are produced by sections of the tool surface corresponding to the partial regions of the steel part, which differ from one another as regards their thermal conductivities. The invention also relates to a further method for producing a metal structural component, as well as a tool and a batch furnace.

Abstract: In order to sharpen and harden a corner portion of a score line edge portion of an iron golf club having a plurality of score lines on a face surface within a prescribed range, heat input is implemented on an edge portion of a groove through laser irradiation after the groove is machined and, as a result, the edge portion is hardened and melted to form a rounded corner R. The hardness is set at a Vickers hardness value (HV) of at least 350. The corner R forms a part of a contour line of the edge portion and this contour line is formed to exist between a first circle that contacts the face surface and a side surface of the groove and has a radius of 0.010 inches (0.254 millimeters) and a second circle that is concentric with the first circle and has a radius of 0.011 inches (0.2794 millimeters).

Abstract: Medical implants with non-equilibrium surface structures are disclosed. The surface treatment of the implants greatly enhances osseointegration, reduces time to recovery following implant surgery, reduces surgery-related infections, and improves outcomes. The implants, including dental implants and other implants for insertion into or attachment to bone, are applicable to treatment of a wide variety of medical conditions. The methods of altering the surface properties of medical implants include exposure of a crystalline surface material, such as metal or ceramic, to a short burst of high thermal energy or shock, resulting in the introduction of a non-equilibrium concentration of crystal lattice defects in a surface layer.

Abstract: A heat treatment technique may include heating an alloy component to a temperature above a transition temperature of the alloy or heating an alloy component to a temperature below the transition temperature of the alloy. The heat treatment technique further may include cooling a first portion of the alloy component at a first cooling rate, and cooling a second portion of the alloy component at a second cooling rate different than the first rate. The first cooling rate may result in formation of a plurality of first precipitate phase domains comprising a first average size in the first portion, and the second cooling rate may result in formation of a plurality of second precipitate phase domains comprising a second average size in the second portion. The average size of the first precipitate phase domains may be different than the average size of the second precipitate phase domains.

Abstract: This ultrasonic oscillation probe is an ultrasonic oscillation probe for transmitting ultrasonic vibration. A first region where the crystal grain size is relatively small and a second region where the crystal grain size is relatively large are respectively formed in at least one place. A method for manufacturing an ultrasonic oscillation probe respectively forms a first region where the crystal grain size is relatively small and a second region where the crystal grain size is relatively large in at least one place and heats a portion of the ultrasonic oscillation probe to a grain coarsening temperature or higher of a material that forms the ultrasonic oscillation probe, to form the second region.

Abstract: A method for producing an automobile column is disclosed. The automobile column has a region of a first type and a region of a second type which have mutually different strengths. A transition region having a width of less than 50 mm is formed between the two regions. The automobile column has in the region of the first type a bainitic structure and in the region of the second type a martensitic structure.

Abstract: A heat treatment technique may include heating an alloy component to a temperature above a transition temperature of the alloy or heating an alloy component to a temperature below the transition temperature of the alloy. The heat treatment technique further may include cooling a first portion of the alloy component at a first cooling rate, and cooling a second portion of the alloy component at a second cooling rate different than the first rate. The first cooling rate may result in formation of a plurality of first precipitate phase domains comprising a first average size in the first portion, and the second cooling rate may result in formation of a plurality of second precipitate phase domains comprising a second average size in the second portion. The average size of the first precipitate phase domains may be different than the average size of the second precipitate phase domains.

Abstract: A method for hardening a portion of the outer surface of a downhole tool body includes friction stirring the vulnerable surface of the tool. Such friction stirring generally includes rotating a friction stir weld tool in contact with the surface until a portion of the tool penetrates the tool. The friction stir weld tool is then translated (while rotating) across a predetermined region of the surface thereby creating a friction stir zone. The friction stir zone is generally considerably harder, and therefore more wear resistant, than the parent material that makes up the tool body. The resulting downhole tool includes at least one surface with a hard friction stir zone.

Abstract: A method for forming a part having a dual property microstructure includes the steps of: forming a blank having a narrow top portion and a wide base portion; heating the blank to an elevated temperature; and forming a dual property microstructure in the blank by cooling different portions of the blank at different cooling rates.

