Spur Tubes Patents (Class 159/28.3)
  • Patent number: 6998026
    Abstract: A tert-C4–C8-alkyl (meth)acrylate is prepared by reacting (meth)acrylic acid with an olefin of the formula where R1 and R2, which may be identical or different, are methyl or ethyl and R3 is H, methyl or ethyl, in homogeneous phase in the presence of an acidic catalyst and isolating the tert-C4–C8-alkyl (meth)acrylate from the reaction mixture, by a process in which the catalyst is separated off as residue by a two-stage distillation of the reaction mixture and the tert-C4–C8-alkyl (meth)acrylate is isolated from the distillates. The novel process makes it possible to use acetic acid-containing (meth)acrylic acid. The danger of cleavage of the ester and of polymerization of (meth)acrylic compounds is reduced.
    Type: Grant
    Filed: July 27, 2001
    Date of Patent: February 14, 2006
    Assignee: BASF Aktiengesellschaft
    Inventors: Ruprecht Kroker, Gerhard Nestler, Werner Schmitt, Winfried Schumm
  • Patent number: 6887345
    Abstract: The present invention relates to a process and a device for evaporating liquids, for example black liquor from cellulose cooking, which contain solid and dissolved substances which are to be concentrated. The liquid is heated to close to boiling temperature in a heat exchanger (1) of the falling-film type. The process is characterized in that the pressure on the liquid side in the falling-film heat exchanger (1) is kept so high that boiling does not take place in this heat exchanger and in that the evaporation takes place, by means of flashing, in a separate expansion tank (7) that has a lower steam.
    Type: Grant
    Filed: November 20, 2001
    Date of Patent: May 3, 2005
    Assignee: Kvaerner Pulping AB
    Inventors: Ismo Hirvonen, Randy Stern
  • Publication number: 20030127315
    Abstract: A tert-C4-C8-alkyl (meth)acrylate is prepared by reacting (meth)acrylic acid with an olefin of the formula 1
    Type: Application
    Filed: January 27, 2003
    Publication date: July 10, 2003
    Inventors: Ruprecht Kroker, Gerhard Nestler, Werner Schmitt, Winfried Schumm