Abstract: A method of controlling the location at which yielding initiates a load bearing component and the collapse mode that is activated at the site of yielding for a designated type of loading is claimed. The steps include selecting a desired area of deformation and a kinematic mode of collapse; selecting a strength-altering pattern including at least a strengthening or weakening zone to control the location in a component where plastic deformation occurs, such that the pattern causes deformation to proceed into a desired collapse mode or shape with the component is subjected to design loading; and applying the strength-altering pattern to the component by friction stir processing, forming at least a strengthened or weakened zone relative to the base material of the component.

Abstract: An elevated temperature forming system in which a sheet metal workpiece is provided in a first stage position of a multi-stage pre-heater, is heated to a first stage temperature lower than a desired pre-heat temperature, is moved to a final stage position where it is heated to a desired final stage temperature, is transferred to a forming press, and is formed by the forming press. The preheater includes upper and lower platens that transfer heat into workpieces disposed between the platens. A shim spaces the upper platen from the lower platen by a distance greater than a thickness of the workpieces to be heated by the platens and less than a distance at which the upper platen would require an undesirably high input of energy to effectively heat the workpiece without being pressed into contact with the workpiece.

Abstract: Disclosed are methods, systems and apparatus for manufacturing complex three dimensional open structures by cold forming the component from unhardened metal stock and then selectively heating and quenching the metal to provide the desired strength profile across the component. The metal is initially formed of unheated and unhardened metal through a combination of rolling, stamping and/or milling operations to produce a component having a complex three dimensional open structure. The formed component is then hardened in strategically predetermined areas by sequentially heating and quenching the predetermined areas of the component. The heating and cooling elements are, in turn, provided on at least one robotic apparatus configured for moving the elements across the surface of the component in a manner sufficient to achieve the desired pattern of hardened and unhardened regions across the component.

Abstract: A method of forming an article from a metal alloy sheet material includes selectively hardening only a first localized area of the metal alloy sheet material without hardening a second localized area of the metal alloy sheet material, wherein the second area adjoins the first area to thereby form a blank. The blank has a hardened region formed from the first area and having a first hardness, and a non-hardened region adjoining the hardened region and formed from the second area, and having a second hardness that is less than the first hardness. The method includes stamping the blank to thereby form a preform having a pre-protrusion at least partially formed from the hardened region, wherein the pre-protrusion has a first height, annealing the preform to thereby form a workpiece, and stamping the workpiece to increase the first height and thereby form the article.

Abstract: A method of forming an article from a metal alloy sheet material includes stamping the metal alloy sheet material to thereby form a preform having at least one protrusion. The at least one protrusion includes a base portion, a first region having a first thickness and spaced apart from the base portion to thereby have a first maximum height, and a second region interconnecting the base portion and the first region and having a second thickness that is greater than the first thickness. After stamping, the method includes selectively annealing the second region without substantially annealing the first region, and, after selectively annealing, concurrently increasing the first maximum height and substantially equalizing the first thickness and the second thickness to thereby form the article.

Abstract: An Al—Mg—Si based aluminum alloy sheet having undergone normal-temperature aging (or being in a underaged state) after a solution treatment thereof is, before press forming, subjected to a heating treatment (partial reversion heating treatment) in which the alloy sheet is partially heated to a temperature in the range of 150 to 350° C. for a time of not more than 5 minutes so that the difference in strength (difference in 0.2% proof stress) between the heated part and the non-heated part will be not less than 10 MPa. The alloy sheet thus treated is subjected to cold press forming in the condition where the heated part with low strength is put in contact with a wrinkle holding-down appliance of the press and the non-heated part with high strength is put in contact with the shoulder part (radius) of the punch. In the partial reversion heating treatment, the temperature rise rate and the cooling rate in cooling down to 100° C. or below are set to be not less than 30° C./min.

Abstract: The invention relates to a method for producing a metal structural component, in particular a vehicle structural component, in which a steel part is hot formed and is hardened at least over sections by contact with a tool surface, in which the steel part is during the hardening cooled in at least two partial regions at different cooling rates, so that the partial regions after the hardening differ in their microstructure, wherein the cooling rates differing from one another are produced by sections of the tool surface corresponding to the partial regions of the steel part, which differ from one another as regards their thermal conductivities. The invention also relates to a further method for producing a metal structural component, as well as a tool and a batch furnace.

Abstract: A manufacturing method for a bent product which can guarantee a high working accuracy and which can provide a large bending angle without damage to the surface condition of a metal material even when a widely varying bent shape is desired or when it is necessary to perform bending of a high strength metal material.

Abstract: The invention relates to a method for producing a component, made of an iron-chromium alloy that precipitates Laves phases and/or particles containing Fe and/or particles containing Cr and/or particles containing Si and/or carbides, by subjecting a semi-finished product made of the alloy to a thermomechanical treatment, wherein in a first step, the alloy is solution heat treated at temperatures?the solution heat treatment temperature and is subsequently quenched in stationary protective gas or air, moving (blown) protective gas or air, or water. In a second step, a mechanical forming of the semi-finished product in a range from 0.05 to 99% is performed, and in a subsequent step, Laves phases Fe2(M, Si) or Fe7(M, Si)6 and/or particles containing Fe and/or particles containing Cr and/or particles containing Si and/or carbides are precipitated in a specific and finely distributed manner in that the component produced from the formed semi-finished product is brought to an application temperature between 550° C.

Abstract: A method for producing a metallic component (B) allows adjoining zones (Z1, Z2, Z3) having differing material properties to be produced in a manner which is simple in terms of production. This is achieved in that a sheet metal element (E) heated to a forming temperature is shaped in a forming tool (1) into an end-shaped component (B), wherein the forming tool (1) has a temperature adjustment means for adjusting the temperature of at least one of the portions (5, 7, 16) thereof that comes into contact with the sheet metal element (E) during the forming process, and in that the forming speed is controlled in consideration of the time for which the portion (5, 7, 16) of the forming tool (1) that is regulated with regard to the temperature thereof is in contact with the respective region (E1, E2, E3) of the sheet metal element (E) that rests against said portion.

Abstract: A method of forming a product from an initial blank comprises subjecting the initial blank to a hot forming and press hardening operation to form the product with substantially a uniform first tensile strength. Subsequently, the product is subjected to post hot-forming processing in which a first region of the product is heated selectively to above a known temperature, using one of conduction heating, resistance heating, and induction heating. The first region is then cooled, such that the first region attains a second tensile strength that is substantially less than the first tensile strength.

Abstract: A device and to a corresponding method for partially hardening a metallic work piece, in which the work piece is transported in a continuous furnace along a conveying direction by means of a conveyor and partially heated by means of a heating device. It is proposed that the heating device generates at least one heating zone that is moved in the conveying direction together with the work piece.

Abstract: A method for hardening a portion of the outer surface of a downhole tool body includes friction stirring the vulnerable surface of the tool. Such friction stirring generally includes rotating a friction stir weld tool in contact with the surface until a portion of the tool penetrates the tool. The friction stir weld tool is then translated (while rotating) across a predetermined region of the surface thereby creating a friction stir zone. The friction stir zone is generally considerably harder, and therefore more wear resistant, than the parent material that makes up the tool body. The resulting downhole tool includes at least one surface with a hard friction stir zone.

Abstract: A method for producing a structural and/or safety-related motor vehicle component having at least one hot-formed and press-hardened part constructed from high-strength steel includes the steps of partially heat-treating a region of the motor vehicle component by heating the region to a heat-up temperature in a temperature range between 500° C. and 900° C.; maintaining the heat-up temperature for a duration of a holding time; and cooling down from the heat-up temperature in one or more phases. A body component constructed as a structural and/or safety-related motor vehicle component from a steel sheet blank that has been hot-formed and press-hardened includes joining flanges and/or coupling locations and/or safety-related parts, wherein the joining flanges, coupling locations and/or safety-related parts are partially heat-treated in several steps with the disclosed method.

Abstract: A unique heat treat method for relieving stresses caused by a repairing weld joint in a full hoop part heat treats locally, at the location of the weld joint, and at a diametrically opposed location. By providing the diametrically opposed heat treat location, the present invention relieves stresses caused by the weld joint, without creating any additional residual stress in the weld joint.

Abstract: Medical instruments, particularly, endodontic instruments with unique limited memory characteristics, and methods for making such instruments. One embodiment includes heat treating a finished endodontic instrument. A related embodiment includes electropolishing a finished endodontic instrument and then heat treating the endodontic instrument.

Abstract: A method for developing fine grained, thermally stable metallic material in which friction stir welding or friction stir processing is performed along at least a portion of the material. Thereafter, a thin layer is removed from either side, or both sides of the material to eliminate the origin of abnormal grain growth occurring when the friction stir welded or friction stir processed material is subjected to subsequent hot forming processes. A sheet of extraneous material is optionally attached to either side, or both sides of the material prior to the friction stir welding or friction stir processing, and this extraneous material is removed after the friction stir welding or friction stir processing. A layer containing pinning particles or a sheet of extraneous material containing pinning particles is further optionally introduced on either side, or both sides of the material prior to the friction stir processing.

Abstract: Heat treatment processes for hardening a workpiece such as a turbine blade include attaching a spacer to a workpiece surface, wherein the spacer comprises an inner profile mirroring the workpiece surface and an outer profile effective to generally uniformly distribute heat to the workpiece surface, heating the spacer to uniformly heat the workpiece surface at a temperature effective to form an austenitic microstructure in the workpiece surface, cooling the workpiece surface at a rate effective to transform the austenitic microstructure to a martensitic microstructure, and removing the spacer from the workpiece prior to or subsequent to cooling.

Abstract: The invention relates to a heat treatment method for monocrystalline or directionally solidified structural components. Said method comprises a heat treatment which results in dissolving at least one crystalline phase of the material of the structural component, referred to in the following as component material. The inventive method is characterized by carrying out the heat treatment by heating the structural component to a dissolution temperature required for dissolving the crystalline phase only in at least one first component area in which the stresses within the component material do not exceed a predetermined value. In at least one second component area in which the stresses within the component material exceed the predetermined value the material is only heated to a temperature below the dissolution temperature.

Abstract: A heat treatment technique may include heating an alloy component to a temperature above a transition temperature of the alloy or heating an alloy component to a temperature below the transition temperature of the alloy. The heat treatment technique further may include cooling a first portion of the alloy component at a first cooling rate, and cooling a second portion of the alloy component at a second cooling rate different than the first rate. The first cooling rate may result in formation of a plurality of first precipitate phase domains comprising a first average size in the first portion, and the second cooling rate may result in formation of a plurality of second precipitate phase domains comprising a second average size in the second portion. The average size of the first precipitate phase domains may be different than the average size of the second precipitate phase domains.

Abstract: Refractory metal products, such as tantalum, can be rejuvenated after metal consumption in selected zones by filling the zones with powder and simultaneously applying focused radiant energy to the powder.

Abstract: A unique heat treat method for relieving stresses caused by a repairing weld joint in a full hoop part heat treats locally, at the location of the weld joint, and at a diametrically opposed location. By providing the diametrically opposed heat treat location, the present invention relieves stresses caused by the weld joint, without creating any additional residual stress in the weld joint.

Abstract: In a method for press-hardening a metallic formed structure made of a hardenable steel sheet, the steel sheet is heated above a transition temperature Ac3 and then placed in a cooled press having a forming tool with at least one uncooled contour section for forming a region of reduced hardness. Marginal regions of the steel sheet are clamped with a sheet holder arrangement which has an inner sheet holder and an outer sheet holder. The inner sheet holder is hereby located closer to the forming tool than the outer sheet holder. The sheet holder arrangement is configured to slow down flow of the marginal regions into the forming tool. After closing the press tool, the steel sheet is formed in a first forming phase by holding the marginal region with the outer sheet holder and in a subsequent forming phase by holding the marginal region with the inner sheet holder.

Abstract: A single crystal component comprising a first region and a second region. The component comprising a nickel base single crystal superalloy having a gamma phase matrix and gamma prime phase precipitates distributed in the gamma phase matrix. The first region of the component comprises a bi-modal distribution of gamma prime phase precipitates in the gamma phase matrix and the second region of the component comprising a uni-modal distribution of gamma prime phase precipitates in the gamma phase matrix.

Abstract: The invention relates to a process for manufacturing a sputter target. The process comprises the steps of—providing a target holder (12); —applying an intermediate layer (14) on said target holder; —applying a top layer (16) on top of said intermediate layer; said top layer comprising a material having a melting point which is substantially higher than the melting point of said target material; —heating the target holder coated with said intermediate layer and said top layer.

Abstract: A heat treating method for a golf club head includes preparing a golf club head having at least one heat treating zone. A protrusion is provided on the heat treating zone. Heat treatment is carried out on the protrusion by a high-energy beam, and the protrusion is removed after the heat treatment. The properties of the material of the golf club head are improved without sacrificing appearance of the golf club head.

Abstract: Systems and methods for providing localized heat treatment of metal components are provided. In this regard, a representative method includes: identifying a portion of a metal component to which localized heat treatment is to be performed; shielding an area in a vicinity of the portion of the metal component; and directing electromagnetic energy in the infrared (IR) spectrum toward the portion of the metal component such that the portion is heated to a desired temperature and such that the area in the vicinity of the portion that is subjected to shielding does not heat to the temperature desired for the heat treatment.

Abstract: A rail manufacturing method is provided, in which a billet is hot-rolled into a rail form and the rail is cooled to ambient temperature. The foot part of the rail can be mechanically restrained to improve the straightness of the rail during at least the period of cooling where the surface temperature is between 800° C. and 400° C. In the subsequent cooling process, at least while the surface temperature of the foot of the rail is between 400° C. and 250° C., the rail is kept in an upright state, and cooled naturally without using insulation or accelerated cooling.

Abstract: A method for quenching a metal workpiece having an internal passage with at least one open end, wherein the workpiece has a plurality of bore holes extending between the internal passage and the external surface, the method including the steps of pressurizing the internal passage with a pressurized fluid source to prevent quenchant from entering the internal passage and the plurality of bore holes; flowing quenchant across the external surface to cool and harden the workpiece.

Abstract: A method for manufacturing a complex heat treated tubular structure includes making a tube assembly having tube portions along its length of differing characteristic. The tube assembly is formed by lengthwise tube bending and hydroforming to provide a desired shape. The tube is formed by lengthwise tube bending and hydroforming to provide a desired shape. The tube is supported in a locating fixture having a plurality of supports spaced along the tube to support the tube against distortion. A local region of the tube is heated in at least one local region to a temperature to heat treat the local region. A quenching medium is then flushed through the hollow interior of the tube, and the tube is removed from the locating fixture..

Abstract: A crankshaft having a crankpin, a crank journal, and a crank arm for linking the crankpin and the crank journal, includes a pin fillet portion located between the crankpin and the crank arm, and a journal fillet portion located between the crank journal and the crank arm. At least one of the crankpin and the crank journal has a diameter of no less than about 20 mm and no more than about 40 mm. At least one of the pin fillet portion and the journal fillet portion contains a quench-hardened layer having a thickness of no less than about 1 mm and no more than about 2 mm in the vicinity of a surface thereof. The crankpin and the crank journal substantially do not contain any quench-hardened layer having a thickness exceeding about 2 mm in the vicinity of a surface thereof.

Abstract: A spacer 44 is inserted between an upper end face 44a of a contact column 40, and a lower face of a flange 14. The flange 14 is supported at plural positions by supporting columns 42. In heating a shoulder portion 16 to a hardening temperature, an electroconductive member 56 is placed close to the shoulder portion 16, and an AC current having a frequency which will cause mutual attraction between the current flowing through the elctroconductive member 56 and the current flowing through the shoulder portion 16 is applied to flow through the electroconductive member 56. The shoulder portion 16 having been heated to the hardening temperature is quenched by ejecting a liquid coolant through ejection outlets of a cooling jacket.

Abstract: A method of performing manufacturing operations on a workpiece made of a high strength alloy is disclosed in which a local area of a workpiece is heated to micro-structurally soften the local area. The local area of the workpiece becomes softened and more ductile. A manufacturing operation involving deformation of the heat softened area is performed with the metal in the heat softened region being more ductile and having less strength than the surrounding portions thereof. Manufacturing operations may include riveting, clinching, hydro-forming, and magnetic pulse joining.

Abstract: Described is a high quality sputtering target and method of manufacture which involves application of equal channel angular extrusion.